CN103609599A - Botanical herbicide powder and preparation method thereof - Google Patents

Botanical herbicide powder and preparation method thereof Download PDF

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Publication number
CN103609599A
CN103609599A CN201310555253.0A CN201310555253A CN103609599A CN 103609599 A CN103609599 A CN 103609599A CN 201310555253 A CN201310555253 A CN 201310555253A CN 103609599 A CN103609599 A CN 103609599A
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parts
extracts
weed killer
killer herbicide
eupatorium herb
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CN201310555253.0A
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CN103609599B (en
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李文斌
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Xuzhou Fengrun Biological Organic Fertilizer Technology Development Co Ltd
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Abstract

The invention relates to botanical herbicide powder and a preparation method thereof, and belongs to the technical field of herbicide processing. The botanical herbicide powder is prepared from the following components in parts by weight: 15 to 20 parts of soapberry testa extract, 10 to 15 parts of sphenoclea zeylanica extract, 10 to 15 parts of fragrant eupatorium herb extracting solution, 5 to 8 parts of tween-80 and 50 to 55 parts of maltodextrin. The preparation method comprises the following steps: mixing the components in proportion, stirring for 30 to 35 minutes and then homogenizing for 25 to 30 minutes under the condition of 300MPa to 350MPa so as to obtain a lactescence; and performing spray drying treatment on the lactescence by controlling spray drying conditions that the inlet air temperature ranges from 165 DEG C to 163 DEG C, the exhaust temperature ranges from 98 DEG C to 101 DEG C, the pumping speed ranges from 8.0mL/min to 8.5mL/min, the exhaust pressure ranges from 100Pa to 150Pa and the inlet air quantity ranges from 1050L/h to 1055L/h, namely, obtaining the botanical herbicide powder. The botanical herbicide powder has the good water solubility and can be used independently or compounded with other herbicides. The botanical herbicide powder has the advantages of being efficient, environment-friendly and difficult to generate resistibility.

