CN102876500A - Preparation method of acidic dye printing anti-staining detergent - Google Patents
Preparation method of acidic dye printing anti-staining detergent Download PDFInfo
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- CN102876500A CN102876500A CN2012104126739A CN201210412673A CN102876500A CN 102876500 A CN102876500 A CN 102876500A CN 2012104126739 A CN2012104126739 A CN 2012104126739A CN 201210412673 A CN201210412673 A CN 201210412673A CN 102876500 A CN102876500 A CN 102876500A
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Abstract
The invention discloses a preparation method of acidic dye printing anti-staining detergent, which comprises the following steps of: A. sequentially adding fatty alcohol-polyoxyethylene ether AEO-9, AEO-25 and water into mixing kettle, heating up to 30-50 DEG C, and stirring for 0.5-1 hour to dissolve the mixture; and B. under the condition of vigorous stirring, sequentially adding poly-4-hydroxy tetramethylene 1, 2-dicarboxylic acid, dodecanol amide ethyl ester sulfo succinic acid disodium salt, cocamidopropyl betaine, ethylene diamine tetraacetic acid (EDTA) disodium salt and sodium metasilicate into the solution obtained in the step A, adding a certain quantity of water into the mixed solution, and stirring for 0.5-2 hours at the temperature of 40-80 DEG C. The prepared acidic dye printing anti-staining detergent is excellent in detergent washing performance and high in contamination prevention performance, and avoids unfixed dye and printing gum contaminating the printed fabric, thus improving the color fastness and the color brilliance of the fabric, and maintaining the definition of the printed pattern.
Description
Technical field:
The present invention relates to the anti-detergent of being stained with of a kind of matching stain stamp, particularly the anti-preparation method who is stained with detergent of a kind of live acid dye printing.
Background technology:
Generally all must strictly wash fully behind the used for textiles dye printing, soap or reduction clearing technique, this is because contain a large amount of superpolymer slurries in the bath of soaping of PRINTED FABRIC, these dyestuffs, printing assistant etc. that wash the superpolymer slurry that comes and not set from fabric are fused together, be easy to stain white ground and the decorative pattern place of PRINTED FABRIC, stain white ground and cause white ground not white, stain and to decorative pattern, cause the variable color of decorative pattern coloured light or color fastness decreased.Along with the increase of chinlon/spandex blending tprinted Fabrics demand, the tarnishing of chinlon/spandex PRINTED FABRIC becomes problem demanding prompt solution.Weak acid dye and neutral premetallized dyes are mainly used in the direct printing of chinlon/spandex elastic force swimsuit fabric.During matching stain stamp aftertreatment (wash, soap), matching stain and the printing gum of not set are arranged in the bath if soap, can return and be stained with on the PRINTED FABRIC, make the color fastness decreased at decorative pattern place, without the flower type light color or be located in vain staining etc., thereby affect the quality of Printing.Guarantee that the chinlon/spandex PRINTED FABRIC is not stain in vain, the stamp colour fastness is good and bright in colour, will select the acid thickening agent that enhancing rate and dye uptake are high, staining is few on the one hand; On the other hand, in washing and soap washing, want the acid stamp of reasonable selection to prevent in vain staiing soaping agent.
Summary of the invention:
Goal of the invention: the defective for prior art exists, the invention provides a kind of washing excellent property, anti-contamination ability is strong, can improve simultaneously the anti-preparation method who is stained with detergent of matching stain stamp of colour fastness and the colour brightness of fabric.
Technical scheme: for achieving the above object, the present invention is by the following technical solutions: the anti-preparation of being stained with detergent of a kind of live acid dye printing: A, add successively fatty alcohol-polyoxyethylene ether AEO-9 in the composite still of 1000ml, AEO-25 and water, be warming up to 30 ~ 50 ℃, stirred 0.5 ~ 1 hour, and made its dissolving.B, under vigorous stirring, in mentioned solution, add successively, poly--4 monohydroxy tetramethylenes 1,2-dicarboxylic acid, dodecanol acid amides ethyl ester disodium sulfosuccinate salt, AMONYL 380LC, EDETATE DISODIUM, Starso adds quantitative water again, stirred 0.5 ~ 2 hour at 40 ~ 80 ℃, make active quantities and be 25% optimization soaping agent product.Raw materials used mass fraction is:
Fatty alcohol-polyoxyethylene ether AEO-9:1 part
AEO-25:1 ~ 1.8 part
Poly--4 monohydroxy tetramethylenes 1,2-dicarboxylic acid: 10 ~ 40 parts
Dodecanol acid amides ethyl ester disodium sulfosuccinate salt: 1 ~ 4.8 part
AMONYL 380LC: 1 ~ 5.2 part
EDETATE DISODIUM: 0. 05 ~ 1 part
Starso: 0.05 ~ 1 part
Water: an amount of.
Described matching stain stamp is anti-to be stained with in the preparation of detergent, AEO-9:AEO-25: poly--4 monohydroxy tetramethylenes 1, the 2-dicarboxylic acid: dodecanol acid amides ethyl ester disodium sulfosuccinate salt: AMONYL 380LC: EDETATE DISODIUM: the mass ratio of Starso is 1:1 ~ 1.8:10 ~ 40:1 ~ 4.8:1 ~ 5.2:0.05 ~ 0.6:0.05 ~ 0.6.
