CN103652868A - Method for preparing lotus plumule superfine powder with airflow superfine grinding technology - Google Patents
Method for preparing lotus plumule superfine powder with airflow superfine grinding technology Download PDFInfo
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- CN103652868A CN103652868A CN201310615488.4A CN201310615488A CN103652868A CN 103652868 A CN103652868 A CN 103652868A CN 201310615488 A CN201310615488 A CN 201310615488A CN 103652868 A CN103652868 A CN 103652868A
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- 240000002853 Nelumbo nucifera Species 0.000 title claims abstract description 31
- 235000006508 Nelumbo nucifera Nutrition 0.000 title claims abstract description 31
- 235000006510 Nelumbo pentapetala Nutrition 0.000 title claims abstract description 31
- 239000000843 powder Substances 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000005516 engineering process Methods 0.000 title abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 239000000463 material Substances 0.000 claims description 13
- 238000004891 communication Methods 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 235000012054 meals Nutrition 0.000 claims description 4
- 238000010298 pulverizing process Methods 0.000 claims description 4
- 239000001506 calcium phosphate Substances 0.000 claims description 3
- 239000008187 granular material Substances 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 230000001954 sterilising effect Effects 0.000 claims description 3
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 3
- 229940078499 tricalcium phosphate Drugs 0.000 claims description 3
- 229910000391 tricalcium phosphate Inorganic materials 0.000 claims description 3
- 235000019731 tricalcium phosphate Nutrition 0.000 claims description 3
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 abstract description 6
- 239000002245 particle Substances 0.000 abstract description 6
- 238000010521 absorption reaction Methods 0.000 abstract description 5
- 239000004480 active ingredient Substances 0.000 abstract description 5
- 229930013930 alkaloid Natural products 0.000 abstract description 2
- 150000003797 alkaloid derivatives Chemical class 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 230000007547 defect Effects 0.000 abstract 2
- 230000002776 aggregation Effects 0.000 abstract 1
- 238000004220 aggregation Methods 0.000 abstract 1
- 239000002552 dosage form Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 abstract 1
- 230000035764 nutrition Effects 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 8
- 238000004090 dissolution Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000002904 solvent Substances 0.000 description 3
- WUYQEGNOQLRQAQ-CQSZACIVSA-N (+)-pronuciferine Chemical compound C([C@H]1N(C)CCC=2C=C(C(=C3C=21)OC)OC)C13C=CC(=O)C=C1 WUYQEGNOQLRQAQ-CQSZACIVSA-N 0.000 description 2
- 229940126678 chinese medicines Drugs 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- WUYQEGNOQLRQAQ-UHFFFAOYSA-N (+)-pronuciferine Natural products C1=2C3=C(OC)C(OC)=CC=2CCN(C)C1CC13C=CC(=O)C=C1 WUYQEGNOQLRQAQ-UHFFFAOYSA-N 0.000 description 1
- KALAUPFACUJBAU-ZRBLBEILSA-N (1R,9R,10R)-6-benzyl-17-azatetracyclo[7.5.3.01,10.02,7]heptadeca-2,4,6-triene Chemical class C=1C=CC([C@@]23CCN[C@@H]([C@@H]3CCCC2)C2)=C2C=1CC1=CC=CC=C1 KALAUPFACUJBAU-ZRBLBEILSA-N 0.000 description 1
- -1 C19H23NO3 Chemical compound 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- AJPXZTKPPINUKN-UHFFFAOYSA-N Isoliensinin Natural products C1=CC(OC)=CC=C1CC1C2=CC(OC=3C(=CC=C(CC4C5=CC(O)=C(OC)C=C5CCN4C)C=3)O)=C(OC)C=C2CCN1C AJPXZTKPPINUKN-UHFFFAOYSA-N 0.000 description 1
- AJPXZTKPPINUKN-FIRIVFDPSA-N Isoliensinine Chemical compound C1=CC(OC)=CC=C1C[C@@H]1C2=CC(OC=3C(=CC=C(C[C@@H]4C5=CC(O)=C(OC)C=C5CCN4C)C=3)O)=C(OC)C=C2CCN1C AJPXZTKPPINUKN-FIRIVFDPSA-N 0.000 description 1
