CN103589333B - A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof - Google Patents
A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof Download PDFInfo
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- CN103589333B CN103589333B CN201310474813.XA CN201310474813A CN103589333B CN 103589333 B CN103589333 B CN 103589333B CN 201310474813 A CN201310474813 A CN 201310474813A CN 103589333 B CN103589333 B CN 103589333B
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- 238000000576 coating method Methods 0.000 title claims abstract description 21
- 239000011248 coating agent Substances 0.000 title claims abstract description 20
- 230000005855 radiation Effects 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims description 10
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 39
- 239000000843 powder Substances 0.000 claims abstract description 33
- -1 dioctyl ester Chemical class 0.000 claims abstract description 10
- QOHMWDJIBGVPIF-UHFFFAOYSA-N n',n'-diethylpropane-1,3-diamine Chemical compound CCN(CC)CCCN QOHMWDJIBGVPIF-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910017083 AlN Inorganic materials 0.000 claims abstract description 9
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000000919 ceramic Substances 0.000 claims abstract description 9
- 239000010445 mica Substances 0.000 claims abstract description 9
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 9
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 9
- 229920002050 silicone resin Polymers 0.000 claims abstract description 9
- 239000010455 vermiculite Substances 0.000 claims abstract description 9
- 229910052902 vermiculite Inorganic materials 0.000 claims abstract description 9
- 235000019354 vermiculite Nutrition 0.000 claims abstract description 9
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims abstract description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 7
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 7
- 238000004581 coalescence Methods 0.000 claims abstract description 7
- 150000002334 glycols Chemical class 0.000 claims abstract description 7
- 239000002105 nanoparticle Substances 0.000 claims abstract description 7
- 229920000570 polyether Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims abstract description 4
- GHKOFFNLGXMVNJ-UHFFFAOYSA-N Didodecyl thiobispropanoate Chemical compound CCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCC GHKOFFNLGXMVNJ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 4
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 4
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 4
- 229940095064 tartrate Drugs 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 21
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 9
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 6
- 239000010977 jade Substances 0.000 claims description 6
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 6
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 6
- 229960003656 ricinoleic acid Drugs 0.000 claims description 6
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 6
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 229910052731 fluorine Inorganic materials 0.000 claims description 3
- 239000011737 fluorine Substances 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000005502 peroxidation Methods 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- VXHFNALHLRWIIU-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropanoate Chemical compound CC(C)(C)OC(=O)C(C)(C)C VXHFNALHLRWIIU-UHFFFAOYSA-N 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 239000008096 xylene Substances 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 230000017525 heat dissipation Effects 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 229910021392 nanocarbon Inorganic materials 0.000 abstract description 2
- 230000032683 aging Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
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- Application Of Or Painting With Fluid Materials (AREA)
Abstract
For an emitting far-infrared heat radiation coating for meter housing, be made up of the raw material of following weight part: silicone resin 50-54, diethyl amino propylamine? DEAPA? 4-5, nano-sized carbon 2-3, aluminium nitride 12-15, vinyl cyanide 6-8, nano far infrared ceramic powder 4-6, silicon carbide 1-2, nanometer vermiculite powder 1-2, nano mica powder 1-2, dibutyl tin laurate 2-3, dioctyl ester 1-2, polyether Glycols 1-2, tartrate 1-2, ethyl acetate 24-26, anti-oxidant DLTP? 1-2, film coalescence aid 4-5.The present invention is by adding aluminium nitride, silicon carbide, and heat conduction rate is high, good heat dissipation effect; By adding nano far infrared ceramic powder, nanometer vermiculite powder, nano mica powder, Nano carbon, this coating is also made to have emitting far-infrared function while adding thermal diffusivity, useful HUMAN HEALTH; This coating uses silicone resin as base material, has excellent thermo-oxidative stability.
Description
Technical field
The invention belongs to technical field of coatings, relate to a kind of heat radiation coating, more particularly, is a kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof.
Background technology
Along with science and technology progress, all kinds of instrument is also arisen at the historic moment, and the heat that instrument is distributed generally can not be very fast, but because instrument can long term operation, put aside a lot of heat, if distribute heat not in time, instrument can be caused overheated, and impact normally works, and also easily damages.Coating design for the performance characteristics of instrument is at present fewer, and can not meet the requirement of productive life, heat dissipation problem is also just more and more focused on by people.There is heatproof and ageing-resistant poor and little to substrate bonding power, the not good and unhandy technical problem of radiating effect in the material that current instrument heat radiation coating uses, is difficult to the requirement meeting heat radiation.
Summary of the invention
The object of this invention is to provide a kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof, it is large that coating of the present invention has cohesive force, the advantage that ageing-resistant, heat extraction coefficient is large.
