CN103643773B - One is photic stores light ceramic brick and production method thereof - Google Patents
One is photic stores light ceramic brick and production method thereof Download PDFInfo
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- CN103643773B CN103643773B CN201310672431.8A CN201310672431A CN103643773B CN 103643773 B CN103643773 B CN 103643773B CN 201310672431 A CN201310672431 A CN 201310672431A CN 103643773 B CN103643773 B CN 103643773B
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- photic
- light
- temperature frit
- frit
- accumulating powder
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- 239000000919 ceramic Substances 0.000 title claims abstract description 36
- 239000011449 brick Substances 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 6
- 239000000463 material Substances 0.000 claims abstract description 32
- 238000000034 method Methods 0.000 claims abstract description 29
- 235000015895 biscuits Nutrition 0.000 claims abstract description 16
- 238000007639 printing Methods 0.000 claims abstract description 12
- 239000011521 glass Substances 0.000 claims abstract description 10
- 238000004020 luminiscence type Methods 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims description 19
- 239000012190 activator Substances 0.000 claims description 6
- 238000007688 edging Methods 0.000 claims description 6
- 239000004744 fabric Substances 0.000 claims description 6
- 239000011159 matrix material Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 238000005498 polishing Methods 0.000 claims description 6
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 6
- 150000002910 rare earth metals Chemical class 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 229910003668 SrAl Inorganic materials 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims 2
- 238000010304 firing Methods 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 8
- 238000005299 abrasion Methods 0.000 abstract description 7
- 230000002688 persistence Effects 0.000 abstract description 6
- 239000003086 colorant Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 238000004891 communication Methods 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 206010039203 Road traffic accident Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000004313 glare Effects 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000012736 patent blue V Nutrition 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000001054 red pigment Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000001060 yellow colorant Substances 0.000 description 1
Landscapes
- Glass Compositions (AREA)
Abstract
The invention discloses and a kind of photicly store light ceramic brick and production method thereof, photic light-storing material is made photic luminescence glass layer through printing or distributing technique by ceramic biscuit, and can present multiple color in the dark, persistence is long.This technique can adopt serigraphy or distributing technique, can change floral designs at any time, and the toning of cooperation colorant, male and female mold more can present the multiple decorative artistic effect that third dimension is strong, pattern level is abundant.Method disclosed by the invention, solves the problem of existing photic light-storing material abrasion performance, weatherability, chemical resistance difference.
Description
Technical field
The invention belongs to the preparation field of architectural pottery product, be specifically related to a kind of photicly store light ceramic brick and production method thereof.
Background technology
Photic light-storing material is also called light storage type self luminous material, on-radiation light-storing material, non-transformer self-luminescent material etc.This material is initiatively inhaled and is stored the visible rays such as sunshine, light, ultraviolet light, veiling glare after 5 ~ 10 minutes, just can continuous illumination 6-8 hour in the dark, and can according to actual needs, make it send the multiple colouramas such as red, green, blue, Huang, purple.Because its distinctive high brightness, fast extinction, length store the excellent physicochemical properties such as light, making it be widely used in the every field such as architectural decoration, communications and transportation, security against fire, electronic communication, electric apparatus, instrument and meter, petrochemical industry, subway tunnel, printing printing and dyeing, advertising board, bullion, is 21 century extremely rising decorative hair luminescent material.
With the mark that photic light-storing material is made, road warning markers, prohibitory sign, Warning Mark, tourist district's mark, road construction safety sign and facility, changeable-message sign can be widely used in, people can clearly recognize in the weather of dark, foggy, bad weather, reduce the incidence of traffic accident, make the guiding of highway communication more convenient, thoughtful.Photic light-storing material is a kind of luminescent material of Intelligent energy-saving, its not electricity consumption, and equipment that need not be complicated, does not generate heat, can not cause fire, utilize the sunlight on daytime and the light at night to store light; Night automatic luminous, completely without manual operation.