- XCUCMLUTCAKSOZ-FIRIVFDPSA-N Liensinine Chemical compound C([C@@H]1C=2C=C(C(=CC=2CCN1C)OC)OC=1C(O)=CC=C(C=1)C[C@H]1N(C)CCC=2C=C(C(=CC=21)OC)OC)C1=CC=C(O)C=C1 XCUCMLUTCAKSOZ-FIRIVFDPSA-N 0.000 description 1
- XCUCMLUTCAKSOZ-JSOSNVBQSA-N Liensinine Natural products C([C@@H]1C=2C=C(C(=CC=2CCN1C)OC)OC=1C(O)=CC=C(C=1)C[C@@H]1N(C)CCC=2C=C(C(=CC=21)OC)OC)C1=CC=C(O)C=C1 XCUCMLUTCAKSOZ-JSOSNVBQSA-N 0.000 description 1
- YXVXMURDCBMPRH-UHFFFAOYSA-N Lirinidine Natural products C1C2=CC=CC=C2C2=C(O)C(OC)=CC3=C2C1N(C)CC3 YXVXMURDCBMPRH-UHFFFAOYSA-N 0.000 description 1
- MIBATSHDJRIUJK-ROJLCIKYSA-N Neferine Chemical compound C1=CC(OC)=CC=C1C[C@@H]1C2=CC(OC=3C(=CC=C(C[C@@H]4C5=CC(OC)=C(OC)C=C5CCN4C)C=3)O)=C(OC)C=C2CCN1C MIBATSHDJRIUJK-ROJLCIKYSA-N 0.000 description 1
- MIBATSHDJRIUJK-UHFFFAOYSA-N Neferine Natural products C1=CC(OC)=CC=C1CC1C2=CC(OC=3C(=CC=C(CC4C5=CC(OC)=C(OC)C=C5CCN4C)C=3)O)=C(OC)C=C2CCN1C MIBATSHDJRIUJK-UHFFFAOYSA-N 0.000 description 1
- ORJVQPIHKOARKV-UHFFFAOYSA-N Nuciferine Natural products C1C2=CC=CC=C2C2=C(OC)C(OC)=CC3=C2C1N(C)CC3 ORJVQPIHKOARKV-UHFFFAOYSA-N 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 210000003056 antler Anatomy 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- ORJVQPIHKOARKV-OAHLLOKOSA-N nuciferine Chemical compound C1C2=CC=CC=C2C2=C(OC)C(OC)=CC3=C2[C@@H]1N(C)CC3 ORJVQPIHKOARKV-OAHLLOKOSA-N 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229930001545 pronuciferine Natural products 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/62—Nymphaeaceae (Water-lily family)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/02—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Botany (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Alternative & Traditional Medicine (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a method for preparing lotus plumule superfine powder with an airflow superfine grinding technology. According to the method, drying is performed for multiple times, an anti-caking agent is added for multiple times, and the lotus plumule superfine powder is prepared in combination of airflow grinding. The method has the advantages as follows: defects that conventional lotus plumule medicinal composition is difficult to dissolve out, the dosage form is single, the utilization rate is low and the application range is narrow are overcome, full-effect utilization of raw materials is realized, the application range of lotus plumule is enlarged, and defects that conventional superfine powder is prone to moisture absorption, aggregation, caking and the like are overcome. A product has the advantages of small particle size, good dispersibility, low possibility of caking, rich nutrition, large dissolving-out amount of active ingredients such as alkaloid and the like, high bioavailability and the like, and is suitable for being added into high-grade health care products.
Description
Technical field
The present invention relates to a kind of air-flow superfine communication technique and prepare the method for lotus nut Ultramicro-powder, belong to agricultural product, food processing technology field.
Technical background
Lotus nut is green young shoot and the radicle in Nymphaeceae nelumbium lotus seed, mainly originates in the ground such as China Jiangxi, Zhejiang, Hunan, Hubei, Fujian, is conventional Chinese medicine, and traditional medicine thinks that it has the effect of clearing away the heart fire and tranquillizing, restoring normal coordination between heart and kidney, unsmoothing the sperm and stopping bleeding.Two benzyl morphinane alkaloids as liensinine, isoliensinine, neferine, C19H23NO3, Nuciferine, Pronuciferine etc. be the main active ingredient in lotus nut, wherein main in the majority with the content of former three.At present, the edible of lotus nut adopts the mode that hot water boils or hot water steeps to obtain active ingredient mostly, and active ingredient dissolved efficiency is lower.
