CN103651968A - Giant salamander and perilla blend oil and preparation method thereof - Google Patents
Giant salamander and perilla blend oil and preparation method thereof Download PDFInfo
- Publication number
- CN103651968A CN103651968A CN201310614189.9A CN201310614189A CN103651968A CN 103651968 A CN103651968 A CN 103651968A CN 201310614189 A CN201310614189 A CN 201310614189A CN 103651968 A CN103651968 A CN 103651968A
- Authority
- CN
- China
- Prior art keywords
- oil
- giant salamander
- acid
- perilla
- ready
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention provides giant salamander and perilla blend oil comprising effective components in percentage by weight as follows: 5%-10% of eicosapentaenoic acid, 0.5%-5.0% of docosahexaenoic acid, 10%-30% of oleic acid, 20%-30% of linoleic acid and 5%-10% of linolenic acid. The preparation method comprises the steps as follows: feeding hot steam into giant salamander adipose tissues for heating, and squeezing, filtering and centrifuging the adipose tissues to obtain crude giant salamander oil; heating the crude giant salamander oil to the temperature of 50-70 DEG C and adding a phosphoric acid solution for acid refining; heating the raw giant salamander oil material obtained through acid refining to the temperature of 50-95 DEG C, adding a caustic soda solution, and standing the mixture for 10-30 min; and adding active carbon at the normal temperature, stirring the mixture for 10-60 min for decolorization and deodorization, centrifuging and filtering the mixture to obtain an oil supernatant, cooling the oil supernatant to obtain the giant salamander oil, and mixing the giant salamander oil, perilla oil and vitamin E to obtain the giant salamander and perilla blend oil product. The obtained oil is balanced in fatty acid composition proportion and rich in alpha-linolenic acid and has beautifying and health-care effects, such as blood vessel softening, blood lipid reduction and the like if the oil is often eaten.
Description
Technical field
The present invention relates to edible oil processing technique field, specifically, be to provide a kind of giant salamander purple perilla ready-mixed oil and preparation method thereof.
Background technology
Chinese giant salamander, Andrias davidianus (Andrias davidianus), is the rare famous and expensive special local product of China, is commonly called as " giant salamander ".It is existing individual maximum amphibian, has the title of living nature living fossil, belongs to Amphibia (amphibian), Caudata (Caudata), Cryptobranchidae (Crytobranchidae) on taxology.Giant salamander has higher nutrition and medical value, is paid close attention to by people always.The skin of giant salamander, muscle, internal organs, bone and secretion thereof all can be used as medicine, and the fat of giant salamander contains multiple unrighted acid, and giant salamander grease can be used as and regulates blood fat, avoids atherosclerotic edible good merchantable brand.Purple Perilla Seed Oil is a kind of natural oil of high degree of unsaturation, and contained Main Ingredients and Appearance is alpha-linolenic acid, and content, up to 50%-70%, is that in all crude vegetals of finding at present, this content of fatty acid is the highest.To reducing the dauer effect that has of cholesterol, reduction blood fat, atherosclerosis, reduction cerebral thrombus and angiocardiopathy.Alpha-linolenic acid can change into 20 carbon 5 olefin(e) acids (EPA) and 22 carbon 6 olefin(e) acids (DHA) after taking in human body under the effect of enzyme in human body, it is exactly the Main Ingredients and Appearance of deep sea fish oil, therefore be again plant deep sea fish oil, than deep sea fish oil, be more preferably it not containing cholesterol, the effect that EPA and DHA have reducing blood lipid and improve memory.
At present, the deep processed product that existing beauty treatment on market, health care, the giant salamander such as medicinal and purple perilla are developed is respectively sold, and the health-care efficacy of giant salamander and purple perilla also more report, yet yet there are no the product of two kinds of joint developments.This product is well combined high-grade animal oil with vegetable oil, can effectively regulate blood fat, has wide market prospects.
Summary of the invention
The object of the present invention is to provide a kind of giant salamander purple perilla ready-mixed oil and preparation method thereof.
A kind of giant salamander purple perilla ready-mixed oil provided by the invention, it is characterized in that, by giant salamander oil and perilla herb oil, be in harmonious proportion and form, its acidity 0.1-2.5%, peroxide value is 1.0-15.0 meq/kg, the active ingredient that contains following percentage by weight: eicosapentaenoic acid 5%-10%, DHA 0.5%-5.0%, oleic acid 10%-30%, linoleic acid 20%-30%, leukotrienes 5%-10%.
Optimize, in giant salamander purple perilla ready-mixed oil, be also added with vitamin E, the weight proportion of giant salamander oil, perilla herb oil and vitamin E is 30-70:25-69:1-5.