The photic light-storing material great majority employing used for safety sign on the market at present contains the resin paste of transparent resins composition and light-storage luminant pigment ingredient and forms light-storage luminant layer, the transparent resins composition of 95% weight of total amount is coordinated in resin paste, above-mentioned material is as the use such as mark of road, and abrasion performance, weatherability, chemical resistance are all poor.
Summary of the invention
In view of the deficiencies in the prior art, the object of the present invention is to provide and a kind of photicly store light ceramic brick and production method thereof, be intended to the problem solving existing photic light-storing material abrasion performance, weatherability, chemical resistance difference.
For achieving the above object, the technical solution used in the present invention is as follows:
One is photic stores light ceramic brick, and photic light-storing material is made photic luminescence glass layer through printing or distributing technique by ceramic biscuit, and can present multiple color in the dark, persistence is long.
Described photic luminescence glass layer, wherein, if by typography, then fills a prescription by mass percentage, comprise the photic light-accumulating powder of 10 ~ 30%, 10 ~ 30% high temperature frit, the glaze stain of 0 ~ 1% and the stamp-pad ink of 40 ~ 60%; If press distributing technique, then fill a prescription by mass percentage, comprise the photic light-accumulating powder of 10 ~ 50%, the low temperature frit of 60 ~ 80% and the glaze stain of 0 ~ 1%.
Wherein, described photic light-accumulating powder is rear-earth-doped high temperature long-afterglow material, and be prepared from by rare earth activators doping matrix material, matrix material is specially Sr
4a1
4o
25, SrAl
2o
4, Sr
2mgSi
2o
7, CaA1
2o
4, CaTiO
3in one or more combination.
Wherein, rare earth activators comprises Eu
2+, Dy
3+, Nd
3+, Ce
3+, Pr
3+, Tb
3+, Yb
2+in one or more combination.
Wherein, the fineness of described high temperature frit is 100-200 order; The fineness of low temperature frit is 70-100 order.
The present invention discloses a kind of photic process storing light ceramic brick product, this technique can adopt serigraphy or distributing technique, can change floral designs at any time, the toning of cooperation colorant, male and female mold more can present the multiple decorative artistic effect that third dimension is strong, pattern level is abundant.
Mainly comprise the steps:
(1) 800 mesh sieves are crossed by by the photic light-accumulating powder taken of filling a prescription;
(2) if by typography, take high temperature frit and glaze stain by formula, after mixing with photic light-accumulating powder, cross 80 mesh sieves, add stamp-pad ink, stir; If press distributing technique, take low temperature frit and glaze stain by formula, after mixing with photic light-accumulating powder, cross 80 mesh sieves;
(3) if by typography, the slip prepared is crossed 80 orders and lead to reticulated printing on ceramic biscuit; If press distributing technique, mixed frit is crossed 80 orders and lead to screen cloth material on ceramic biscuit;
(4) in adobe, one deck low temperature frit is executed again;
(5) burn till through 850-950 DEG C of kiln after, edging polishing.
beneficial effect
1, photic light-storing material is covered on ceramic body as glass composite bed, the product made compared to resinae product on the market, more wear-resisting, chemical resistance, longer service life.
2, adopt ceramic process to produce, technology controlling and process is easy, can be used for producing in enormous quantities.
3, adopt frit serigraphy or distributing technique, can change floral designs at any time, the toning of cooperation colorant, male and female mold more can present the multiple decorative artistic effect that third dimension is strong, pattern level is abundant.
Accompanying drawing explanation
Fig. 1 is the rear-earth-doped photic process chart storing light ceramic brick and prepare.
Detailed description of the invention
One is photic stores light ceramic brick, and photic light-storing material is made photic luminescence glass layer through printing or distributing technique by ceramic biscuit.
