CN103614901B - A kind of preparation method of soft type noctilucent coating fabric - Google Patents
A kind of preparation method of soft type noctilucent coating fabric Download PDFInfo
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- CN103614901B CN103614901B CN201310615448.XA CN201310615448A CN103614901B CN 103614901 B CN103614901 B CN 103614901B CN 201310615448 A CN201310615448 A CN 201310615448A CN 103614901 B CN103614901 B CN 103614901B
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Abstract
The invention discloses the preparation method of a kind of soft type noctilucent coating fabric, including step it is: by fatty acid Ethoxylate, alkyl acrylate and water mix and blend, the rare earth aluminic acid strontium adding solvent naphtha, fatty alcohol-polyoxyethylene ether, nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium, amino modified polysiloxane and interpolation europium dysprosium continues stirring, and add ammonia and be neutralized to neutrality, obtain mixing slurry；Mixing slurry is coated on fabric and bakes and obtain soft type noctilucent coating fabric.By the way, the preparation method of the soft type noctilucent coating fabric of the present invention, the method is not on the premise of affecting noctilucent coating fabric luminescent properties and physical and mechanical properties, improve the softness of noctilucent coating fabric, improve wearability, the method production cost is low and technique simple, can large-scale development application.
Description
Technical field
The present invention relates to function textile processing and manufacturing field, particularly relate to the preparation method of a kind of soft type noctilucent coating fabric.
Background technology
Noctilucent coating fabric is a kind of novel high-tech multifunctional fabric, as long as this fabric absorbs visible ray or ultraviolet light ten minutes or more than ten minutes, just can be stored among fabric by luminous energy.Noctilucent coating fabric can reach more than 10 hours by continuous illumination at night or dark, and the light sent has such as various colors such as white, aeruginous, redness, yellow.Noctilucent coating fabric fluorescent lifetime length and brightness are high, and the nontoxic radiationless property of light sent will not produce any harm to environment and human body.Noctilucent coating fabric is because it is in the observability at night, and application in recent years is relatively broad, is mainly used in the fields such as building decoration, transportation, night work, daily life and amusement clothing.
Chinese patent CN1333402A discloses the production method of a kind of luminous fabric, and it uses the technique of PLATE SCREAM PRINTING, there is production cost high, and complex process, fabric feeling is harder, and affect noctilucent coating textile develops application further.
Summary of the invention
The technical problem that present invention mainly solves is to provide the preparation method of a kind of soft type noctilucent coating fabric, and the wearability of fabric obtained is good.
For solving above-mentioned technical problem, the technical scheme that the present invention uses is: provides the preparation method of a kind of soft type noctilucent coating fabric, including step is:
(1) by fatty acid Ethoxylate, alkyl acrylate and water mix and blend, the rare earth aluminic acid strontium adding solvent naphtha, fatty alcohol-polyoxyethylene ether, nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium, amino modified polysiloxane and interpolation europium dysprosium continues stirring, and add ammonia and be neutralized to neutrality, obtain mixing slurry；
(2) described mixing slurry is coated on fabric and bakes obtain soft type noctilucent coating fabric.
In a preferred embodiment of the present invention, the ratio of the described soft type each component of noctilucent coating fabric is: with opposed fabric gravimeter, fatty acid Ethoxylate 0.1-0.5 part, alkyl acrylate 8-15 part, solvent naphtha 0.01-3 part, fatty alcohol-polyoxyethylene ether 0.2-0.5 part, nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium 0.2-0.5 part, amino modified polysiloxane 0.5-1.5 part, interpolation rare earth aluminic acid 25-45 part of europium dysprosium, 100 parts of fabric.
In a preferred embodiment of the present invention, mixing process described in step (1) be speed of agitator be 100-150 rev/min, temperature be 15-25 DEG C under conditions of stir 10-30 minute.
In a preferred embodiment of the present invention, continuing whipping process described in step (1) is to stir 30-50 minute under conditions of speed of agitator is 500-800 rev/min.
In a preferred embodiment of the present invention, described in step (2), fabric is woven fabric, knitted fabric or non-weaving cloth.
In a preferred embodiment of the present invention, mixing slurry described in step (2) is coated on described fabric by the method for dyeing and finishing, stamp or coating.
