CN101869298A - Compound walnut and linseed oil fat emulsion oral solution, beverage and preparation method - Google Patents
Compound walnut and linseed oil fat emulsion oral solution, beverage and preparation method Download PDFInfo
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- CN101869298A CN101869298A CN201010197199A CN201010197199A CN101869298A CN 101869298 A CN101869298 A CN 101869298A CN 201010197199 A CN201010197199 A CN 201010197199A CN 201010197199 A CN201010197199 A CN 201010197199A CN 101869298 A CN101869298 A CN 101869298A
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Abstract
The invention relates to a compound walnut and linseed oil fat emulsion oral solution, beverage and a preparation method. The oral solution comprises raw materials of walnut oil, linseed oil, lecithin, glycerin, sterile pure water, an antioxidant, a stabilizing agent, a pH regulating agent, a flavoring agent, essence, and the like. The preparation process comprises the following steps of: in the presence of the protection of nitrogen, heating, dissolving and mixing the walnut oil, the linseed oil and the lecithin into an oil phase; mixing the glycerin, the antioxidant, the stabilizing agent, the flavoring agent, the essence and the sterile pure water into a water phase; slowly adding the oil phase into the strongly stirred water phase and shearing into a primary emulsion at high speed; regulating the pH value of the primary emulsion to be 6.5-8.5 by using a few of pH regulating agent; emulsifying by using a high-pressure homogenizer; filtering by using a microporous membrane; and filling, sealing and sterilizing to obtain the oral solution with the oil content of 1-50 percent. The compound walnut and linseed oil fat emulsion oral solution is used in the field of healthy food, 5-50 percent of the fat emulsion oral solutions can be used as nutritional functional health-care beverages, and 1-20 percent of the fat emulsion oral solutions can be used as table beverages and popular beverages.
Description
Technical field
The invention belongs to the healthy food field, relate to a kind of compound walnut and linseed oil fat emulsion oral solution, beverage and manufacture method, this invention is by walnut oil, linseed oil, emulsifying agent, sterile pure water after emulsification, makes oil droplet size less than below 800 nanoscales, form chylomicron, oral back enters blood circulation, directly by body or cell institute digestibility and utilization in the easier absorption of intestines and stomach.
The fat emulsion oral solution of 5-50% high concentration is as trophism functional health drink, and the fat emulsion oral solution of 1-20% low concentration is as dining table beverage and popular drink.
This compound walnut and linseed oil fat emulsion oral solution, beverage contain ω-6 polyunsaturated fatty acid and ω-3 polyunsaturated fatty acid of high-load simultaneously, be used for pregnant woman, infant, children, student, a middle-aged person, the elderly, provide with added body in multiple essential fatty acid;
Compound walnut and linseed oil fat emulsion oral solution, the research and development of beverage and production for directly drinking simultaneously walnut oil and linseed oil, replenish ω-6 and ω-3 essential fatty acid comprehensively, and a reliable and effective method and approach are provided.
Background technology
World-renowned nutritionist, doctor Xi Mopulesi are according to pointing out in " the Europe miaow gal health " book to the upright work in investigation back, seven continents, the world, when the ratio of essential fatty acid ω-3 and ω in the human body-6 in 1: 4, extraneous disease is difficult to invade human body, and human body just is in absolute health status.
In our daily edible soya-bean oil, peanut oil, rapeseed oil, the corn wet goods vegetable oil, be rich in the serial linoleic acid of ω-6 in institute's pufa-containing, and the linolenic acid content of ω-3 series is lower, the ratio 1 of its ω-3 and ω-6: 20-30.Daily edible above-mentioned vegetable oil, additional is a large amount of serial linoleic acid of ω-6, the leukotrienes of ω-3 series is few; Long-term ω-3 or ω-6 series fatty acid of replenishing can cause that all ω-3 and ω-6 fatty acid proportion in the body is unbalance singlely, and people's health just is subject to the attack of numerous disease, causes relevant disease to take place.
Walnut oil (Walnut oil) is the seed walnut of Juglandaceae Juglans plant walnut (Juglans regia L.), shells and presses or the refining oily liquids that forms of hot pressing press for extracting juice extraction through colding pressing.
