CN103599149A - Controllable preparation method of active pseudo-ginseng particle - Google Patents
Controllable preparation method of active pseudo-ginseng particle Download PDFInfo
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- CN103599149A CN103599149A CN201310575668.4A CN201310575668A CN103599149A CN 103599149 A CN103599149 A CN 103599149A CN 201310575668 A CN201310575668 A CN 201310575668A CN 103599149 A CN103599149 A CN 103599149A
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Abstract
The invention relates to a controllable preparation method of an active pseudo-ginseng particle and belongs to the technical field of pseudo-ginseng processing technologies. The controllable preparation method of the active pseudo-ginseng particle comprises five steps of per-treatment, pre-freezing, sublimation drying, resolving, and discharging and packing; in the method, a modern sensor technology and a freeze-drying technology are combined, the temperature and the humidity can be accurately controlled in the processing process; the time is not required to be set, the freezing process and the heating process are carried out in an intermittent manner; energy is saved, the active ingredients of active pseudo-ginseng particles treated by adopting the method can not be damaged, the reconstitution property is good, the crushing is easy, the shelf life is long, and simultaneously the method is simple, high in practicability and suitable for large-scale production.
Description
Technical field
The present invention relates to a kind of controlled method for preparing active pseudo-ginseng granule, belong to Radix Notoginseng technology field.
Background technology
The rare Chinese medicine that Radix Notoginseng ，Shi China is traditional.Except thering is the medicinal efficacies such as blood circulation promoting and blood stasis dispelling, hemostasia and detumescence, modern study shows---Radix Notoginseng also has the physiological hygiene function widely such as defying age, resisting fatigue, atherosclerosis, antitumor, blood pressure lowering, blood sugar lowering, tranquillizing and allaying excitement, enhancing immunity and beauty treatment, is a kind of health food resource that has very much exploitation to be worth.
Due to the unique significantly effect of Radix Notoginseng, constantly expanded purposes, health care, chemical industry, medical consumption continue to rise, and especially China enters the cardiovascular and cerebrovascular disease high-incidence season, and relevant research and development product emerges in an endless stream, and demand is huge.Radix Notoginseng, as rare Chinese medicine, is found through modern scientific research, adopts the Radix Notoginseng processing method of traditional Exposure to Sunlight or baking very easily to destroy its saponin including and volatile oil isoreactivity composition, affects medical value and the curative effect of Radix Notoginseng, causes the waste of resource; Meanwhile, because the Radix Notoginseng that processing obtains is too hard, be difficult to pulverize, cause family, the personal inconvenience of individual, and mouthfeel be too bitter, has restricted applying of its health care.Traditional processing mode, can cause the active component failure loss in Radix Notoginseng besides, causes the wasting of resources, and end product quality declines.
And fresh Radix Notoginseng owing to preserving difficulty, and cannot directly be used; At present, also there are some patents to adopt cryodesiccated method processing fresh Radix Notoginseng, yet, in the course of processing, need the time in man-hour longer, resolution temperature is up to 120 ℃, " Active pseudo-ginseng " prepared at this temperature is difficult to keep the primary activity of fresh Radix Notoginseng, and can cause the coking of Radix Notoginseng, in addition, in the course of processing, temperature and humidity is wayward, often adopts the method for range estimation or sets longer time, accurately controlled working process, simultaneously, also cause the huge waste of resource, it is very inconvenient to the course of processing, to bring, and has a strong impact on product quality.
Summary of the invention
For the problems referred to above, the object of the present invention is to provide a kind of controlled method for preparing active pseudo-ginseng granule, adopt Modern Transducer Technology to combine with freeze drying technology, the temperature and humidity of accurate controlled working process, without setting-up time, refrigerating process and heating process adopt batch (-type) to carry out, energy savings, the active component that the active pseudo-ginseng granule of processing through this method contains is not destroyed, and rehydration is good, easily pulverize, long shelf-life, meanwhile, this method is simple, practical, be applicable to large-scale production.