Description

A kind of plant resource weed killer herbicide pulvis and preparation method thereof
Technical field
The present invention relates to a kind of weed killer herbicide, be specifically related to a kind of plant resource weed killer herbicide pulvis and preparation method thereof, belong to weed killer herbicide processing technique field.
Background technology
In the later stage forties 20th century, chemical synthetic pesticide gains great popularity because of the feature such as efficient, quick-acting, insecticidal spectrum is wide, and this makes the research of botanical pesticide and use be once absorbed in low ebb.Yet along with the use of chemical pesticide, its drawback also reveals gradually, " 3R " problem (residual, pesticide resistance, insect rampant again) for example.Botanical pesticide, because the features such as it is efficient, low toxicity, low-residual, selectivity is high, pest is difficult for developing immunity to drugs cause people's concern again, becomes the focus of current pesticide research.Because botanical pesticide is low to person poultry toxicity, easily degraded in environment, essentially no obvious residual hazard problem.Therefore, botanical pesticide can be applied to the aspects such as vegetables, tealeaves, traditional Chinese medicine, the production of flowers and plants and urban afforestation prevention and elimination of disease and pests.
Nowadays, global agrochemical market continues to increase, and pesticide market sales volume is up to 30,000,000,000 dollars of left and right, and year increases by 1.2%.Wherein weed killer herbicide is 15,000,000,000 dollars of left and right, accounts for 50%, year growth by 1.2%.Weed killer herbicide claims again weedicide, in order to eliminate or to suppress a class material of plant growth.Effect is subject to the impact of weed killer herbicide, plant and environmental condition three factors.By effect, be divided into go out natural disposition and selective herbicide, conventional kind is organic compound.Can be widely used in ground weeds, the assorted noxious plants such as tree of filling with, mix such as control farmland, orchard, floral nursery, grassland and uncultivated area, railway line, river course, reservoir, warehouse.Along with the development of Chinese agricultural modernization and agricultural workforce's progressively transfer, cultivation tillage method trends towards scale and intensive, and the demand of agricultural chemicals is significantly increased.Wherein, weed killer herbicide growth rate in recent years, far above insecticide and bactericide development level, accounts for 1/3 of agricultural chemicals output proportion.Current national farmland chemical weed control area has reached 0.53 hundred million hectare of left and right, compared with 1980, has increased more than 10 times.Although the development of weed killer herbicide is rapid, but still exist many problems.The one, herbicide resistance is on the rise.Over the past two decades, in world wide, have at least 30 above countries to find that different weeds have produced resistance to the different polytype weed killer herbicide of chemical constitution; The 2nd, weed killer herbicide product on the market exists the problems such as herbicide spectral limit is narrow, efficiency is low, safety shortcoming.
The thick thick bull pine of cusp scape; the irregular wrinkle striped of surface tool; in areas such as China Taiwan, Guangdong, Guangxi, Yunnan, all there is distribution; research shows; the methanolic extract of cusp flower can suppress the growth of rice seedling; sampling point and leaf age that inhibitory action is spent because of cusp are variant: the extract of reproductive organs is the strongest to rice inhibiting effect, is secondly leaf, stem, and the inhibitory action of root is the poorest; The cusp flower inhibitory action that leaf age is large is strong.Fragrant eupatorium herb ethanol extract has allelopathy in various degree to cowpea, green cucumber, radish, cabbage heart, Chinese cabbage, a variety of Chinese cabbage, paddy rice and barnyard grass.In addition, in soapberry exosper, be also rich in the active ingredient that weed growth is played to inhibition.It is the weed killer herbicide pulvis of a kind of efficient, environmentally friendly and difficult generation resistance of main herbicidal active component exploitation that the present invention utilizes soapberry exosper extract, cusp flower extract, fragrant eupatorium herb extract, overcomes the problem that prior art exists.
Summary of the invention
The object of this invention is to provide a kind of plant resource weed killer herbicide pulvis, this weed killer herbicide pulvis good water solubility, can be used separately or use with other mixture of herbicides, has the advantages such as efficient, environmentally friendly and difficult generation resistance.
In order to address the above problem, the technical solution adopted in the present invention is:
A plant resource weed killer herbicide pulvis, the weight portion of each component is:
15 ~ 20 parts of soapberry exosper extracts, 10 ~ 15 parts of cusp flower extracts, 10 ~ 15 parts of fragrant eupatorium herb extracts, 5 ~ 8 parts of Tween-80s, 50 ~ 55 parts of maltodextrins;
15 ~ 18 parts of soapberry exosper extracts, 10 ~ 13 parts of cusp flower extracts, 10 ~ 13 parts of fragrant eupatorium herb extracts, 6 ~ 8 parts of Tween-80s, 50 ~ 53 parts of maltodextrins;
15 ~ 18 parts of soapberry exosper extracts, 13 ~ 15 parts of cusp flower extracts, 10 ~ 13 parts of fragrant eupatorium herb extracts, 6 ~ 8 parts of Tween-80s, 53 ~ 55 parts of maltodextrins;
