CN103602515A - Production technology of grape seed oil for beauty treatment - Google Patents
Production technology of grape seed oil for beauty treatment Download PDFInfo
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- CN103602515A CN103602515A CN201310196100.1A CN201310196100A CN103602515A CN 103602515 A CN103602515 A CN 103602515A CN 201310196100 A CN201310196100 A CN 201310196100A CN 103602515 A CN103602515 A CN 103602515A
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- vitis viniferae
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Abstract
A production technology of grape seed oil for beauty treatment is characterized by comprising the following specific steps: (1) grape seed sorting; (2) pulverization treatment; (3) softening and enzymatic hydrolysis; (4) dehydration; (5) squeezing; (6) coarse filtration; (7) filtration; (8) finished product loading. The production technology has the following advantages: 1, the purity of grape seed oil is high; 2, the grape seed oil is rich in resveratrol, and the content of resveratrol is as high as 400 mg/L; 3, the technology is advanced and environment-friendly, and no solvent residue is left; 4, the resource of grape seed is fully utilized, the additional value of grape seed is increased, and the waste generated during the wine making process is recycled and utilized; 5, the technology does not affect the quality characteristics of grape seed oil, and the finish product is stable and uniform, meets the grape seed oil national standard examination (GB/T22478-2008), and is suitable for being used as base oil for skins, hairs, bathing, and massage.
Description
(1) technical field:
The present invention relates to raisin seed oil production technique field, particularly a kind of beauty treatment by the production technique of raisin seed oil.
(2) background technology:
Trans-resveratrol is a kind of degeneration-resistant material in vitis spp, and in grape, content is very high.Trans-resveratrol, as a kind of natural antioxidant, can reduce blood viscosity, anti-platelet clotting and vasorelaxation, keep unobstructed blood, generation and development that can preventing cancer, have atherosclerosis and coronary heart disease, ischemic heart disease, the preventive and therapeutic effect of hyperlipidemia.The effect that suppresses tumour also has estrogen-like effects, can be used for treating the diseases such as mammary cancer.Since the nineties in 20th century; China scientific worker deepens continuously to the research of trans-resveratrol; and disclose its pharmacological action: suppress the improper cohesion of thrombocyte; prevention myocardial infarction, cerebral embolism; anoxic heart is had to provide protection; burn or the cardiac output that causes of hemorrhagic shock are declined and have efficient recovery, and can expansion artery blood vessel and improve microcirculation.During the anti-ageing canon > of U.S. Ai Ermin Dare writing < < > in 1998, trans-resveratrol is classified as " 100 kinds of effective anti-ageing materials the most popular " it.
But the water-soluble and oil soluble of trans-resveratrol is very poor, water-soluble and oily hardly, its bioavailability is very low, has had a strong impact on its widespread use in every field.Therefore, existing explained hereafter raisin seed oil, is difficult to improve the content of trans-resveratrol in oil, if reach that people expect every day 2～10mg the best amount of trans-resveratrol, just need to obtain by other approach.
Raisin seed oil unsaturated fatty acid content reaches 92%, main component linoleic acid content is up to more than 80%, can reduce LDL in blood (low-density lipoprotein) cholesterol levels, improve HDL (high-density lipoprotein (HDL)) cholesterol, the ratio that reduces low density lipoprotein cholesterol and high density lipoprotein increasing cholesterol is the important method of prevention cardiovascular and cerebrovascular diseases.The daily edible peanut oil of people, wherein linoleic acid content is 30%～40%, and raisin seed oil is almost its twice.And contain 20 several mineral materials, and as calcium, zinc, iron, magnesium, copper, potassium, sodium, manganese, cobalt and various trace elements, multivitamin, vitamin A, E, D, K, P, particularly content of vitamin E is higher; In one soup ladle raisin seed oil, approximately contain one day required vitamin-E of people.Vitamin-E has good health-care effect to skin and muscle, and has the effect of beautifying face and moistering lotion.
In addition, pycnogenols (OPC) is one of effective ingredient of raisin seed oil, and OPC has strong antioxygenation, and its resistance of oxidation is vitamins C and vitamin-E 20～50 times, is efficient free-radical scavengers.OPC can suppress the peroxidation of lipid in human body, improves microvascular permeability. and it is conducive to the generation of collagen protein, makes skin flexible, reduces wrinkle, delaying human body skin aging, skin maintenance.And pycnogenols can intercept ultraviolet ray, increase capability of resistance to radiation, prevent the diseases relevant with free radical such as allergy, sacroiliitis, cataract, cancer, strengthening immunity.