Method for preparing active pseudo-ginseng of the present invention is comprised of following steps: a kind of controlled method for preparing active pseudo-ginseng granule, carries out according to step below:
One, pre-treatment: the fresh Radix Notoginseng after excavating, through sorting, pick, by after the appended clip of fresh Radix Notoginseng, fibrous root, floss root segregation excision, obtain Radix Notoginseng main root, clean and remove surface attachments, drain surface moisture, make section, select non-standard, incomplete relic or the bar root of fresh Radix Notoginseng, blended into muddy, muddy thickness is 3-5 millimeter, by needle-like Temperature Humidity Sensor in Radix Notoginseng mud;
Two, precooling: first, material ambient temperature is set as to 40-50 ℃, adopts batch (-type) refrigeration, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud inside is monitored; Under cryogenic conditions, Radix Notoginseng mud becomes solid, and when Radix Notoginseng mud central temperature reaches 20-25 ℃, precooling process finishes;
Three, sublimation drying: by the good Radix Notoginseng mud solids of precooling, pave and be positioned on the platform dish of being made by Heat Conduction Material, layer thickness is controlled at 1.5-5cm, moves to vacuum drying indoor; After airtight, start evacuation, keep internal vacuum pressure 30～70 handkerchiefs, heating process adopts batch (-type) to carry out, and, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud solids inside is monitored meanwhile; First, set temperature is 0 ℃; When Radix Notoginseng mud solids central temperature reaches 0 ℃, adjust temperature setting, increase to 20 ℃; When Radix Notoginseng mud solids central temperature reaches 20 ℃, again adjust temperature setting, increase to 40 ℃; Until Radix Notoginseng mud solids central temperature reaches 40 ℃, sublimation process finishes;
Four, resolve: keeping platform dish temperature is 40 ℃, continue to the heat supply of platform dish and, simultaneously, further reduce vacuum, in sublimation process, utilize Temperature Humidity Sensor to detect the moisture of Radix Notoginseng mud solids, until material moisture is while reaching 5%～10%, resolving finishes;
Five, discharging packing: after parsing finishes, stop heating, discharging after discharge vacuum, sieve goes after fine powder, and filling bag is dressed up the form of teabag, then packs with gift box.
Described Temperature Humidity Sensor adopts horizontal and vertical being staggered, and the spacing between adjacent Temperature Humidity Sensor is 2-5 millimeter.
Beneficial effect of the present invention: this method adopts Modern Transducer Technology to combine with freeze drying technology, and the temperature and humidity of accurate controlled working process, without setting-up time, refrigerating process and heating process adopt batch (-type) to carry out, energy savings, the active component that the active pseudo-ginseng granule of processing through this method contains is not destroyed, and rehydration is good, easily pulverize, long shelf-life, meanwhile, this method is simple, practical, be applicable to large-scale production.
Accompanying drawing explanation
Fig. 1 is the flow chart of this method.
The specific embodiment
Below in conjunction with accompanying drawing, the present invention will be further described, to facilitate the technical staff to understand.
As shown in Figure 1: a kind of controlled method for preparing active pseudo-ginseng granule, carries out according to step below:
One, pre-treatment: the fresh Radix Notoginseng after excavating, through sorting, pick, by after the appended clip of fresh Radix Notoginseng, fibrous root, floss root segregation excision, obtain Radix Notoginseng main root, clean and remove surface attachments, drain surface moisture, make section, select non-standard, incomplete relic or the bar root of fresh Radix Notoginseng, blended into muddy, muddy thickness is 3-5 millimeter, by needle-like Temperature Humidity Sensor in Radix Notoginseng mud;
Two, precooling: first, material ambient temperature is set as to 40-50 ℃, adopts batch (-type) refrigeration, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud inside is monitored; Under cryogenic conditions, Radix Notoginseng mud becomes solid, and when Radix Notoginseng mud central temperature reaches 20-25 ℃, precooling process finishes;
Three, sublimation drying: by the good Radix Notoginseng mud solids of precooling, pave and be positioned on the platform dish of being made by Heat Conduction Material, layer thickness is controlled at 1.5-5cm, moves to vacuum drying indoor; After airtight, start evacuation, keep internal vacuum pressure 30～70 handkerchiefs, heating process adopts batch (-type) to carry out, and, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud solids inside is monitored meanwhile; First, set temperature is 0 ℃; When Radix Notoginseng mud solids central temperature reaches 0 ℃, adjust temperature setting, increase to 20 ℃; When Radix Notoginseng mud solids central temperature reaches 20 ℃, again adjust temperature setting, increase to 40 ℃; Until Radix Notoginseng mud solids central temperature reaches 40 ℃, sublimation process finishes;
Four, resolve: keeping platform dish temperature is 40 ℃, continue to the heat supply of platform dish and, simultaneously, further reduce vacuum, in sublimation process, utilize Temperature Humidity Sensor to detect the moisture of Radix Notoginseng mud solids, until material moisture is while reaching 5%～10%, resolving finishes;
Five, discharging packing: after parsing finishes, stop heating, discharging after discharge vacuum, sieve goes after fine powder, and filling bag is dressed up the form of teabag, then packs with gift box.