Contain amounts of protein and fat in the walnut kernel, its vegetalitas unsaturated fatty acid content 〉=85%, ω-6 linoleic acid and ω-3 linolenic acid content 〉=71%, its main component is ω-6 linoleic acid, content is up to more than 63%.
Linseed oil (Flaxseed oil) is seed-linseed of flax family (Linaceae) plant flax (Linum usitatissimum L.), and cold press or hot moulding are produced, and gets linseed oil through making with extra care.
Contain amounts of protein and fat in the linseed, its vegetalitas unsaturated fatty acid content 〉=90%, ω-6 linoleic acid and ω-3 linolenic acid content 〉=70%, alpha-linolenic acid is up to 60%, in common vegetable oil, the alpha-linolenic acid content ratio in the linseed is higher.
Walnut oil, linseed oil and edible oil component commonly used contrast
Often take certain proportion miscella with walnut oil and linseed oil preparation; can complementary single deficiency of taking; replenish ω-3 and the serial polyunsaturated fatty acid of ω-6 all sidedly; what help body absorbs multiple essential fatty acid fully; impel ω-3 and ω-6 fatty acid proportion trend normalization in the control agent; prevent and prevent the body fat metabolic disorder; cause body biochemical metabolism confusion not normal; cause the generation of metabolic disease; the generation that gives rise to diseases is as obesity; hypertension; high fat of blood; diabetes; coronary heart disease; multiple disease such as artery sclerosis and cardiovascular and cerebrovascular.
Its main component is the serial polyunsaturated fatty acid-linoleic acid of ω-6 in the walnut oil, and content is up to more than 63%.Be rich in the serial polyunsaturated fatty acid of ω-3 in the linseed oil, Main Ingredients and Appearance is an alpha-linolenic acid, and linoleic acid plus linolenic acid all belongs to essential fatty acid, can't transform synthetic, necessary additional by taking in absorption in the food at human body self.
On the domestic market walnut oil, the single crude oil products of linseed oil and soft capsule are arranged at present, the compound product that does not have walnut oil and linseed oil miscella, single routinely walnut oil and the linseed oil taken can not replenish ω-3 and the serial polyunsaturated fatty acid of ω-6 easily comprehensively.
Direct oral walnut oil and linseed oil are difficult for absorbing, or absorb not exclusively, take linseed oil in a large number or for a long time and can cause the diarrhoea side effect.
For this reason, this invention is that walnut oil and linseed oil mix by required proportioning, after emulsification, particle diameter reaches below 800 nanoscales, forms chylomicron, makes compound walnut and linseed oil fat emulsion, oral back enters blood circulation, directly by body or cell institute digestibility and utilization in the easier absorption of intestines and stomach.
Compound walnut and linseed oil fat emulsion oral solution, the research and development of beverage and production are simultaneously direct edible walnut oil, linseed oil, replenish ω-3 and the serial multiple essential fatty acid of ω-6 comprehensively, and a reliable and effective method and approach are provided.
Summary of the invention
The object of the invention provides a kind of compound walnut and linseed oil fat emulsion oral solution, beverage and manufacture method.
Walnut oil (Walnut oil) is the seed walnut of Juglandaceae Juglans plant walnut (Juglans regia L.), shells and presses or the refining oily liquids that forms of hot pressing press for extracting juice extraction through colding pressing.
Linseed oil (Flaxseed oil) is seed-linseed of flax family (Linaceae) plant flax (Linum usitatissimum L.), and cold press or hot moulding are produced, through the refining oily liquids that forms.
Compound walnut and linseed oil fat emulsion oral solution, beverage formula are: every 1000ml fat breast contains refining walnut oil and the total oil mass 1-50% of linseed oil, emulsion 1.0-15.0%, isotonic regulator 1.0-5.0%, antioxidant 0.01-0.5%, stabilizing agent 0.1-10%, it is 6.5-8.5 that flavor enhancement 0.01-10%, pH conditioning agent are transferred fat emulsion pH, and all the other are sterile pure water.