Health-care effect due to raisin seed oil, it has the use history of more than 100 year in Europe, be used as baby, grownup's high-grade nutrient oil, working aloft person and pilot's high-class healthy oil, and be called and " eat the application of cosmetics ”，Dan China very few by domestic and international nutritionist and medical circle.
The production technique of tradition raisin seed oil is as follows: Semen Vitis viniferae sorting, and fragmentation, softening, dehydration, squeezing, filters finished product.In the production raisin seed oil of traditional technology, the content of trans-resveratrol cannot record, and the content of trans-resveratrol is subject to the impact of production process many factors, and trans-resveratrol cannot become small molecules and discharge from raw material position.
(3) summary of the invention:
The object of the present invention is to provide a kind of beauty treatment by the production technique of raisin seed oil.This process using fermented by biological enzyme technology is produced the raisin seed oil that is rich in trans-resveratrol, and Semen Vitis viniferae raw material is carried out to wind-force or manpower sorting, makes Semen Vitis viniferae substantially free from foreign meter.After fragmentation; softening process; add in right amount compound trans-resveratrol biological enzyme; improve leaching degree and the speed of polyphenol components trans-resveratrol in grape; protect trans-resveratrol not to be destroyed in subsequent process simultaneously, finally develop Resveratrol content and reach high-content of resveratrol raisin seed oil more than 400mg/L.
Technical scheme of the present invention: a kind of beauty treatment by the production technique of raisin seed oil, is characterized in that concrete steps are as follows:
(1) Semen Vitis viniferae sorting: select raw material Semen Vitis viniferae, sorting Semen Vitis viniferae is removed impurity;
(2) break process: use crusher in crushing Semen Vitis viniferae, form Semen Vitis viniferae particle, make Semen Vitis viniferae particle reach middle grain or particulate requirement;
(3) softening enzymolysis: be 12%～55% to adding water to moisture content in Semen Vitis viniferae particle, 30～120 minutes hold-times, 20 ℃～55 ℃ of temperature, reach softening; Add high-purity polygalacturonase 2～8g/100kg Semen Vitis viniferae, be incubated 18 ℃～42 ℃, enzymolysis 1～3 day;
(4) dehydration: fry base, the duration and degree of heating must be evenly, 80～120 ℃ of material temperatures, discharging moisture is 7%～15%, require non-burnt, fry saturating, 20～60 minutes time;
(5) squeezing: the thick 1～3mm that is controlled at of cake, moisture controlled 5%～10%;
(6) coarse filtration: use the filter cloth of 2～3 layers to carry out coarse filtration to oil product, remove oil cake slag foam;
(7) filter: the oil product after coarse filtration is filtered again, except deoiling middle solid impurity;
(8) finished product is filling.
In step described above (1), sorting Semen Vitis viniferae adopts wind-force or manpower.
Selection raw material Semen Vitis viniferae in step described above (1), its Semen Vitis viniferae derives from following grape variety, grape variety comprises Muscat Hamburg (Muscat Hamburg), Chardonney (Chardonnay), Sauvignon Blanc (Sauvignon blanc), Riesling (Riesling), Traminer (Gewurz-Traminer), Selillon (Semillon), Italian Riesling (Italian Riesling), Bai Yu (Rkatsiteli), general Li (Pinot Blanc), at least one in Chenin Blanc (Chenin Blanc).
Crusher in step described above (2) adopts single roller, two roller or multiroll crusher.
The Semen Vitis viniferae particle that makes in step described above (2) reaches middle grain or particulate requirement; middle grain is less than 30mm for the maximum particle diameter of particle; and the granule content that is wherein less than 20mm is no less than 85%; described particulate is that the maximum particle diameter of particle is less than 10mm, and the granule content that is wherein less than 2mm is no less than 95%.
High-purity polygalacturonase in the softening enzymolysis of step described above (3) is at least one in Lafase Press, Lafase Extract, Lafase Arom, Extralyse, Filtrozym, Lafase clarification, Optizym, Lafase Thermo.
High-purity polygalacturonase described above derives from French LAFFORT company.