For Measurement accuracy, described Temperature Humidity Sensor can adopt horizontal and vertical being staggered, and the spacing between adjacent Temperature Humidity Sensor is 2-5 millimeter.
Embodiment 1:
A controlled method for preparing active pseudo-ginseng granule, carries out according to step below:
One, pre-treatment: the fresh Radix Notoginseng after excavating, through sorting, pick, by after the appended clip of fresh Radix Notoginseng, fibrous root, floss root segregation excision, obtain Radix Notoginseng main root, clean and remove surface attachments, drain surface moisture, make section, select non-standard, incomplete relic or the bar root of fresh Radix Notoginseng, blended into muddy, muddy thickness is 3 millimeters, by needle-like Temperature Humidity Sensor in Radix Notoginseng mud; For Measurement accuracy, described Temperature Humidity Sensor can adopt horizontal and vertical being staggered, and the spacing between adjacent Temperature Humidity Sensor is 2 millimeters;
Two, precooling: first, material ambient temperature is set as to 40 ℃, adopts batch (-type) refrigeration, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud inside is monitored; Under cryogenic conditions, Radix Notoginseng mud becomes solid, and when Radix Notoginseng mud central temperature reaches 20 ℃, precooling process finishes;
Three, sublimation drying: by the good Radix Notoginseng mud solids of precooling, pave and be positioned on the platform dish of being made by Heat Conduction Material, layer thickness is controlled at 1.5cm, moves to vacuum drying indoor; After airtight, start evacuation, keep internal vacuum pressure 30 handkerchiefs, heating process adopts batch (-type) to carry out, and, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud solids inside is monitored meanwhile; First, set temperature is 0 ℃; When Radix Notoginseng mud solids central temperature reaches 0 ℃, adjust temperature setting, increase to 20 ℃; When Radix Notoginseng mud solids central temperature reaches 20 ℃, again adjust temperature setting, increase to 40 ℃; Until Radix Notoginseng mud solids central temperature reaches 40 ℃, sublimation process finishes;
Four, resolve: keeping platform dish temperature is 40 ℃, continue to the heat supply of platform dish and, simultaneously, further reduce vacuum, in sublimation process, utilize Temperature Humidity Sensor to detect the moisture of Radix Notoginseng mud solids, until material moisture is while reaching 5%, resolving finishes;
Five, discharging packing: after parsing finishes, stop heating, discharging after discharge vacuum, sieve goes after fine powder, and filling bag is dressed up the form of teabag, then packs with gift box.
Embodiment 2:
A controlled method for preparing active pseudo-ginseng granule, carries out according to step below:
One, pre-treatment: the fresh Radix Notoginseng after excavating, through sorting, pick, by after the appended clip of fresh Radix Notoginseng, fibrous root, floss root segregation excision, obtain Radix Notoginseng main root, clean and remove surface attachments, drain surface moisture, make section, select non-standard, incomplete relic or the bar root of fresh Radix Notoginseng, blended into muddy, muddy thickness is 5 millimeters, by needle-like Temperature Humidity Sensor in Radix Notoginseng mud; For Measurement accuracy, described Temperature Humidity Sensor can adopt horizontal and vertical being staggered, and the spacing between adjacent Temperature Humidity Sensor is 5 millimeters;
Two, precooling: first, material ambient temperature is set as to 50 ℃, adopts batch (-type) refrigeration, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud inside is monitored; Under cryogenic conditions, Radix Notoginseng mud becomes solid, and when Radix Notoginseng mud central temperature reaches 25 ℃, precooling process finishes;
Three, sublimation drying: by the good Radix Notoginseng mud solids of precooling, pave and be positioned on the platform dish of being made by Heat Conduction Material, layer thickness is controlled at 5cm, moves to vacuum drying indoor; After airtight, start evacuation, keep internal vacuum pressure 70 handkerchiefs, heating process adopts batch (-type) to carry out, and, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud solids inside is monitored meanwhile; First, set temperature is 0 ℃; When Radix Notoginseng mud solids central temperature reaches 0 ℃, adjust temperature setting, increase to 20 ℃; When Radix Notoginseng mud solids central temperature reaches 20 ℃, again adjust temperature setting, increase to 40 ℃; Until Radix Notoginseng mud solids central temperature reaches 40 ℃, sublimation process finishes;
Four, resolve: keeping platform dish temperature is 40 ℃, continue to the heat supply of platform dish and, simultaneously, further reduce vacuum, in sublimation process, utilize Temperature Humidity Sensor to detect the moisture of Radix Notoginseng mud solids, until material moisture is while reaching 10%, resolving finishes;
Five, discharging packing: after parsing finishes, stop heating, discharging after discharge vacuum, sieve goes after fine powder, and filling bag is dressed up the form of teabag, then packs with gift box.