Described photic luminescence glass layer, wherein, if by typography, then fills a prescription by mass percentage, comprise the photic light-accumulating powder of 10 ~ 30%, 10 ~ 30% high temperature frit, the glaze stain of 0 ~ 1% and the stamp-pad ink of 40 ~ 60%; If press distributing technique, then fill a prescription by mass percentage, comprise the photic light-accumulating powder of 10 ~ 50%, the low temperature frit of 60 ~ 80% and the glaze stain of 0 ~ 1%.
Wherein, described photic light-accumulating powder is rear-earth-doped high temperature long-afterglow material, and be prepared from by rare earth activators doping matrix material, matrix material is specially Sr
4a1
4o
25, SrAl
2o
4, Sr
2mgSi
2o
7, CaA1
2o
4, CaTiO
3in one or more combination.
Wherein, rare earth activators comprises Eu
2+, Dy
3+, Nd
3+, Ce
3+, Pr
3+, Tb
3+, Yb
2+in one or more combination.
Wherein, the fineness of described high temperature frit is 100-200 order; The fineness of low temperature frit is 70-100 order.
The present invention discloses a kind of photic process storing light ceramic brick, comprise the steps:
(1) 800 mesh sieves are crossed by by the photic light-accumulating powder taken of filling a prescription;
(2) if by typography, take high temperature frit and glaze stain by formula, after mixing with photic light-accumulating powder, cross 80 mesh sieves, add stamp-pad ink, stir; If press distributing technique, take low temperature frit and glaze stain by formula, after mixing with photic light-accumulating powder, cross 80 mesh sieves;
(3) if by typography, the slip prepared is crossed 80 orders and lead to reticulated printing on ceramic biscuit; If press distributing technique, mixed frit is crossed 80 orders and lead to screen cloth material on ceramic biscuit;
(4) in adobe, one deck low temperature frit is executed again;
(5) burn till through 850-950 DEG C of kiln after, edging polishing.
Photic light-storing material is made photic luminescence glass layer through printing or distributing technique by process of the present invention on ceramic biscuit, and can present multiple color in the dark, persistence is long.This technique can adopt serigraphy or distributing technique, can change floral designs at any time, and the toning of cooperation colorant, male and female mold more can present the multiple decorative artistic effect that third dimension is strong, pattern level is abundant.Method disclosed by the invention, solves the problem of existing photic light-storing material abrasion performance, weatherability, chemical resistance difference.
Embodiment 1:
By mass percentage, by the Sr of 15%
4a1
4o
25doping Eu
2+, Dy
3+energy-saving luminous material and 15% CaA1
2o
4doping Eu
2+, Nd
3+energy-saving luminous material crosses 800 mesh sieves together, mixes with the low temperature frit (fineness is 70-100 order) of 70%, crosses 80 mesh sieves afterwards.Get ceramic biscuit, mixed frit is crossed 80 orders and lead to screen cloth material on ceramic biscuit, then execute one deck low temperature frit.After burn till through 850 DEG C of kilns, edging polishing, finished product be send out coloured light in the dark sky blue store light ceramic brick, reach 6.5 hours persistence.This Ceramic Tiles has 4 grades of abrasion resistancies, good weatherability properties, not easily aging, strong resistance to chemical corrosion, 18%(V/V) hydrochloric acid---GHA level, 100g/L potassium hydroxide---GHA level.
Embodiment 2:
By mass percentage, by the Sr of 25%
2mgSi
2o
7energy-saving luminous material crosses 800 mesh sieves, crosses 80 mesh sieves, then adds the stamp-pad ink of 50%, stir after the high temperature frit (fineness is 100-200 order) with 25% mixes.Mixed slip is crossed 80 orders and lead to reticulated printing on ceramic biscuit, then execute one deck low temperature frit.After burn till through 950 DEG C of kilns, edging polishing, finished product be turn blue green light in the dark store light ceramic brick, reach 8 hours persistence.This Ceramic Tiles has 4 grades of abrasion resistancies, good weatherability properties, not easily aging, strong resistance to chemical corrosion, 18%(V/V) hydrochloric acid---GHA level, 100g/L potassium hydroxide---GHA level.