The technical solution adopted in the present invention is:
For an emitting far-infrared heat radiation coating for meter housing, it is characterized in that being made up of the raw material of following weight part: silicone resin 50-54, diethyl amino propylamine DEAPA4-5, nano-sized carbon 2-3, aluminium nitride 12-15, vinyl cyanide 6-8, nano far infrared ceramic powder 4-6, silicon carbide 1-2, nanometer vermiculite powder 1-2, nano mica powder 1-2, dibutyl tin laurate 2-3, dioctyl ester 1-2, polyether Glycols 1-2, tartrate 1-2, ethyl acetate 24-26, anti-oxidant DLTP 1-2, film coalescence aid 4-5;
Described film coalescence aid is obtained by the raw material of following weight part: nanometer jade powder 2-4, linking agent TAC2-3, alcohol ester 12 4-5, Silane coupling agent KH550 1-2, vinylbenzene 3-4, ricinolic acid 1-2, MALEIC ANHYDRIDE 2-3, morpholine 2-3, peroxidation trimethylacetic acid tert-butyl ester 0.3-0.4, different fluorine that ketone 1-2, dimethylbenzene 4-5, ethyl acetate 12-13; Preparation method is: by nanometer jade powder, morpholine, vinylbenzene, ricinolic acid mixing, join in ethyl acetate and xylene mixture solvent, stir 5-10 minute, be heated to 65-70 DEG C, under 800-1200 rev/min, stir 15-30 minute, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 15-30 minute, add other remaining component again, stirring reaction 45-60 minute, to obtain final product.
The preparation method of the described emitting far-infrared heat radiation coating for meter housing, it is characterized in that comprising the following steps: by ethyl acetate, polyether Glycols, nano-sized carbon, aluminium nitride, nano far infrared ceramic powder, silicon carbide, nanometer vermiculite powder, nano mica powder mixes, be heated to 50-60 DEG C, 1100-1600 rev/min of lower stirring reaction 30-40 minute, then, be warming up to 70-80 DEG C, add silicone resin, diethyl amino propylamine DEAPA, vinyl cyanide, dibutyl tin laurate, continue to stir 30-40 minute, add other remaining component again, continue stirring reaction 60-80 minute, grinding obtains slurry, obtain.
Beneficial effect of the present invention
The present invention is by adding aluminium nitride, silicon carbide, and heat conduction rate is high, good heat dissipation effect; By adding nano far infrared ceramic powder, nanometer vermiculite powder, nano mica powder, Nano carbon, also make this coating have emitting far-infrared function while adding thermal diffusivity, useful HUMAN HEALTH, and oilness is good, easily constructs; Improve can opening effect, not stratified; This coating uses silicone resin as base material, and good insulating has excellent thermo-oxidative stability.
Embodiment
For an emitting far-infrared heat radiation coating for meter housing, it is characterized in that being made up of the raw material of following weight part: silicone resin 52, diethyl amino propylamine DEAPA4, nano-sized carbon 2, aluminium nitride 13, vinyl cyanide 7, nano far infrared ceramic powder 5, silicon carbide 1, nanometer vermiculite powder 1, nano mica powder 1, dibutyl tin laurate 2, dioctyl ester 1, polyether Glycols 1, tartrate 1, ethyl acetate 25, anti-oxidant DLTP 1, film coalescence aid 4;
Described film coalescence aid is obtained by the raw material of following weight part (kilogram): nanometer jade powder 3, linking agent TAC2, alcohol ester 12, Silane coupling agent KH550 1, vinylbenzene 3, ricinolic acid 1, MALEIC ANHYDRIDE 2, morpholine 2, the peroxidation trimethylacetic acid tert-butyl ester 0.3, different fluorine that ketone 1, dimethylbenzene 4, ethyl acetate 12; Preparation method is: by nanometer jade powder, morpholine, vinylbenzene, ricinolic acid mixing, join in ethyl acetate and xylene mixture solvent, stir 8 minutes, be heated to 65 DEG C, stir 20 minutes under 1000 revs/min, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 20 minutes, add other remaining component again, stirring reaction 50 minutes, to obtain final product.
The preparation method of the described emitting far-infrared heat radiation coating for meter housing, it is characterized in that comprising the following steps: by ethyl acetate, polyether Glycols, nano-sized carbon, aluminium nitride, nano far infrared ceramic powder, silicon carbide, nanometer vermiculite powder, nano mica powder mixes, be heated to 55 DEG C, 1300 revs/min of lower stirring reactions 30 minutes, then, be warming up to 75 DEG C, add silicone resin, diethyl amino propylamine DEAPA, vinyl cyanide, dibutyl tin laurate, continue stirring 35 minutes, add other remaining component again, continue stirring reaction 70 minutes, grinding obtains slurry, obtain.
Coating of the present invention is applied on meter housing, artificial accelerated aging test under 80 DEG C and 300W ultraviolet light irradiation condition, 5000 hours ageing-resistant time, heatproof high temperature 285 DEG C, bonding shearing force 19MPa., thermal conductivity 250W/(mK).