Further optimize, the weight proportion of giant salamander oil, perilla herb oil and vitamin E is 60:40:2.
The preparation method of giant salamander purple perilla ready-mixed oil provided by the invention, comprises the following steps:
(1) get the adipose tissue in giant salamander body, put in stainless steel jacketed pan, pass into heat steam, heat 90-100 ℃ of about 1-2 hour, then push, resulting fluid filtration, centrifugal, obtain slightly oil of giant salamander;
(2) the thick oil of giant salamander is heated to 50-70 ℃, adds phosphoric acid solution to enter after sufficiently mixing acid refining retort, stop after 10-30 minute, standing, standby;
(3) by step (2) gained giant salamander oil heating raw materials to 50-95 ℃, add soda bath, mix, stop after 10-30 minute, standing, standby;
(4) by step (3) gained giant salamander oil raw material, add at normal temperatures active carbon, stir 10-60 minute, decolouring, deodorizing, centrifugal, filter and remove residue, obtains supernatant fluid;
(5) supernatant fluid is slowly stirred, control cooling velocity, be cooled to 0～10 ℃ of left and right, be 12-48 hour cool time, obtains giant salamander oil;
(6) get purple perilla seed, decortication, adopts low-temperature physics squeezing, then through membrane filtration, decolour with active carbon, obtains perilla herb oil;
(7) the giant salamander oil of 30-70 weight portion, the perilla herb oil of 25-69 part weight portion are mixed with the vitamin E of 1-5 weight portion, 200-500 rpm is stirred 1-6 hour.
In step (2), the concentration of described phosphoric acid solution is 60-90 %, and addition is the 0.1-1.0% of the thick weight of oil of giant salamander.
In step (3), the concentration of described soda bath is 10-40%, and addition is the 0.1-2.0% of step (2) gained giant salamander oil raw material weight.
In step (4), the addition of active carbon is the 1-20% of step (3) gained giant salamander oil raw material weight.
Giant salamander purple perilla ready-mixed oil prepared by said method, its acidity 0.1-2.5%, peroxide value is 1.0-15.0 meq/kg, the active ingredient that contains following percentage by weight: eicosapentaenoic acid 5%-10%, DHA 0.5%-5.0%, oleic acid 10%-30%, linoleic acid 20%-30%, leukotrienes 5%-10%.
The present invention obtains a kind of giant salamander edible oil, for the exploitation of giant salamander grease provide a kind of feasibility mode, its preparation method has retained the active ingredient in giant salamander oil to greatest extent, the product fatty acid oil proportion of composing obtaining is balanced, and be rich in the health care that alpha-linolenic acid has softening blood vessel, reduces blood fat, often eat and there is various health care functions and beauty functions.
The specific embodiment
Get the adipose tissue in giant salamander body, get the adipose tissue in giant salamander body, clean up, put in stainless steel jacketed pan, pass into heat steam, heat 90-100 ℃ of about 1-2 hour, then push, resulting fluid filter, remove slag, centrifugal, get supernatant fluid, obtain slightly oil of giant salamander; The thick oil of giant salamander is heated to 50-70 ℃, adds the phosphoric acid that oily heavily 0.1-1.0%, concentration are 60-90 % to enter after sufficiently mixing acid refining retort, stop after 10-30 minute, standing, standby; By standby giant salamander oil heating raw materials, to 50-95 ℃, adding the heavy 0.1-2.0% of oil, adding concentration is 10-40% soda bath, stops after 10-30 minute, standing, standby; By standby giant salamander oil raw material at normal temperatures, adding mass ratio is the active carbon of 100:1-100:20, stirs 10-60 minute, decolouring, deodorizing, and centrifugal, filter and remove residue, obtains supernatant fluid.Supernatant fluid is slowly stirred, control cooling velocity, be cooled to 0～10 ℃ of left and right, be 12-48 hour cool time, and purity is 95%, standby; Get purple perilla seed, decortication, adopts low-temperature physics squeezing, then through membrane filtration, decolour with active carbon, obtains perilla herb oil, and purity is 95%, standby.The standby giant salamander oil material liquid of 50 weight portions is mixed with the perilla herb oil of 45 weight portions and the vitamin E of 5 weight portions, and 200 rpms are stirred 2 hours, and bottling, obtains product.
After testing, the purple perilla ready-mixed oil that said method makes, its acidity 0.1-2.5%, peroxide value is 1.0-15.0 meq/kg, the active ingredient that contains following percentage by weight: eicosapentaenoic acid 5%-10%, DHA 0.5%-5.0%, oleic acid 10%-30%, linoleic acid 20%-30%, leukotrienes 5%-10%.