Principle of work of the present invention: in raisin seed oil production process; by the pre-treatment of Semen Vitis viniferae process; suitably the high-purity polygalacturonase of allotment acts on Semen Vitis viniferae; the hydrolysis of resveratrol glucoside key discharges; improve leaching degree and the speed of polyphenol components trans-resveratrol in grape; protect trans-resveratrol not to be destroyed in subsequent process, drying and squeezing process are produced the raisin seed oil that is rich in trans-resveratrol simultaneously.
Superiority of the present invention: 1, raisin seed oil purity is high; 2, be rich in trans-resveratrol, its content is up to 400mg/L; 3, technique is advanced, there is no dissolvent residual, environmental protection; 4, make full use of Semen Vitis viniferae resource, increase the added value of Semen Vitis viniferae, the waste in recycle wine making process; 5, this technique does not affect the qualitative characteristics of end product raisin seed oil, and finished product stable and uniform, meets raisin seed oil national standard check (GB/T22478-2008), is applicable to the base oil of skin, hair, shower and massage.
(4) specific embodiments:
Embodiment 1: a kind of production technique of raisin seed oil (every liter contains the raisin seed oil that is greater than 100mg trans-resveratrol) for beauty treatment, is characterized in that concrete steps are as follows:
(1) Semen Vitis viniferae sorting: select raw material Semen Vitis viniferae, manpower sorting Semen Vitis viniferae is removed impurity;
(2) break process: with double roll crusher grape mass seed, form Semen Vitis viniferae particle, make Semen Vitis viniferae particle reach the requirement of middle grain, the maximum particle diameter of particle is less than 30mm, and the granule content that is wherein less than 20mm is no less than 85%;
(3) softening enzymolysis: be 45% to adding water to moisture content in Semen Vitis viniferae particle, 50 minutes hold-times, 35 ℃ of temperature, reach softening; Add high-purity polygalacturonase Lafase Press and Lafase clarification1:1 to mix, total amount is 3g/100kg Semen Vitis viniferae, is incubated 32 ℃, enzymolysis 1 day,
(4) dehydration: fry base, the duration and degree of heating must be evenly, 110 ℃ of material temperatures, discharging moisture is 9%, require non-burnt, fry saturating, 30 minutes time;
(5) squeezing: the thick 1.5mm that is controlled at of cake, moisture controlled 10%, squeezes;
(6) coarse filtration: use the filter cloth of 2 layers to carry out coarse filtration to oil product, remove oil cake slag foam;
(7) filter: the oil product after coarse filtration is filtered again, except deoiling middle solid impurity;
(8) finished product is filling.
Selection raw material Semen Vitis viniferae in step described above (1), its Semen Vitis viniferae derives from following grape variety, grape variety comprises Muscat Hamburg (Muscat Hamburg), Chardonney (Chardonnay), Sauvignon Blanc (Sauvignon blanc), at least one in Riesling (Riesling), Traminer (Gewurz-Traminer), Selillon (Semillon), Italian Riesling (Italian Riesling), Bai Yu (Rkatsiteli), general Li (Pinot Blanc) or Chenin Blanc (Chenin Blanc).
High-purity polygalacturonase described above derives from French LAFFORT company.
The censorship of raisin seed oil packing, with reference to national standard check: GB/T22478-2008
Raisin seed oil quality index
Embodiment 2: a kind of production technique of raisin seed oil (every liter contains the raisin seed oil that is greater than 400mg trans-resveratrol) for beauty treatment, is characterized in that concrete steps are as follows:
(1) Semen Vitis viniferae sorting: select raw material Semen Vitis viniferae, pneumatic separating Semen Vitis viniferae is removed impurity;
(2) break process: with double roll crusher grape mass seed, form Semen Vitis viniferae particle, make Semen Vitis viniferae particle reach particulate requirement, the maximum particle diameter of particle is less than 10mm, and the granule content that is less than 2mm is no less than 95%;
(3) softening enzymolysis: be 45% to adding water to moisture content in Semen Vitis viniferae particle, 50 minutes hold-times, 35 ℃ of temperature, reach softening; Add high-purity polygalacturonase Lafase Press, Lafase clarification, Optizym1:1:0.4 to mix, total amount is 5g/100kg Semen Vitis viniferae, is incubated 33 ℃, enzymolysis 2 days,
(4) dehydration: fry base, the duration and degree of heating must be evenly, 115 ℃ of material temperatures, discharging moisture is 11%, require non-burnt, fry saturating, 45 minutes time;
(5) squeezing: the thick 1.2mm that is controlled at of cake, moisture controlled 8.5%, squeezes;
(6) coarse filtration: use the filter cloth of 3 layers to carry out coarse filtration to oil product, remove oil cake slag foam;
(7) filter: the oil product after coarse filtration is filtered again, except deoiling middle solid impurity;
(8) finished product is filling.