Superfine communication technique starts from late 1990s in the application of the field of Chinese medicines, has now manifested distinctive advantage and wide application prospect, and it has the following advantages: as high in breaking-wall cell rate, be conducive to the emission and absorption of medicine; Increase drug absorption rate, improve its bioavilability; Reduce dosage, conservation, raises the efficiency, and reduces costs; The homogenising that is conducive to each active ingredient in herbal mixture pulverizing, the action effect of raising medicine; Powder distribution is even, takes mouthfeel good, is easy to moulding, is convenient to the features such as application.Because superfine communication technique has so many advantage, this technology has now applied to ginseng, and pilose antler, in the exploitation of the Chinese medicines such as Radix Angelicae Sinensis.If lotus nut ultramicro grinding is made to Ultramicro-powder, can make the pharmacy composition stripping at faster speed in lotus nut, will more be conducive to the absorption of human body.
Yet, although ultramicro grinding is prepared solubility and dissolution rate that powder can increase medicine, but along with medicament powder specific area increases, surface can make particle surface more easily adsorb moisture and the electric charge in bad border, medicinal powder can become and easily assemble, mobility, dispersed variation, powder is in unsteady state, and this is that restriction superfine communication technique is applied to obtain a large obstacle in Chinese medicine.
Summary of the invention
The object of the present invention is to provide a kind of air-flow superfine communication technique to prepare the method for lotus nut Ultramicro-powder, to solve the easily drawback of caking of conventional Ultramicro-powder.
The method processing step that a kind of air-flow superfine communication technique of the present invention is prepared lotus nut Ultramicro-powder is as follows:
(1) dry for the first time: lotus nut dry 12-24 hour in 60-80 degree baking oven Celsius to be sold in city, be placed in drier standby;
(2) in the material after step (1), add anticaking agent sodium silicoaluminate, addition is 1g/kg material;
(3) coarse crushing: adopt medicinal herb grinder to carry out coarse crushing lotus nut, sieve, get 28-140 object coarse granule;
(4) in the material after step (3), add anticaking agent silica, addition is 10g/kg material;
(5) dry for the second time: corase meal is placed in to the dry 2-3 hour of 60-80 degree baking oven Celsius;
(6) air-flow crushing: carry out air-flow crushing with YQ100 collar plate shape airslide disintegrating mill pulverizing pressure and feed pressure and be respectively under the condition of 70 Psi and 100 Psi;
(7) in the material after step (6), add anticaking agent tricalcium phosphate, addition is 10g/kg material;
(8) dry for the third time: Ultramicro-powder is placed in to the dry 2-3 hour of 60-80 degree baking oven Celsius;
(9) packaging sterilizing.
Beneficial effect of the present invention: utilize impact, shearing, collision, the friction of air-flow lotus nut to be carried out to the effect of ultramicro grinding and modification.By coarse crushing with repeatedly add anticaking agent, repeatedly dry mode has reasonably been controlled granularity and the water content of charging, makes material embrittlement simultaneously, has larger crushing efficiency in air-flow crushing.The invention solves current lotus nut effective component and be difficult to stripping, formulation is single, and utilization rate is low, and the shortcoming that range of application is narrow has realized the full effect utilization of raw material and widened the range of application of lotus nut.More solve the very easily moisture absorption of conventional ultra-micro powder, assembled the shortcomings such as caking.It is little that product has particle diameter, and good dispersion does not lump, nutritious, alkaloid isoreactivity composition stripping quantity is high, bioavilability advantages of higher, is suitable for the interpolation of high-grade health products.
Accompanying drawing explanation
fig. 1 isthe dissolution rate figure of lotus nut in solvent distilled water before and after ultramicro grinding:
fig. 2 isthe dissolution rate figure of lotus nut in solvent absolute ethyl alcohol before and after ultramicro grinding;
fig. 3 isthe dissolution rate figure of lotus nut in solvent simulated gastric fluid before and after ultramicro grinding;
In figure: abscissa is time (min), ordinate is Cumulative release amount (%).