Compound walnut and linseed oil fat emulsion oral solution, drink and production process flow process are:
A) under nitrogen protection, will make with extra care walnut oil, linseed oil mixing, be heated to 70-90 ℃, stir the adding emulsifying agent and form oil phase liquid until dissolving;
B) with glycerine, antioxidant, stabilizing agent, flavor enhancement, join in the sterile pure water, stirring and dissolving forms water liquid;
C) under nitrogen protection, in the intensively stirred water liquid of the slow adding of oil phase liquid, strong agitation forms colostric fluid;
D), regulate the pH to 6.5-8.5 of colostric fluid with a spot of pH conditioning agent;
E) use high pressure homogenizer under the pressure of 500-25000psi, with colostrum emulsifying repeatedly, the granularity of prepared fat breast is less than 2 microns, and its average particle size range is the 20-800 nanometer;
F) with the filtration sterilization of the process of the fats emulsion behind homogeneous 0.22-0.8 micron microporous membrane filters, under aseptic GMP clean environment, quantitatively pour in the packing container (the glass bottle, mould bottle, PVC bag, non-PVC bag, mould packaging paper product and metal can packing), seal behind the inflated with nitrogen;
G) the fats emulsion goods with package encapsulation place microwave bacteria degermer sterilization or heat sterilization.
The specific embodiment
Below the present invention is described, but the present invention is limited in the example not exclusively by concrete case study on implementation.
Embodiment one,
Prescription: refining walnut oil 30g, linseed oil 20g, edible lecithin 3g, edible glycerol 6g, stabilizing agent is an amount of, sweetener is an amount of, flavoring essence is an amount of, and the NaOH thin liquid is an amount of, and sterile pure water adds to 1000ml.
1, preparation oil phase liquid: get edible refining walnut oil, linseed oil, the edible lecithin of formula ratio, under nitrogen protection, be heated to 80 ℃ of stirrings and make that to be dissolved into oil phase liquid standby;
2, preparation water liquid: it is standby that edible glycerol, stabilizing agent, sweetener, flavoring essence and the sterile pure water of getting formula ratio is stirred into water liquid;
3, first emulsion: under nitrogen protection, under water liquid high-speed stirred, lentamente oil phase liquid is splashed into water liquid, after dripping off, use the high speed shear agitator, first emulsification 15 minutes;
4, regulate pH: under agitation, transfer pH7.4, and add sterile pure water to the full dose of filling a prescription with dilute sodium hydroxide water liquid;
5, emulsifying: utilize the high pressure homogenization machine with colostric fluid homogeneous repeatedly, adjusting pressure is 15000psi, and homogeneous 3-6 time is in the 100-400nm scope up to the newborn particle diameter of fat;
6, filter can: fats emulsion behind the filtering with microporous membrane in 0.8 μ m aperture, is poured into 600ml and moulds in the bottle, fill nitrogen, sealing;
7, sterilization: place the rotary steam Sterilization Kettle to sterilize the fats emulsion of filling and sealing, sterilized F0 value 15 minutes 30 minutes for 115 ℃.Promptly get finally 5% compound walnut and linseed oil fat emulsion oral beverage products.
Embodiment two,
Prescription: refining walnut oil 100g, linseed oil 200g, edible lecithin 18g, edible glycerol 30g, stabilizing agent is an amount of, sweetener is an amount of, essence is an amount of, and the NaOH thin liquid is an amount of, and sterile pure water adds to 1000ml.