Embodiment 3:
A controlled method for preparing active pseudo-ginseng granule, carries out according to step below:
One, pre-treatment: the fresh Radix Notoginseng after excavating, through sorting, pick, by after the appended clip of fresh Radix Notoginseng, fibrous root, floss root segregation excision, obtain Radix Notoginseng main root, clean and remove surface attachments, drain surface moisture, make section, select non-standard, incomplete relic or the bar root of fresh Radix Notoginseng, blended into muddy, muddy thickness is 4 millimeters, by needle-like Temperature Humidity Sensor in Radix Notoginseng mud; For Measurement accuracy, described Temperature Humidity Sensor can adopt horizontal and vertical being staggered, and the spacing between adjacent Temperature Humidity Sensor is 3 millimeters;
Two, precooling: first, material ambient temperature is set as to 45 ℃, adopts batch (-type) refrigeration, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud inside is monitored; Under cryogenic conditions, Radix Notoginseng mud becomes solid, and when Radix Notoginseng mud central temperature reaches 23 ℃, precooling process finishes;
Three, sublimation drying: by the good Radix Notoginseng mud solids of precooling, pave and be positioned on the platform dish of being made by Heat Conduction Material, layer thickness is controlled at 3cm, moves to vacuum drying indoor; After airtight, start evacuation, keep internal vacuum pressure 50 handkerchiefs, heating process adopts batch (-type) to carry out, and, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud solids inside is monitored meanwhile; First, set temperature is 0 ℃; When Radix Notoginseng mud solids central temperature reaches 0 ℃, adjust temperature setting, increase to 20 ℃; When Radix Notoginseng mud solids central temperature reaches 20 ℃, again adjust temperature setting, increase to 40 ℃; Until Radix Notoginseng mud solids central temperature reaches 40 ℃, sublimation process finishes;
Four, resolve: keeping platform dish temperature is 40 ℃, continue to the heat supply of platform dish and, simultaneously, further reduce vacuum, in sublimation process, utilize Temperature Humidity Sensor to detect the moisture of Radix Notoginseng mud solids, until material moisture is while reaching 8%, resolving finishes;
Five, discharging packing: after parsing finishes, stop heating, discharging after discharge vacuum, sieve goes after fine powder, and filling bag is dressed up the form of teabag, then packs with gift box.
comparative tests:
The Radix Notoginseng of choosing the fresh Radix Notoginseng of processing through this method and common fresh Radix Notoginseng, conventional process compares: saponin constituent Rg1, Rb1, the R1 content of Active pseudo-ginseng are respectively 3.73%, 3.26%, 1.13%, and saponin constituent Rg1, the Rb1 of the dry Radix Notoginseng of traditional drying, R1 content are respectively 2.64%, 2.16%, 0.69%.By relatively drawing: saponin constituent Rg1, the Rb1 in the fresh Radix Notoginseng of processing through this method, the Radix Notoginseng that R1 content is crossed apparently higher than conventional process.
Active pseudo-ginseng has following characteristics: active ingredient loss is few, and mode of appearance is substantially constant, and abnormal smells from the patient color and luster is substantially constant, and tissue looseness easily pulverizes, and rehydration is well easily soaked, and mouthfeel suitable (sweetness and bitterness Hui Tian) is easily accepted, the low easy preservation of moisture content.Therefore, Active pseudo-ginseng can replace fresh goods Radix Notoginseng to use.
The present invention be take fresh Radix Notoginseng as raw material, to fresh Radix Notoginseng, carry out freezing, Radix Notoginseng main root is refrigerated to below the eutectic point of-25 ℃, moisture freezes in fresh Radix Notoginseng is become after ice crystal (solid-state), evacuation under cryogenic conditions again, allow ice crystal be directly sublimed into gaseous state and take away, reach the object of dehydrate.Make the heat-sensitive materials in Radix Notoginseng can degeneration, its physics, chemistry, biological characteristics etc. can be retained to greatest extent, therefore, have had advantages of that other drying meanss are incomparable.
The Radix Notoginseng that this method obtains, has high activity component content and low water content, the easy characteristic of easily pulverizing of preserving, and by the appellation with " Active pseudo-ginseng " of hat.