In a preferred embodiment of the present invention, the process that bakes described in step (2) is to bake 3-7 minute at 120-180 DEG C.
The invention has the beneficial effects as follows: the preparation method of the soft type noctilucent coating fabric of the present invention, the method is not on the premise of affecting noctilucent coating fabric luminescent properties and physical and mechanical properties, overcome the existing shortcoming that noctilucent coating textile touch is harder, wearability is the most excellent, improve the softness of noctilucent coating fabric, improve wearability, the method production cost is low and technique simple, can large-scale development application.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, all other embodiments that those of ordinary skill in the art are obtained under not making creative work premise, broadly fall into the scope of protection of the invention.
Embodiment one:
The preparation method of a kind of soft type noctilucent coating fabric is provided, including processing step be:
(1) adding in homogenizers by 1.5 parts of fatty acid Ethoxylates, 25 parts of alkyl acrylates and 20 parts of water, low whipping speed is 100 revs/min, temperature stirs 30 minutes under conditions of being 20 DEG C, is allowed to mix homogeneously；The rare earth aluminic acid strontium adding 65 parts of solvent naphthas, 0.7 part of nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium, 2 parts of amino modified polysiloxanes and 20 parts of interpolation europium dysprosiums stirs 30 minutes under the mixing speed of 500 revs/min, add ammonia and be neutralized to neutrality, prepare noctilucence soft type fabric mixing slurry；
(2) by the method for coating, above-mentioned noctilucence soft type fabric mixing slurry is coated in the surface of woven fabric, then the fabric after coating is baked 7 minutes under conditions of 150 DEG C, obtain soft type noctilucent coating fabric.
Embodiment two:
The preparation method of a kind of soft type noctilucent coating fabric is provided, including processing step be:
(1) adding in homogenizers by 2.1 parts of fatty acid Ethoxylates, 32 parts of alkyl acrylates and 25 parts of water, low whipping speed is 110 revs/min, temperature stirs 30 minutes under conditions of being 25 DEG C, is allowed to mix homogeneously；The rare earth aluminic acid strontium adding 70 parts of solvent naphthas, 1.0 parts of nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium, 2.4 parts of amino modified polysiloxanes and 23 parts of interpolation europium dysprosiums stirs 40 minutes under the mixing speed of 600 revs/min, add ammonia and be neutralized to neutrality, prepare noctilucence soft type fabric mixing slurry；
(2) by the method for stamp, above-mentioned noctilucence soft type fabric mixing slurry is coated in the surface of knitted fabric, then the fabric after coating is baked 5 minutes under conditions of 160 DEG C, obtain soft type noctilucent coating fabric.
Embodiment three:
The preparation method of a kind of soft type noctilucent coating fabric is provided, including processing step be:
(1) adding in homogenizers by 2.5 parts of fatty acid Ethoxylates, 45 parts of alkyl acrylates and 30 parts of water, low whipping speed is 150 revs/min, temperature stirs 30 minutes under conditions of being 25 DEG C, is allowed to mix homogeneously；The rare earth aluminic acid strontium adding 75 parts of solvent naphthas, 1.2 parts of nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium, 2.6 parts of amino modified polysiloxanes and 30 parts of interpolation europium dysprosiums stirs 50 minutes under the mixing speed of 800 revs/min, add ammonia and be neutralized to neutrality, prepare noctilucence soft type fabric mixing slurry.
(2) by the method for coating, above-mentioned noctilucence soft type fabric mixing slurry is coated in the surface of supatex fabric, then the fabric after coating is baked 4 minutes under conditions of 170 DEG C, obtain soft type noctilucent coating fabric.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every equivalent structure utilizing description of the invention content to be made or equivalence flow process conversion; or directly or indirectly it is used in other relevant technical field, the most in like manner it is included in the scope of patent protection of the present invention.