Claims (7)
1. a giant salamander purple perilla ready-mixed oil, it is characterized in that, by giant salamander oil and perilla herb oil, be in harmonious proportion and form, its acidity 0.1-2.5%, peroxide value is 1.0-15.0 meq/kg, the active ingredient that contains following percentage by weight: eicosapentaenoic acid 5%-10%, DHA 0.5%-5.0%, oleic acid 10%-30%, linoleic acid 20%-30%, leukotrienes 5%-10%.
2. giant salamander purple perilla ready-mixed oil according to claim 1, is characterized in that, in giant salamander purple perilla ready-mixed oil, is also added with vitamin E, and the weight proportion of giant salamander oil, perilla herb oil and vitamin E is 30-70:25-69:1-5.
3. giant salamander purple perilla ready-mixed oil according to claim 1, is characterized in that, the weight proportion of giant salamander oil, perilla herb oil and vitamin E is 60:40:2.
4. a preparation method for giant salamander giant salamander purple perilla ready-mixed oil as claimed in claim 1, is characterized in that, comprises the following steps:
(1) get the adipose tissue in giant salamander body, put in stainless steel jacketed pan, pass into heat steam, heat 90-100 ℃ of about 1-2 hour, then push, resulting fluid filtration, centrifugal, obtain slightly oil of giant salamander;
(2) the thick oil of giant salamander is heated to 50-70 ℃, adds phosphoric acid solution to enter after sufficiently mixing acid refining retort, stop after 10-30 minute, standing, standby;
(3) by step (2) gained giant salamander oil heating raw materials to 50-95 ℃, add soda bath, mix, stop after 10-30 minute, standing, standby;
(4) by step (3) gained giant salamander oil raw material, add at normal temperatures active carbon, stir 10-60 minute, decolouring, deodorizing, centrifugal, filter and remove residue, obtains supernatant fluid;
(5) supernatant fluid is slowly stirred, control cooling velocity, be cooled to 0～10 ℃ of left and right, be 12-48 hour cool time, obtains giant salamander oil;
(6) get purple perilla seed, decortication, adopts low-temperature physics squeezing, then through membrane filtration, decolour with active carbon, obtains perilla herb oil;
(7) the giant salamander oil of 30-70 weight portion, the purple perilla E of 25-69 part weight portion are mixed, 200-500 rpm is stirred 1-6 hour.
5. the preparation method of giant salamander giant salamander purple perilla ready-mixed oil according to claim 2, is characterized in that, in step (2), the concentration of described phosphoric acid solution is 60-90 %, and addition is the 0.1-1.0% of the thick weight of oil of giant salamander.
6. the preparation method of giant salamander giant salamander purple perilla ready-mixed oil according to claim 2, is characterized in that, in step (3), the concentration of described soda bath is 10-40%, and addition is the 0.1-2.0% of step (2) gained giant salamander oil raw material weight.
7. the preparation method of giant salamander giant salamander purple perilla ready-mixed oil according to claim 2, is characterized in that, in step (4), the addition of active carbon is the 1-20% of step (3) gained giant salamander oil raw material weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310614189.9A CN103651968B (en) | 2013-11-28 | 2013-11-28 | A kind of giant salamander purple perilla ready-mixed oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310614189.9A CN103651968B (en) | 2013-11-28 | 2013-11-28 | A kind of giant salamander purple perilla ready-mixed oil and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103651968A true CN103651968A (en) | 2014-03-26 |
| CN103651968B CN103651968B (en) | 2015-08-12 |
Family
ID=50291685
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310614189.9A Active CN103651968B (en) | 2013-11-28 | 2013-11-28 | A kind of giant salamander purple perilla ready-mixed oil and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103651968B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105124566A (en) * | 2015-06-09 | 2015-12-09 | 汉中领维生物科技发展有限公司 | Preparation and health-care effects of soft capsules of mixture of giant salamander oil, eucommia seed oil, red kojic rice and hawthorn fruit extract and black tea extract |
| CN110916196A (en) * | 2019-12-11 | 2020-03-27 | 付俊 | Giant salamander protein peptide soft capsule and preparation method thereof |
| CN112869149A (en) * | 2021-01-28 | 2021-06-01 | 付俊 | Health-care capsule for softening blood vessels and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1919233A (en) * | 2006-08-29 | 2007-02-28 | 李富民 | Nourishing and health care capsule with intelligence development and memory improvement function and method for making same |
| CN101721432A (en) * | 2009-12-10 | 2010-06-09 | 张家界金鲵生物科技有限公司 | Giant salamander oil soft capsule, method for preparing same and use thereof |