18 ~ 20 parts of soapberry exosper extracts, 13 ~ 15 parts of cusp flower extracts, 13 ~ 15 parts of fragrant eupatorium herb extracts, 6 ~ 8 parts of Tween-80s, 53 ~ 55 parts of maltodextrins;
18 ~ 20 parts of soapberry exosper extracts, 13 ~ 15 parts of cusp flower extracts, 13 ~ 15 parts of fragrant eupatorium herb extracts, 5 ~ 6 parts of Tween-80s, 53 ~ 55 parts of maltodextrins;
15 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 13 parts of fragrant eupatorium herb extracts, 6 parts of Tween-80s, 53 parts of maltodextrins;
20 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 15 parts of fragrant eupatorium herb extracts, 5 parts of Tween-80s, 55 parts of maltodextrins.
Another object of the present invention is to provide a kind of preparation method of plant resource weed killer herbicide pulvis, comprises the steps:
Above material is mixed according to the above ratio, stir 30 ~ 35min, then homogeneous 25 ~ 30min under the condition of 300 ~ 350Mpa, obtains emulsion; Controlling spraying drying condition is 165 ~ 163 ℃ of EATs, 98 ~ 101 ℃ of temperature of outgoing airs, pump speed 8.0 ~ 8.5mL/min, air draft pressure 100~150Pa, intake: 1050 ~ 1055L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.
The present invention with respect to the beneficial effect of prior art is:
The present invention adopts soapberry exosper extract, cusp flower extract, fragrant eupatorium herb extract is composite forms, make full use of the mixed synergistic effect of different activities material, overcome single herbicide agent exploitation with duration, cost is high, cost is large, and consumption is used the weeds shortcoming that easily develops immunity to drugs to obtain greatly, for a long time, make weed killer herbicide pulvis good water solubility, can use separately or use with other mixture of herbicides, there is the advantages such as efficient, environmentally friendly and difficult generation resistance; Its preparation technology is simple to operate, with low cost, is adapted at industrial promoting the use of.
Embodiment
Below by embodiment, the present invention is described in further details, these embodiment are only used for illustrating the present invention, do not limit the scope of the invention.
embodiment 1
A plant resource weed killer herbicide pulvis, the weight portion of each component is:
15 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 13 parts of fragrant eupatorium herb extracts, 6 parts of Tween-80s, 53 parts of maltodextrins.
Its preparation method, comprises the steps:
Above material is mixed according to the above ratio, stir 32min, then homogeneous 30min under the condition of 300Mpa, obtains emulsion; Controlling spraying drying condition is 165 ± 1 ℃ of EATs, 98 ℃ of temperature of outgoing airs, pump speed 8.0mL/min, air draft pressure 150Pa, intake: 1055L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.
embodiment 2
A plant resource weed killer herbicide pulvis, the weight portion of each component is:
20 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 15 parts of fragrant eupatorium herb extracts, 5 parts of Tween-80s, 55 parts of maltodextrins.
Its preparation method, comprises the steps:
Above material is mixed according to the above ratio, stir 30min, then homogeneous 30min under the condition of 300Mpa, obtains emulsion; Controlling spraying drying condition is 165 ± 1 ℃ of EATs, 98 ℃ of temperature of outgoing airs, pump speed 8.0mL/min, air draft pressure 150Pa, intake: 1050L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.
embodiment 3
A plant resource weed killer herbicide pulvis, the weight portion of each component is:
18 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 15 parts of fragrant eupatorium herb extracts, 6 parts of Tween-80s, 55 parts of maltodextrins.
Its preparation method, comprises the steps:
Above material is mixed according to the above ratio, stir 30min, then homogeneous 30min under the condition of 300Mpa, obtains emulsion; Controlling spraying drying condition is 165 ± 1 ℃ of EATs, 98 ℃ of temperature of outgoing airs, pump speed 8.2mL/min, air draft pressure 130Pa, intake: 1050L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.
embodiment 4
A plant resource weed killer herbicide pulvis, the weight portion of each component is:
18 parts of soapberry exosper extracts, 13 parts of cusp flower extracts, 13 parts of fragrant eupatorium herb extracts, 8 parts of Tween-80s, 53 parts of maltodextrins.
Its preparation method, comprises the steps:
Above material is mixed according to the above ratio, stir 33min, then homogeneous 30min under the condition of 310Mpa, obtains emulsion; Controlling spraying drying condition is 165 ± 1 ℃ of EATs, 98 ℃ of temperature of outgoing airs, pump speed 8.2mL/min, air draft pressure 130Pa, intake: 1050L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.
embodiment 5
A plant resource weed killer herbicide pulvis, the weight portion of each component is:
20 parts of soapberry exosper extracts, 13 parts of cusp flower extracts, 13 parts of fragrant eupatorium herb extracts, 8 parts of Tween-80s, 55 parts of maltodextrins;
Its preparation method, comprises the steps:
Above material is mixed according to the above ratio, stir 33min, then homogeneous 30min under the condition of 310Mpa, obtains emulsion; Controlling spraying drying condition is 165 ± 1 ℃ of EATs, 98 ℃ of temperature of outgoing airs, pump speed 8.2mL/min, air draft pressure 130Pa, intake: 1053L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.