1, preparation oil phase liquid: get edible refining walnut oil, linseed oil, the edible lecithin of formula ratio, under nitrogen protection, be heated to 80 ℃ of stirrings and make that to be dissolved into oil phase liquid standby;
2, preparation water liquid: it is standby that edible glycerol, stabilizing agent and the sterile pure water of getting formula ratio is stirred into water liquid;
3, first emulsion: under nitrogen protection, under water liquid high-speed stirred, lentamente oil phase liquid is splashed into water liquid, after dripping off, use the high speed shear agitator, first emulsification 15 minutes;
4, regulate pH: under agitation, transfer pH7.4, add sweetener, flavoring essence, and add sterile pure water to the full dose of filling a prescription with dilute sodium hydroxide water liquid;
5, emulsifying: utilize the high pressure homogenization machine with colostric fluid homogeneous repeatedly, adjusting pressure is 15000psi, and homogeneous 3-6 time is in the 100-400nm scope up to the newborn particle diameter of fat;
6, filter can: fats emulsion behind the filtering with microporous membrane in 0.8 μ m aperture, is poured in the 10ml glass bottle nitrogen-filled seal;
7, sterilization: the fats emulsion of filling and sealing is placed the microwave bacteria degermer sterilization, promptly get finally 30% compound walnut and linseed oil fat emulsion oral solution, as trophism functional health drink.
Embodiment three,
Prescription: refining walnut oil 50g, linseed oil 50g, edible lecithin 6g, edible glycerol 12g, stabilizing agent is an amount of, sweetener is an amount of, essence is an amount of, and the NaOH thin liquid is an amount of, and sterile pure water adds to 1000ml.
1, preparation oil phase liquid: get edible refining walnut oil, linseed oil, the edible lecithin of formula ratio, under nitrogen protection, be heated to 80 ℃ of stirrings and make that to be dissolved into oil phase liquid standby;
2, preparation water liquid: it is standby that edible glycerol, stabilizing agent, sweetener, flavoring essence and the sterile pure water of getting formula ratio is stirred into water liquid;
3, first emulsion: under nitrogen protection, under water liquid high-speed stirred, lentamente oil phase liquid is splashed into water liquid, after dripping off, use the high speed shear agitator, first emulsification 15 minutes;
4, regulate pH: under agitation, transfer pH7.4, and add sterile pure water to the full dose of filling a prescription with dilute sodium hydroxide water liquid;
5, emulsifying: utilize the high pressure homogenization machine with colostric fluid homogeneous repeatedly, adjusting pressure is 15000psi, and homogeneous 3-6 time is in the 100-400nm scope up to the newborn particle diameter of fat;
6, filter can: fats emulsion behind the filtering with microporous membrane in 0.8 μ m aperture, is poured in the 240ml metal can, fill nitrogen, sealing;
7, sterilization: place the rotary steam Sterilization Kettle to sterilize the fats emulsion of filling and sealing, sterilized F0 value 15 minutes 30 minutes for 115 ℃.Promptly get finally 10% compound walnut and linseed oil fat emulsion oral beverage products.
Claims (10)
1. compound walnut and linseed oil fat emulsion oral solution, beverage, it is characterized in that this prescription is: every 1000ml compound walnut and linseed oil fat emulsion oral solution contains refining walnut oil and the total oil mass 1-50% of linseed oil, emulsifying agent 1.0-15.0%, isotonic regulator 1.0-5.0%, antioxidant 0.01-0.5%, stabilizing agent 0.1-10%, flavor enhancement 0.01-10%, pH conditioning agent are transferred fats emulsion pH to 6.5-8.5, and all the other are sterile pure water.
2. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage, it is characterized in that (1) described refining walnut oil (Walnut oil) is the seed walnut of Juglandaceae Juglans plant walnut (Juglans regia L.), shell and press or the refining oily liquids that forms of hot pressing press for extracting juice extraction through colding pressing;
(2) described refining linseed oil (Flaxseed oil) is the seed flax seed of flax family (Linaceae) plant flax (Linum usitatissimum L.), presses through colding pressing or the refining oily liquids that forms of hot pressing press for extracting juice extraction;
(3) walnut oil and linseed oil proportioning are: walnut oil: linseed oil=1: 1～99; Or walnut oil: linseed oil=1～99: 1.
3. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage is characterized in that described emulsifying agent is a kind of or several in refined lecithin, soybean lecithin, egg yolk lecithin, poloxamer, polyethylene glycol glycerol ester, the polyoxyethylene methyl castor oil ether.
4. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage is characterized in that described isotonic regulator is a kind of or several in glycerine, sorbierite, the sweet dew alcohol and glucose.
5. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage is characterized in that described antioxidant is one or more in vitamin E, vitamin C, sodium hydrogensulfite, the natrium adetate.
6. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage is characterized in that described stabilizing agent is one or more in hydroxy propyl-Beta-cyclodextrine, polyethylene glycol, polyvinylpyrrolidone, hydroxypropyl methylcellulose, the oligomeric generation hydroxypropyl cellulose.
7. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage, it is characterized in that described pH conditioning agent is one or more mixing materials in hydrochloric acid, NaOH, phosphoric acid, phosphate, citric acid, citrate, acetic acid, the acetate, regulate walnut oil fat emulsion oral solution pH scope at 6.5-8.5.
8. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage, it is characterized in that described flavor enhancement is sodium chloride, wood sugar, lactose, fructose, sucrose, one or more in the flavor enhancements such as A Siba is sweet, Sucralose, honey element, flavoring orange essence, lemon extract, strawberry essence, lychee flavor, fragrant burnt odor essence, flavoring pineapple essence.
9. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage is characterized in that described preparation technology is:
A) under nitrogen protection, will make with extra care walnut oil and linseed oil and mix, be heated to 60-90 ℃, stir the adding emulsifying agent and form oil phase liquid until dissolving;
B) glycerine, antioxidant, stabilizing agent, flavor enhancement are joined in the sterile pure water, stirring and dissolving forms water liquid;
C) under nitrogen protection, in the intensively stirred water liquid of the slow adding of oil phase liquid, strong agitation forms colostric fluid;
D), regulate the pH to 6.5-8.5 of colostric fluid with a spot of pH conditioning agent;
E) use high pressure homogenizer under the pressure of 500-25000psi, with colostrum emulsifying repeatedly, the granularity of prepared fats emulsion is less than 2 microns, and its average particle size range is the 20-500 nanometer;
F) with the filtration sterilization of the process of the fats emulsion behind homogeneous 0.22-0.8 micron microporous membrane filters, in aseptic GMP clean environment, quantitatively pour in the packing container (the glass bottle, mould bottle, PVC bag, non-PVC bag, mould packaging paper product and metal can packing), seal behind the inflated with nitrogen;
G) the fats emulsion goods with package encapsulation place microwave bacteria degermer sterilization, heat sterilization.
10. compound walnut and linseed oil fat emulsion oral solution according to claim 1, beverage, it is characterized in that being applied to the healthy food field, make the compound walnut and linseed oil fat emulsion oral solution of high concentration, containing the total oil mass of walnut oil and linseed oil is 5-50%, packing specification is 5-100ml, as trophism functional health drink; The compound walnut and linseed oil fat emulsion oral solution of low concentration, containing the total oil mass of walnut oil and linseed oil is 1-20%, packing specification is 30-5000ml, as dining table beverage and popular drink.
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Cited By (3)
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| CN102907603A (en) * | 2012-10-23 | 2013-02-06 | 新疆中富益健生物科技有限公司 | Composite micro-capsule powder containing badam extractive and preparation method of composite micro-capsule powder |
| CN103053906A (en) * | 2013-01-20 | 2013-04-24 | 湖南奇异生物科技有限公司 | Preparation method of kiwi fruit seed oil oral emulsion |
| CN106509557A (en) * | 2016-10-25 | 2017-03-22 | 三河汇福生物科技有限公司 | Omega-3 fatty acid enriched lipidosome exercise drink and preparation method thereof |
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| CN103053906A (en) * | 2013-01-20 | 2013-04-24 | 湖南奇异生物科技有限公司 | Preparation method of kiwi fruit seed oil oral emulsion |
| CN106509557A (en) * | 2016-10-25 | 2017-03-22 | 三河汇福生物科技有限公司 | Omega-3 fatty acid enriched lipidosome exercise drink and preparation method thereof |
| CN106509557B (en) * | 2016-10-25 | 2020-02-07 | 三河汇福生物科技有限公司 | Omega-3 fatty acid-rich liposome sports beverage and preparation method thereof |
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Application publication date: 20101027 |