Claims (6)
1. the preparation method of a soft type noctilucent coating fabric, it is characterised in that include that step is:
(1) by fatty acid Ethoxylate, alkyl acrylate and water mix and blend, the rare earth aluminic acid strontium adding solvent naphtha, fatty alcohol-polyoxyethylene ether, nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium, amino modified polysiloxane and interpolation europium dysprosium continues stirring, and add ammonia and be neutralized to neutrality, obtain mixing slurry；
(2) described mixing slurry is coated on fabric and bakes obtain soft type noctilucent coating fabric；
The ratio of the described soft type each component of noctilucent coating fabric is: with opposed fabric gravimeter, fatty acid Ethoxylate 0.1-0.5 part, alkyl acrylate 8-15 part, solvent naphtha 0.01-3 part, fatty alcohol-polyoxyethylene ether 0.2-0.5 part, nonylphenol polyoxyethylenes ether propyl sulfonic acid sodium 0.2-0.5 part, amino modified polysiloxane 0.5-1.5 part, interpolation rare earth aluminic acid strontium 25-45 part of europium dysprosium, 100 parts of fabric.
The preparation method of soft type noctilucent coating fabric the most according to claim 1, it is characterised in that mixing process described in step (1) be speed of agitator be 100-150 rev/min, temperature be 15-25 DEG C under conditions of stir 10-30 minute.
The preparation method of soft type noctilucent coating fabric the most according to claim 1, it is characterised in that continuing whipping process described in step (1) is to stir 30-50 minute under conditions of speed of agitator is 500-800 rev/min.
The preparation method of soft type noctilucent coating fabric the most according to claim 1, it is characterised in that described in step (2), fabric is woven fabric, knitted fabric or non-weaving cloth.
The preparation method of soft type noctilucent coating fabric the most according to claim 1, it is characterised in that mixing slurry described in step (2) is coated on described fabric by the method for stamp or coating.
The preparation method of soft type noctilucent coating fabric the most according to claim 1, it is characterised in that the process that bakes described in step (2) is to bake 3-7 minute at 120-180 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310615448.XA CN103614901B (en) | 2013-11-28 | 2013-11-28 | A kind of preparation method of soft type noctilucent coating fabric |
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| CN201310615448.XA CN103614901B (en) | 2013-11-28 | 2013-11-28 | A kind of preparation method of soft type noctilucent coating fabric |
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| CN103614901A CN103614901A (en) | 2014-03-05 |
| CN103614901B true CN103614901B (en) | 2016-08-17 |
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| CN112301748A (en) * | 2019-07-31 | 2021-02-02 | 晋江市创健鞋材贸易有限公司 | Preparation method of luminous fabric |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101429731A (en) * | 2008-12-25 | 2009-05-13 | 李商熙 | Luminous fabric pressing panel |
| CN101979761A (en) * | 2010-10-19 | 2011-02-23 | 顾军 | Luminous coating fabric and processing method thereof |
| CN102154824A (en) * | 2011-02-14 | 2011-08-17 | 江南大学 | Preparation method of functional fabric capable of emitting light at night |
| JP2012046855A (en) * | 2010-08-30 | 2012-03-08 | Mitsubishi Rayon Co Ltd | Acrylic fiber bundle as carbon fiber precursor and method for producing the same |
-
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- 2013-11-28 CN CN201310615448.XA patent/CN103614901B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101429731A (en) * | 2008-12-25 | 2009-05-13 | 李商熙 | Luminous fabric pressing panel |
| JP2012046855A (en) * | 2010-08-30 | 2012-03-08 | Mitsubishi Rayon Co Ltd | Acrylic fiber bundle as carbon fiber precursor and method for producing the same |
| CN101979761A (en) * | 2010-10-19 | 2011-02-23 | 顾军 | Luminous coating fabric and processing method thereof |
| CN102154824A (en) * | 2011-02-14 | 2011-08-17 | 江南大学 | Preparation method of functional fabric capable of emitting light at night |
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Effective date of registration: 20220908 Address after: No. 1-3, Daizhuang Road, Gaoyou Street, Gaoyou City, Yangzhou City, Jiangsu Province 225600 Patentee after: Yangzhou Jianghui Textile Technology Co.,Ltd. Address before: Building 1, No. 8, Jindu Road, Southeast Economic Development Zone, Changshu City, Suzhou City, Jiangsu Province 215558 Patentee before: CHANGSHU JIANGHUI FIBER PRODUCTS TECHNOLOGY CO.,LTD. |
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