Claims (2)
1. for an emitting far-infrared heat radiation coating for meter housing, it is characterized in that being made up of the raw material of following weight part: silicone resin 50-54, diethylaminopropylamine 4-5, nano-sized carbon 2-3, aluminium nitride 12-15, vinyl cyanide 6-8, nano far infrared ceramic powder 4-6, silicon carbide 1-2, nanometer vermiculite powder 1-2, nano mica powder 1-2, dibutyl tin laurate 2-3, dioctyl ester 1-2, polyether Glycols 1-2, tartrate 1-2, ethyl acetate 24-26, anti-oxidant DLTP 1-2, film coalescence aid 4-5;
Described film coalescence aid is obtained by the raw material of following weight part: nanometer jade powder 2-4, linking agent TAC2-3, alcohol ester 12 4-5, Silane coupling agent KH550 1-2, vinylbenzene 3-4, ricinolic acid 1-2, MALEIC ANHYDRIDE 2-3, morpholine 2-3, peroxidation trimethylacetic acid tert-butyl ester 0.3-0.4, different fluorine that ketone 1-2, dimethylbenzene 4-5, ethyl acetate 12-13; Preparation method is: by nanometer jade powder, morpholine, vinylbenzene, ricinolic acid mixing, join in ethyl acetate and xylene mixture solvent, stir 5-10 minute, be heated to 65-70 DEG C, under 800-1200 rev/min, stir 15-30 minute, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 15-30 minute, add other remaining component again, stirring reaction 45-60 minute, to obtain final product.
2. the preparation method of the emitting far-infrared heat radiation coating for meter housing according to claim 1, it is characterized in that comprising the following steps: by ethyl acetate, polyether Glycols, nano-sized carbon, aluminium nitride, nano far infrared ceramic powder, silicon carbide, nanometer vermiculite powder, nano mica powder mixes, be heated to 50-60 DEG C, 1100-1600 rev/min of lower stirring reaction 30-40 minute, then, be warming up to 70-80 DEG C, add silicone resin, diethylaminopropylamine, vinyl cyanide, dibutyl tin laurate, continue to stir 30-40 minute, add other remaining component again, continue stirring reaction 60-80 minute, grinding obtains slurry, obtain.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310474813.XA CN103589333B (en) | 2013-10-12 | 2013-10-12 | A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof |
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| CN201310474813.XA CN103589333B (en) | 2013-10-12 | 2013-10-12 | A kind of emitting far-infrared heat radiation coating for meter housing and preparation method thereof |
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| CN103589333A CN103589333A (en) | 2014-02-19 |
| CN103589333B true CN103589333B (en) | 2016-03-16 |
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| CN105038495A (en) * | 2015-07-08 | 2015-11-11 | 当涂县科辉商贸有限公司 | Nanometer cellulose-loaded super thermal-insulation heat-preserving paint and preparation method thereof |
| CN107163836A (en) * | 2017-07-11 | 2017-09-15 | 合肥东恒锐电子科技有限公司 | The manufacture method of a kind of electronic equipment heat radiation coating |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101353553A (en) * | 2008-09-02 | 2009-01-28 | 飞力固有限公司 | Heat radiation coating and preparation thereof |
| CN102634245A (en) * | 2012-04-28 | 2012-08-15 | 江苏元京电子科技有限公司 | Ultraviolet light polymerization heat conduction and dissipation coating and preparation method thereof |
| CN102838892A (en) * | 2012-09-28 | 2012-12-26 | 江苏元京电子科技有限公司 | Ultraviolet curing and heat-conducting radiating coating and preparation method thereof |
| CN102964948A (en) * | 2012-11-15 | 2013-03-13 | 江苏元京电子科技有限公司 | Heat-curing heat-conduction heat-dissipation paint and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100972753B1 (en) * | 2009-11-19 | 2010-07-28 | 탁명수 | Aluminum nitride coating composite for sinking heat, heat sink using the composite and manufacturing method of the heat sink |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101353553A (en) * | 2008-09-02 | 2009-01-28 | 飞力固有限公司 | Heat radiation coating and preparation thereof |
| CN102634245A (en) * | 2012-04-28 | 2012-08-15 | 江苏元京电子科技有限公司 | Ultraviolet light polymerization heat conduction and dissipation coating and preparation method thereof |
| CN102838892A (en) * | 2012-09-28 | 2012-12-26 | 江苏元京电子科技有限公司 | Ultraviolet curing and heat-conducting radiating coating and preparation method thereof |
| CN102964948A (en) * | 2012-11-15 | 2013-03-13 | 江苏元京电子科技有限公司 | Heat-curing heat-conduction heat-dissipation paint and preparation method thereof |
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Denomination of invention: Far-infrared ray-launching radiating paint used for meter housing and preparation method thereof Effective date of registration: 20190925 Granted publication date: 20160316 Pledgee: Tianchang Science and Technology Financing Guarantee Co., Ltd. Pledgor: ANHUI AUTOMATION INSTRUMENT CO., LTD. Registration number: Y2019340000085 |
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