CN103616456B - 二硫代磷酸酯类农药代谢物的高效液相色谱-串联质谱检测方法 - Google Patents
二硫代磷酸酯类农药代谢物的高效液相色谱-串联质谱检测方法 Download PDFInfo
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- CN103616456B CN103616456B CN201310674588.4A CN201310674588A CN103616456B CN 103616456 B CN103616456 B CN 103616456B CN 201310674588 A CN201310674588 A CN 201310674588A CN 103616456 B CN103616456 B CN 103616456B
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Abstract
Description
时间(min) | 流速(ml/min) | A溶剂(%) | B溶剂(%) |
0.0 | 0.25 | 30 | 70 |
0.5 | 0.25 | 30 | 70 |
1.0 | 0.25 | 65 | 35 |
2.0 | 0.25 | 65 | 35 |
2.5 | 0.25 | 30 | 70 |
3.0 | 0.25 | 30 | 70 |
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CN105891354B (zh) * | 2016-03-31 | 2018-03-09 | 山东五洲检测有限公司 | 一种高粱种植土壤中倍硫磷含量的检测方法 |
CN111257442A (zh) * | 2020-01-06 | 2020-06-09 | 桂林理工大学 | 一种分离富集水环境中16种有机磷农药的方法 |
CN115436556B (zh) * | 2022-09-20 | 2024-04-19 | 常州佳德医药科技有限公司 | 一种利用反相液相色谱法测定硼酸酯类化合物纯度的方法及应用 |
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Non-Patent Citations (5)
Title |
---|
Medicinal Chemistry》.2002,第10卷3807-3815. * |
Toshiaki Matsui,et al.Discovery of Novel Phosphonic Acid Derivatives as New Chemical Leads for Inhibitors of TNF-a Production.《Bioorganic & * |
Yeong-Beom Lee,et al.Simple synthetic route to soluble polyimides via nitro-displacement reaction and their second-order nonlinear optical properties.《J. Mater. Chem.》.1999,第9卷第2346页右栏最后1段至第2347页左栏第1段. * |
有机磷农药的分子结构和化学性质;苏寿承;《浙江林学院学报》;19881231;第5卷(第3期);第321页第2.1节,图1 * |
气相色谱法分析尿样中六种有机磷农药代谢产物;杨玉林等;《中国卫生检验杂志》;20030228;第13卷(第1期);24-26 * |
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