Embodiment 3:
By mass percentage, by the SrAl of 30%
2o
4doping Eu
2+, Dy
3+energy-saving luminous material crosses 800 mesh sieves, mixes with the low temperature frit (fineness is 70-100 order) of 70%.The golden yellow colorant of additional 0.3%, the Red pigment of 0.3%, mix respectively.Get ceramic biscuit, mixed frit is crossed respectively 80 order flower nets, through secondary material distributing on ceramic biscuit.After cloth, then execute one deck low temperature frit, after burn till through 900 DEG C of kilns, edging polishing.Finished product is store light ceramic brick with the colour of floral designs, reaches 7 hours persistence.This Ceramic Tiles has 4 grades of abrasion resistancies, good weatherability properties, not easily aging, strong resistance to chemical corrosion, 18%(V/V) hydrochloric acid---GHA level, 100g/L potassium hydroxide---GHA level.
Last it is noted that obviously, above-described embodiment is only for example of the present invention is clearly described, and the restriction not to embodiment.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without the need to also giving all embodiments.And thus the apparent change of amplifying out or variation be still among protection scope of the present invention.
Claims (2)
1. photicly store a light ceramic brick, it is characterized in that: on ceramic biscuit, photic light-storing material is made photic luminescence glass layer by printing or distributing technique;
When adopting typography, the raw material mass mixture ratio of described photic luminescence glass layer, comprise the photic light-accumulating powder of 10 ~ 30%, 10 ~ 30% high temperature frit, the glaze stain of 0 ~ 1% and the stamp-pad ink of 40 ~ 60%; Adopt distributing technique, the raw material mass mixture ratio of described photic luminescence glass layer, comprises the photic light-accumulating powder of 10 ~ 50%, the low temperature frit of 60 ~ 80% and the glaze stain of 0 ~ 1%;
Described photic light-accumulating powder is rear-earth-doped high temperature long-afterglow material, is prepared from by rare earth activators doping matrix material,
Wherein, described matrix material is specially Sr
4a1
4o
25, SrAl
2o
4, Sr
2mgSi
2o
7, CaA1
2o
4, CaTiO
3in one or more combination;
Described rare earth activators comprises Eu
2+, Dy
3+, Nd
3+, Ce
3+, Pr
3+, Tb
3+, Yb
2+in one or more combination.
2. the photic production method storing light ceramic brick as claimed in claim 1, is characterized in that: comprise the steps,
(1) the photic light-accumulating powder taken by pulp furnish is sieved;
(2) if by typography, take high temperature frit and glaze stain by pulp furnish, after mixing with photic light-accumulating powder, cross 80 mesh sieves, add stamp-pad ink, stir; If press distributing technique, take low temperature frit and glaze stain by pulp furnish, after mixing with photic light-accumulating powder, cross 80 mesh sieves;
(3) if by typography, the slip prepared is crossed logical reticulated printing on ceramic biscuit; If press distributing technique, mixed frit is crossed logical screen cloth material on ceramic biscuit;
(4) in adobe, one deck low temperature frit is executed again;
(5) burn till through kiln after, edging polishing;
Photic light-accumulating powder in described step (1) crosses grit number: 800 orders;
In described step (2), the fineness of high temperature frit is 100-200 order; The fineness of low temperature frit is 70-100 order;
The order number crossing logical reticulated printing or cloth in described step (3) is: 80 orders;