According to above technical scheme, can realize following beneficial effect: compared with prior art, the present invention has the following advantages: the anti-detergent washing excellent property of being stained with of the obtained matching stain stamp of the present invention, anti-contamination ability is strong, in the time of can avoiding chinlon/spandex BLENDED FABRIC stamp to soap, the dyestuff of set and printing gum do not stain PRINTED FABRIC, improve colour fastness and the colour brightness of fabric, keep the sharpness of decalcomania.
Embodiment:
Below in conjunction with embodiment the present invention is done further detailed description, but the scope of protection of present invention is not limited to the scope that embodiment represents.
Embodiment 1:
Add successively 10g fatty alcohol-polyoxyethylene ether AEO-9 in the composite still of 1000ml, 13g AEO-25 and 500ml water are warming up to 30 ~ 50 ℃, stir 0.5 ~ 1 hour, make its dissolving; Under vigorous stirring, in mentioned solution, add successively, 180g gathers-4 monohydroxy tetramethylenes 1,2-dicarboxylic acid, 23g dodecanol acid amides ethyl ester disodium sulfosuccinate salt, the 26g AMONYL 380LC, the 3g EDETATE DISODIUM, the 2g Starso adds 270ml water again, stirred 0.5 ~ 2 hour at 40 ~ 80 ℃, make active quantities and be 25% optimization soaping agent product.
Claims (2)
1. the anti-preparation method who is stained with detergent of a matching stain stamp: it is characterized in that: A, add successively fatty alcohol-polyoxyethylene ether AEO-9 in the composite still of 1000ml, AEO-25 and water are warming up to 30 ~ 50 ℃, stir 0.5 ~ 1 hour, make its dissolving; B, under vigorous stirring, in mentioned solution, add successively, poly--4 monohydroxy tetramethylenes 1,2-dicarboxylic acid, dodecanol acid amides ethyl ester disodium sulfosuccinate salt, AMONYL 380LC, EDETATE DISODIUM, Starso adds quantitative water again, stirred 0.5 ~ 2 hour at 40 ~ 80 ℃, make active quantities and be 25% optimization detergent product; Raw materials used mass fraction is:
Fatty alcohol-polyoxyethylene ether AEO-9:1 part
AEO-25:1 ~ 1.8 part
Poly--4 monohydroxy tetramethylenes 1,2-dicarboxylic acid: 10 ~ 40 parts
Dodecanol acid amides ethyl ester disodium sulfosuccinate salt: 1 ~ 4.8 part
AMONYL 380LC: 1 ~ 5.2 part
EDETATE DISODIUM: 0. 05 ~ 1 part
Starso: 0.05 ~ 1 part
Water: an amount of.
2. the anti-preparation method who is stained with detergent of described matching stain stamp according to claim 1, it is characterized in that: AEO-9:AEO-25: poly--4 monohydroxy tetramethylenes 1, the 2-dicarboxylic acid: dodecanol acid amides ethyl ester disodium sulfosuccinate salt: AMONYL 380LC: EDETATE DISODIUM: the mass ratio of Starso is 1:1 ~ 1.8:10 ~ 40:1 ~ 4.8:1 ~ 5.2:0.05 ~ 0.6:0.05 ~ 0.6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104126739A CN102876500A (en) | 2012-10-25 | 2012-10-25 | Preparation method of acidic dye printing anti-staining detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104126739A CN102876500A (en) | 2012-10-25 | 2012-10-25 | Preparation method of acidic dye printing anti-staining detergent |
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| Publication Number | Publication Date |
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| CN102876500A true CN102876500A (en) | 2013-01-16 |
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| CN2012104126739A Pending CN102876500A (en) | 2012-10-25 | 2012-10-25 | Preparation method of acidic dye printing anti-staining detergent |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103498272A (en) * | 2013-09-17 | 2014-01-08 | 上海婉静纺织科技有限公司 | Fabric blended by milk protein fibers and cotton fibers |
| CN103643559A (en) * | 2013-11-30 | 2014-03-19 | 常熟市华宇针织印染有限公司 | Preparation method of textile dyeing and finishing aid |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101130717A (en) * | 2006-08-21 | 2008-02-27 | 上海德桑精细化工有限公司 | Agent for cleaning dacron and blending dyeing material |
-
2012
- 2012-10-25 CN CN2012104126739A patent/CN102876500A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101130717A (en) * | 2006-08-21 | 2008-02-27 | 上海德桑精细化工有限公司 | Agent for cleaning dacron and blending dyeing material |
Non-Patent Citations (1)
| Title |
|---|
| 展义臻，等: "活性染料常用净洗剂的研究进展", 《染整技术》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103498272A (en) * | 2013-09-17 | 2014-01-08 | 上海婉静纺织科技有限公司 | Fabric blended by milk protein fibers and cotton fibers |
| CN103498272B (en) * | 2013-09-17 | 2015-07-01 | 上海婉静纺织科技有限公司 | Fabric blended by milk protein fibers and cotton fibers |
| CN103643559A (en) * | 2013-11-30 | 2014-03-19 | 常熟市华宇针织印染有限公司 | Preparation method of textile dyeing and finishing aid |
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Application publication date: 20130116 |