Selection raw material Semen Vitis viniferae in step described above (1), its Semen Vitis viniferae derives from following grape variety, grape variety comprises Muscat Hamburg (Muscat Hamburg), Chardonney (Chardonnay), Sauvignon Blanc (Sauvignon blanc), at least one in Riesling (Riesling), Traminer (Gewurz-Traminer), Selillon (Semillon), Italian Riesling (Italian Riesling), Bai Yu (Rkatsiteli), general Li (Pinot Blanc) or Chenin Blanc (Chenin Blanc).
High-purity polygalacturonase described above derives from French LAFFORT company.
The censorship of raisin seed oil packing, with reference to national standard check: GB/T22478-2008
Raisin seed oil quality index
Embodiment 3: a kind of beauty treatment by the production technique of raisin seed oil, is characterized in that concrete steps are as follows:
(1) Semen Vitis viniferae sorting: select raw material Semen Vitis viniferae, manpower sorting Semen Vitis viniferae is removed impurity;
(2) break process: with single roll crusher grape mass seed, form Semen Vitis viniferae particle, make Semen Vitis viniferae particle reach the requirement of middle grain, the maximum particle diameter of particle is less than 30mm, and the granule content that is wherein less than 20mm is no less than 85%.
(3) softening enzymolysis: be 12% to adding water to moisture content in Semen Vitis viniferae particle, 30 minutes hold-times, 20 ℃ of temperature, reach softening; Add high-purity polygalacturonase Lafase Arom and Extralyse2:1 to mix, total amount is 2g/100kg Semen Vitis viniferae, is incubated 18 ℃, enzymolysis 1 day;
(4) dehydration: fry base, the duration and degree of heating must be evenly, 80 ℃ of material temperatures, discharging moisture is 7%, require non-burnt, fry saturating, 20 minutes time;
(5) squeezing: the thick 1mm that is controlled at of cake, moisture controlled 5%, squeezes;
(6) coarse filtration: use the filter cloth of 2 layers to carry out coarse filtration to oil product;
(7) filter: the oil product after coarse filtration is filtered again, except deoiling middle solid impurity;
(8) finished product is filling.
Selection raw material Semen Vitis viniferae in step described above (1), its Semen Vitis viniferae derives from following grape variety, grape variety comprises Muscat Hamburg (Muscat Hamburg), Chardonney (Chardonnay), Sauvignon Blanc (Sauvignon blanc), at least one in Riesling (Riesling), Traminer (Gewurz-Traminer), Selillon (Semillon), Italian Riesling (Italian Riesling), Bai Yu (Rkatsiteli), general Li (Pinot Blanc) or Chenin Blanc (Chenin Blanc).
High-purity polygalacturonase described above derives from French LAFFORT company.
Embodiment 4: a kind of beauty treatment by the production technique of raisin seed oil, is characterized in that concrete steps are as follows:
(1) Semen Vitis viniferae sorting: select raw material Semen Vitis viniferae, pneumatic separating Semen Vitis viniferae is removed impurity;
(2) break process: with multiroll crusher grape mass seed, form Semen Vitis viniferae particle, make Semen Vitis viniferae particle reach particulate requirement, the maximum particle diameter of particle is less than 10mm, and the granule content that is wherein less than 2mm is no less than 95%;
(3) softening enzymolysis: be 55% to adding water to moisture content in Semen Vitis viniferae particle, 120 minutes hold-times, 55 ℃ of temperature, reach softening; Add high-purity polygalacturonase Filtrozym, Optizym and Lafase Thermo1:1:0.4 to mix, total amount is 8g/100kg Semen Vitis viniferae, is incubated 42 ℃, enzymolysis 3 days;
(4) dehydration: fry base, the duration and degree of heating must be evenly, 120 ℃ of material temperatures, discharging moisture is 15%, require non-burnt, fry saturating, 60 minutes time;
(5) squeezing: the thick 3mm that is controlled at of cake, moisture controlled 10%, squeezes;
(6) coarse filtration: use the filter cloth of 3 layers to carry out coarse filtration to oil product;
(7) filter: the oil product after coarse filtration is filtered again, except deoiling middle solid impurity;
(8) finished product is filling.