In described step (5), firing temperature is 850-950 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310672431.8A CN103643773B (en) | 2013-12-12 | 2013-12-12 | One is photic stores light ceramic brick and production method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310672431.8A CN103643773B (en) | 2013-12-12 | 2013-12-12 | One is photic stores light ceramic brick and production method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103643773A CN103643773A (en) | 2014-03-19 |
| CN103643773B true CN103643773B (en) | 2015-11-25 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310672431.8A Active CN103643773B (en) | 2013-12-12 | 2013-12-12 | One is photic stores light ceramic brick and production method thereof |
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| CN (1) | CN103643773B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108117260B (en) * | 2015-12-30 | 2019-11-29 | 诸暨市烈火工业设计工作室 | The preparation method of the accumulating type luminous glaze glass ceramic material of low temperature of glaze firing |
| CN112010673A (en) * | 2020-10-26 | 2020-12-01 | 佛山市东鹏陶瓷发展有限公司 | Luminous ceramic tile and preparation method thereof |
| CN113845306B (en) * | 2021-10-09 | 2023-03-28 | 广东松发陶瓷股份有限公司 | Ceramic color glaze material for underglaze transfer printing decoration, daily ceramic utensil and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197043A (en) * | 1998-04-27 | 1998-10-28 | 况学成 | Luminous printing glaze and prodn. method of printed luminous glazed tile |
| CN1408679A (en) * | 2002-08-28 | 2003-04-09 | 佛山欧神诺陶瓷有限公司 | Method for producing pattern permeating ceramic tile |
| GB2404379A (en) * | 2003-07-12 | 2005-02-02 | Andrew David Curtis | Method of producing a photoluminescent mosaic glass tile |
| CN1609027A (en) * | 2003-10-20 | 2005-04-27 | 梁锋 | High temperature luminous glazing and its production process and application in luminous glazed tile |
| CN101215189A (en) * | 2008-01-21 | 2008-07-09 | 尤晴波 | Outdoor cold-light source (luminous brick, noctilucent brick, fluorescent brick) |
| KR20090007342U (en) * | 2008-01-16 | 2009-07-21 | 김진철 | A Photo Luminescence Tile For Safety Refuge Mark |
-
2013
- 2013-12-12 CN CN201310672431.8A patent/CN103643773B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1197043A (en) * | 1998-04-27 | 1998-10-28 | 况学成 | Luminous printing glaze and prodn. method of printed luminous glazed tile |
| CN1408679A (en) * | 2002-08-28 | 2003-04-09 | 佛山欧神诺陶瓷有限公司 | Method for producing pattern permeating ceramic tile |
| GB2404379A (en) * | 2003-07-12 | 2005-02-02 | Andrew David Curtis | Method of producing a photoluminescent mosaic glass tile |
| CN1609027A (en) * | 2003-10-20 | 2005-04-27 | 梁锋 | High temperature luminous glazing and its production process and application in luminous glazed tile |
| KR20090007342U (en) * | 2008-01-16 | 2009-07-21 | 김진철 | A Photo Luminescence Tile For Safety Refuge Mark |
| CN101215189A (en) * | 2008-01-21 | 2008-07-09 | 尤晴波 | Outdoor cold-light source (luminous brick, noctilucent brick, fluorescent brick) |
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| Publication number | Publication date |
|---|---|
| CN103643773A (en) | 2014-03-19 |
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Address after: 528138 fan Lake Industrial Zone, Leping Town, Sanshui District, Guangdong, Foshan Patentee after: FOSHAN OCEANO CERAMICS Co.,Ltd. Address before: 528137 fan Lake Industrial Zone, Leping Town, Sanshui District, Guangdong, Foshan Patentee before: OCEANO CERAMICS Co.,Ltd. |
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Effective date of registration: 20231228 Address after: 333000 Jingdezhen Ceramic Industrial Park, Fuliang County, Jingdezhen City, Jiangxi Province Patentee after: JINGDEZHEN OUSHENNUO CERAMIC CO.,LTD. Address before: 528138 fan Lake Industrial Zone, Leping Town, Sanshui District, Guangdong, Foshan Patentee before: FOSHAN OCEANO CERAMICS Co.,Ltd. |