Claims (10)

1. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
15 ~ 20 parts of soapberry exosper extracts, 10 ~ 15 parts of cusp flower extracts, 10 ~ 15 parts of fragrant eupatorium herb extracts, 5 ~ 8 parts of Tween-80s, 50 ~ 55 parts of maltodextrins.
2. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
15 ~ 18 parts of soapberry exosper extracts, 10 ~ 13 parts of cusp flower extracts, 10 ~ 13 parts of fragrant eupatorium herb extracts, 6 ~ 8 parts of Tween-80s, 50 ~ 53 parts of maltodextrins.
3. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
15 ~ 18 parts of soapberry exosper extracts, 13 ~ 15 parts of cusp flower extracts, 10 ~ 13 parts of fragrant eupatorium herb extracts, 6 ~ 8 parts of Tween-80s, 53 ~ 55 parts of maltodextrins.
4. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
18 ~ 20 parts of soapberry exosper extracts, 13 ~ 15 parts of cusp flower extracts, 13 ~ 15 parts of fragrant eupatorium herb extracts, 6 ~ 8 parts of Tween-80s, 53 ~ 55 parts of maltodextrins.
5. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
18 ~ 20 parts of soapberry exosper extracts, 13 ~ 15 parts of cusp flower extracts, 13 ~ 15 parts of fragrant eupatorium herb extracts, 5 ~ 6 parts of Tween-80s, 53 ~ 55 parts of maltodextrins.
6. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
15 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 13 parts of fragrant eupatorium herb extracts, 6 parts of Tween-80s, 53 parts of maltodextrins.
7. a plant resource weed killer herbicide pulvis, is characterized in that: the weight portion of each component is:
20 parts of soapberry exosper extracts, 15 parts of cusp flower extracts, 15 parts of fragrant eupatorium herb extracts, 5 parts of Tween-80s, 55 parts of maltodextrins.
8. according to a kind of plant resource weed killer herbicide pulvis described in claim 1 ~ 7, it is characterized in that: the ethanol extract that described fragrant eupatorium herb extract is fragrant eupatorium herb.
9. a preparation method for plant resource weed killer herbicide pulvis, is characterized in that: comprise the following steps:
Above material is mixed according to the above ratio, stir 30 ~ 35min, then homogeneous 25 ~ 30min under the condition of 300 ~ 350Mpa, obtains emulsion; Controlling spraying drying condition is 165 ~ 163 ℃ of EATs, 98 ~ 101 ℃ of temperature of outgoing airs, pump speed 8.0 ~ 8.5mL/min, air draft pressure 100~150Pa, intake: 1050 ~ 1055L/h, and emulsion is carried out to spray drying treatment, obtains weed killer herbicide pulvis.
10. the preparation method of a kind of plant resource weed killer herbicide pulvis according to claim 9, is characterized in that: the ethanol extract that described fragrant eupatorium herb extract is fragrant eupatorium herb.
CN201310555253.0A 2013-11-11 2013-11-11 A kind of Botanical herbicide powder and preparation method thereof Expired - Fee Related CN103609599B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105028494A (en) * 2015-08-10 2015-11-11 云南师范大学 Chromolaena odorata-source water hyacinth growth regulating agent and preparation method
CN106719911A (en) * 2016-11-23 2017-05-31 广西大学 Herbicide of pest control weeds and preparation method thereof
CN106922746A (en) * 2017-01-22 2017-07-07 嵊州市派特普科技开发有限公司 A kind of herbicide for wooden land weeds and preparation method thereof
CN106993635A (en) * 2017-04-14 2017-08-01 广西大学 Weeding pulvis that a kind of Tillage conservation deteriorates and preparation method thereof

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Publication number Priority date Publication date Assignee Title
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CN102669187A (en) * 2012-05-25 2012-09-19 国际竹藤中心 Soluble powder of botanical herbicide and preparation method thereof
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Publication number Priority date Publication date Assignee Title
CN101218910A (en) * 2007-01-11 2008-07-16 深圳职业技术学院 Airplane grass microemulsion and preparation method thereof
KR20130011644A (en) * 2011-07-22 2013-01-30 전한택 Composition for controlling lawn-disease comprising plant extracts and vegetable oils as effective components
CN102669187A (en) * 2012-05-25 2012-09-19 国际竹藤中心 Soluble powder of botanical herbicide and preparation method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105028494A (en) * 2015-08-10 2015-11-11 云南师范大学 Chromolaena odorata-source water hyacinth growth regulating agent and preparation method
CN106719911A (en) * 2016-11-23 2017-05-31 广西大学 Herbicide of pest control weeds and preparation method thereof
CN106922746A (en) * 2017-01-22 2017-07-07 嵊州市派特普科技开发有限公司 A kind of herbicide for wooden land weeds and preparation method thereof
CN106993635A (en) * 2017-04-14 2017-08-01 广西大学 Weeding pulvis that a kind of Tillage conservation deteriorates and preparation method thereof

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Effective date of registration: 20150910

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Applicant after: NINGBO YUANFENG FIRE EQUIPMENT CO., LTD.

Address before: 525100, Zhanjiang, Guangdong province Huazhou city road under the Yin Guo Road, No. 3

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Address after: 221125 Gou Shan village, Tashan Town, Jiawang District, Xuzhou, Jiangsu

Patentee after: XUZHOU FENGRUN BIOLOGICAL ORGANIC FERTILIZER TECHNOLOGY DEVELOPMENT CO., LTD.

Address before: 315400 Zhengxiang village, low Tang street, Yuyao City, Ningbo, Zhejiang

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