| CN102488718A (en) * | 2011-12-27 | 2012-06-13 | 深圳市麦金利实业有限公司 | Fish oil soft capsule and its preparation method |
| CN102925279A (en) * | 2012-11-13 | 2013-02-13 | 湖北金鲤鱼食品有限公司 | Technology of extracting and refining fish oil from internal organs of silver carps |
-
2013
- 2013-11-28 CN CN201310614189.9A patent/CN103651968B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1919233A (en) * | 2006-08-29 | 2007-02-28 | 李富民 | Nourishing and health care capsule with intelligence development and memory improvement function and method for making same |
| CN101721432A (en) * | 2009-12-10 | 2010-06-09 | 张家界金鲵生物科技有限公司 | Giant salamander oil soft capsule, method for preparing same and use thereof |
| CN102488718A (en) * | 2011-12-27 | 2012-06-13 | 深圳市麦金利实业有限公司 | Fish oil soft capsule and its preparation method |
| CN102925279A (en) * | 2012-11-13 | 2013-02-13 | 湖北金鲤鱼食品有限公司 | Technology of extracting and refining fish oil from internal organs of silver carps |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105124566A (en) * | 2015-06-09 | 2015-12-09 | 汉中领维生物科技发展有限公司 | Preparation and health-care effects of soft capsules of mixture of giant salamander oil, eucommia seed oil, red kojic rice and hawthorn fruit extract and black tea extract |
| CN110916196A (en) * | 2019-12-11 | 2020-03-27 | 付俊 | Giant salamander protein peptide soft capsule and preparation method thereof |
| CN112869149A (en) * | 2021-01-28 | 2021-06-01 | 付俊 | Health-care capsule for softening blood vessels and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103651968B (en) | 2015-08-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104432059B (en) | A kind of anti-acid microalgae DHA grease microscapsule powder | |
| CN103125802B (en) | Nutrition taking propolis cream, medlar cream, honey and desert ginseng powder as raw materials and preparation method of nutrition | |
| CN106490189B (en) | A kind of margarine and preparation method thereof | |
| CN103666742A (en) | Extraction method of giant salamander oil and giant salamander oil product | |
| CN101843336A (en) | Linseed oil fat emulsion oral solution, beverage and manufacturing method thereof | |
| CN104840612A (en) | Low-sugar tea oil emulsion | |
| CN104673490B (en) | The method of refining of rice bran oil | |
| CN103651968B (en) | A kind of giant salamander purple perilla ready-mixed oil and preparation method thereof | |
| CN103651942A (en) | Preparation methods of natural plant dilute cream, animal and plant dilute cream and degreased plant protein powder | |
| CN101816423A (en) | Purple perilla seed oil lipid emulsion oral solution, beverage and manufacturing method thereof | |
| CN108094575A (en) | A kind of edible oil containing peony seed oil and preparation method thereof | |
| CN104127857A (en) | Fish oil soft capsule and preparation method thereof | |
| CN103689135A (en) | Omega-3 unsaturated fatty acid-rich blend oil | |
| CN109362897A (en) | A kind of prandial oil and preparation method thereof | |
| CN105124566A (en) | Preparation and health-care effects of soft capsules of mixture of giant salamander oil, eucommia seed oil, red kojic rice and hawthorn fruit extract and black tea extract | |
| CN105030832A (en) | Preparing method for white emulsification odor type alligator oil | |
| CN105147762A (en) | Soybean oil emulsion | |
| CN109077127A (en) | A kind of nutrition oil and preparation method thereof rich in nervonic acid and alpha-linolenic acid | |
| CN101869297A (en) | Compound evening primrose and perilla herb oil fat emulsion oral solution, beverage and preparation method | |
| KR20100032776A (en) | The development of tofu coagulant using natural magnesium chloride and tofu manufacturing method | |
| Lee | Essent ial Fat ty Acids | |
| CN107183219A (en) | A kind of low temperature nutrient blend oil and preparation method thereof | |
| TW201234975A (en) | Oil-and-fat composition for processed food of fishery product and processed food of fishery product using the same | |
| CN105901170A (en) | Stomach-strengthening antioxidant sesame oil and a preparing method thereof | |
| CN101869298A (en) | Compound walnut and linseed oil fat emulsion oral solution, beverage and preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP02 | Change in the address of a patent holder |
Address after: 427100 he Qun Cun, Bai nationality township, Furong Qiao, Sangzhi County, Zhangjiajie City, Hunan Province Patentee after: ZHANGJIAJIE JINNI BIOTECHNOLOGY Co.,Ltd. Address before: 427000 Zhangjiajie province Hunan city Yongding District Nanzhuang Ping Dayong Road No. 99 Zhangjiajie jinni International Hotel Patentee before: ZHANGJIAJIE JINNI BIOTECHNOLOGY Co.,Ltd. |
|
| CP02 | Change in the address of a patent holder |