This method adopts Modern Transducer Technology to combine with freeze drying technology, and the temperature and humidity of accurate controlled working process, without setting-up time, refrigerating process and heating process adopt batch (-type) to carry out, energy savings, the active component that the active pseudo-ginseng granule of processing through this method contains is not destroyed, and rehydration is good, easily pulverize, long shelf-life, meanwhile, this method is simple, practical, be applicable to large-scale production.
The present invention describes by accompanying drawing, without departing from the present invention, can also carry out various conversion and be equal to replacement patent of the present invention, therefore, patent of the present invention is not limited to disclosed specific implementation process, and should comprise the whole embodiments that fall within the scope of Patent right requirement of the present invention.
Claims (2)
1. a controlled method for preparing active pseudo-ginseng granule, is characterized in that: a kind of controlled method for preparing active pseudo-ginseng carries out according to step below:
One, pre-treatment: the fresh Radix Notoginseng after excavating, through sorting, pick, by after the appended clip of fresh Radix Notoginseng, fibrous root, floss root segregation excision, obtain Radix Notoginseng main root, clean and remove surface attachments, drain surface moisture, make section, select non-standard, incomplete relic or the bar root of fresh Radix Notoginseng, blended into muddy, muddy thickness is 3-5 millimeter, by needle-like Temperature Humidity Sensor in Radix Notoginseng mud;
Two, precooling: first, material ambient temperature is set as to 40-50 ℃, adopts batch (-type) refrigeration, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud inside is monitored; Under cryogenic conditions, Radix Notoginseng mud becomes solid, and when Radix Notoginseng mud central temperature reaches 20-25 ℃, precooling process finishes;
Three, sublimation drying: by the good Radix Notoginseng mud solids of precooling, pave and be positioned on the platform dish of being made by Heat Conduction Material, layer thickness is controlled at 1.5-5cm, moves to vacuum drying indoor; After airtight, start evacuation, keep internal vacuum pressure 30～70 handkerchiefs, heating process adopts batch (-type) to carry out, and, by Temperature Humidity Sensor, the temperature of Radix Notoginseng mud solids inside is monitored meanwhile; First, set temperature is 0 ℃; When Radix Notoginseng mud solids central temperature reaches 0 ℃, adjust temperature setting, increase to 20 ℃; When Radix Notoginseng mud solids central temperature reaches 20 ℃, again adjust temperature setting, increase to 40 ℃; Until Radix Notoginseng mud solids central temperature reaches 40 ℃, sublimation process finishes;
Four, resolve: keeping platform dish temperature is 40 ℃, continue to the heat supply of platform dish and, simultaneously, further reduce vacuum, in sublimation process, utilize Temperature Humidity Sensor to detect the moisture of Radix Notoginseng mud solids, until material moisture is while reaching 5%～10%, resolving finishes;
Five, discharging packing: after parsing finishes, stop heating, discharging after discharge vacuum, sieve goes after fine powder, and filling bag is dressed up the form of teabag, then packs with gift box.
2. according to a kind of controlled method for preparing active pseudo-ginseng granule described in claim 1, it is characterized in that, described Temperature Humidity Sensor adopts horizontal and vertical being staggered, and the spacing between adjacent Temperature Humidity Sensor is 2-5 millimeter.
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| CN109619555A (en) * | 2018-12-20 | 2019-04-16 | 丁传波 | A kind of preparation method and production technology of fresh Radix Notoginseng powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109619555A (en) * | 2018-12-20 | 2019-04-16 | 丁传波 | A kind of preparation method and production technology of fresh Radix Notoginseng powder |
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Owner name: YUNNAN HAONONGFU AGRICULTURE DEVELOPMENT CO., LTD. Free format text: FORMER OWNER: YUNNAN TONGGEN PSEUDO GINSENG INDUSTRY CO., LTD. Effective date: 20140509 |
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Effective date of registration: 20140509 Address after: 663000, Yunnan province Wenshan Kaihua South Road treasure big business exchange 11 group 1, No. 1, third floor facade Applicant after: Yunnan good farmers agricultural development Co., Ltd. Applicant after: WENSHAN SANQI RESEARCH INSTITUTE, WENSHAN UNIVERSITY Address before: 663000, Wenshan Zhuang and Miao Autonomous Prefecture of Wenshan province Yunnan civilized South Road treasure industry big business exchange 11 group 1, No. 1 Applicant before: YUNNAN TONGGEN SANQI INDUSTRY CO., LTD. Applicant before: WENSHAN SANQI RESEARCH INSTITUTE, WENSHAN UNIVERSITY |
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