The specific embodiment
(1) dry for the first time: lotus nut to be sold to by city and in 70 degree baking ovens Celsius, be dried 15 hours, be placed in drier standby;
(2) sneak into for the first time anticaking agent: get 10 kg lotus nuts, add wherein 10 g sodium silicoaluminates, mix;
(3) coarse crushing: the lotus nut in step (2) is added in medicinal herb grinder and carries out coarse crushing, sieve, get the coarse granule between 28-140 order;
(4) dry for the second time: corase meal is placed in to 60 degree baking oven Celsius dry 3 hours;
(5) sneak into for the second time anticaking agent: the silica to adding 10 grams/kilogram in corase meal, mixes;
(6) air-flow crushing: carry out air-flow crushing with YQ100 collar plate shape airslide disintegrating mill pulverizing pressure and feed pressure and be respectively under the condition of 70 Psi and 100 Psi;
(7) dry for the third time: Ultramicro-powder is placed in to 80 degree baking oven Celsius dry 2 hours;
(8) sneak into for the third time anticaking agent: the tricalcium phosphate to adding 10 grams/kilogram in Ultramicro-powder, mixes;
(9) packaging sterilizing.After packing, adopt ultra violet lamp half an hour, put into apotheca.
The particle diameter of measuring powder with laser particle analyzer, shows after ultramicro grinding, the particle diameter of lotus nut powder is 4-18 μ m.
Gained powder is measured its powder property with BT-1000 powder bulk properties analyzer, and angle of repose is 60.15
o, decentralization is 16.25%, shows that lotus nut Ultramicro-powder has good dispersiveness.
Claims (1)
1. with air-flow superfine communication technique, prepare a method for lotus nut Ultramicro-powder, it is characterized in that:
(1) dry for the first time: lotus nut dry 12-24 hour in 60-80 degree baking oven Celsius to be sold in city, be placed in drier standby;
(2) in the material after step (1), add anticaking agent sodium silicoaluminate, addition is 1g/kg material;
(3) coarse crushing: adopt medicinal herb grinder to carry out coarse crushing lotus nut, sieve, get 28-140 object coarse granule;
(4) in the material after step (3), add anticaking agent silica, addition is 10g/kg material;
(5) dry for the second time: corase meal is placed in to the dry 2-3 hour of 60-80 degree baking oven Celsius;
(6) air-flow crushing: carry out air-flow crushing with YQ100 collar plate shape airslide disintegrating mill pulverizing pressure and feed pressure and be respectively under the condition of 70 Psi and 100 Psi;
(7) in the material after step (6), add anticaking agent tricalcium phosphate, addition is 10g/kg material;
(8) dry for the third time: Ultramicro-powder is placed in to the dry 2-3 hour of 60-80 degree baking oven Celsius;
(9) packaging sterilizing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310615488.4A CN103652868A (en) | 2013-11-28 | 2013-11-28 | Method for preparing lotus plumule superfine powder with airflow superfine grinding technology |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310615488.4A CN103652868A (en) | 2013-11-28 | 2013-11-28 | Method for preparing lotus plumule superfine powder with airflow superfine grinding technology |
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|---|---|
| CN103652868A true CN103652868A (en) | 2014-03-26 |
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| CN201310615488.4A Pending CN103652868A (en) | 2013-11-28 | 2013-11-28 | Method for preparing lotus plumule superfine powder with airflow superfine grinding technology |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108210465A (en) * | 2016-12-14 | 2018-06-29 | 河南后羿实业集团有限公司 | Anti-caking compound carbasalate calcium pulvis and preparation method thereof |
| CN114392286A (en) * | 2021-12-21 | 2022-04-26 | 河北万邦复临药业有限公司 | Preparation method of omphalia powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108210465A (en) * | 2016-12-14 | 2018-06-29 | 河南后羿实业集团有限公司 | Anti-caking compound carbasalate calcium pulvis and preparation method thereof |
| CN114392286A (en) * | 2021-12-21 | 2022-04-26 | 河北万邦复临药业有限公司 | Preparation method of omphalia powder |
| CN114392286B (en) * | 2021-12-21 | 2023-03-07 | 河北万邦复临药业有限公司 | Preparation method of omphalia powder |
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Application publication date: 20140326 |