Selection raw material Semen Vitis viniferae in step described above (1), its Semen Vitis viniferae derives from following grape variety, grape variety comprises Muscat Hamburg (Muscat Hamburg), Chardonney (Chardonnay), Sauvignon Blanc (Sauvignon blanc), at least one in Riesling (Riesling), Traminer (Gewurz-Traminer), Selillon (Semillon), Italian Riesling (Italian Riesling), Bai Yu (Rkatsiteli), general Li (Pinot Blanc) or Chenin Blanc (Chenin Blanc).
High-purity polygalacturonase described above derives from French LAFFORT company.
Claims (7)
1. improve looks by a production technique for raisin seed oil, it is characterized in that concrete steps are as follows:
(1) Semen Vitis viniferae sorting: select raw material Semen Vitis viniferae, sorting Semen Vitis viniferae is removed impurity;
(2) break process: use crusher in crushing Semen Vitis viniferae, form Semen Vitis viniferae particle, make Semen Vitis viniferae particle reach middle grain or particulate requirement;
(3) softening enzymolysis: be 12%～55% to adding water to moisture content in Semen Vitis viniferae particle, 30～120 minutes hold-times, 20 ℃～55 ℃ of temperature, reach softening; Add high-purity polygalacturonase 2～8g/100kg Semen Vitis viniferae, be incubated 18 ℃～42 ℃, enzymolysis 1～3 day;
(4) dehydration: fry base, the duration and degree of heating must be evenly, 80～120 ℃ of material temperatures, discharging moisture is 7%～15%, require non-burnt, fry saturating, 20～60 minutes time;
(5) squeezing: the thick 1～3mm that is controlled at of cake, moisture controlled 5%～10%;
(6) coarse filtration: use the filter cloth of 2～3 layers to carry out coarse filtration to oil product, remove oil cake slag foam;
(7) filter: the oil product after coarse filtration is filtered again, except deoiling middle solid impurity;
(8) finished product is filling.
2. a kind of beauty treatment used the production technique of raisin seed oil according to claim 1, it is characterized in that in described step (1), sorting Semen Vitis viniferae adopts wind-force or manpower.
3. a kind of beauty treatment used the production technique of raisin seed oil according to claim 1, it is characterized in that the selection raw material Semen Vitis viniferae in described step (1), its Semen Vitis viniferae derives from following grape variety, grape variety comprises Muscat Hamburg (Muscat Hamburg), Chardonney (Chardonnay), Sauvignon Blanc (Sauvignon blanc), Riesling (Riesling), Traminer (Gewurz-Traminer), Selillon (Semillon), Italian Riesling (Italian Riesling), Bai Yu (Rkatsiteli), general Li (Pinot Blanc), at least one in Chenin Blanc (Chenin Blanc).
4. a kind of beauty treatment used the production technique of raisin seed oil according to claim 1, it is characterized in that the crusher in described step (2) adopts single roller, two roller or multiroll crusher.
5. a kind of beauty treatment used the production technique of raisin seed oil according to claim 1; it is characterized in that the Semen Vitis viniferae particle that makes in described step (2) reaches middle grain or particulate requirement; middle grain is less than 30mm for the maximum particle diameter of particle; and the granule content that is wherein less than 20mm is no less than 85%; described particulate is that the maximum particle diameter of particle is less than 10mm, and the granule content that is wherein less than 2mm is no less than 95%.
6. a kind of beauty treatment used the production technique of raisin seed oil according to claim 1, it is characterized in that the high-purity polygalacturonase in the softening enzymolysis of described step (3) is at least one in Lafase Press, Lafase Extract, Lafase Arom, Extralyse, Filtrozym, Lafase clarification, Optizym, Lafase Thermo.
7. a kind of production technique of improving looks with raisin seed oil according to claim 6, is characterized in that described high-purity polygalacturonase derives from French LAFFORT company.
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| CN104017640A (en) * | 2014-06-30 | 2014-09-03 | 黄海英 | Processing technique for refining grape seed oil |
| CN109370771A (en) * | 2018-11-29 | 2019-02-22 | 乌鲁木齐上善元生物科技有限公司 | A kind of grape pip benevolence oil producing method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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Application publication date: 20140226 |