CN103589269B - A kind of anti-oxidant heat radiation coating for meter housing and preparation method thereof - Google Patents
A kind of anti-oxidant heat radiation coating for meter housing and preparation method thereof Download PDFInfo
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- CN103589269B CN103589269B CN201310474841.1A CN201310474841A CN103589269B CN 103589269 B CN103589269 B CN 103589269B CN 201310474841 A CN201310474841 A CN 201310474841A CN 103589269 B CN103589269 B CN 103589269B
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- 238000000576 coating method Methods 0.000 title claims abstract description 19
- 239000011248 coating agent Substances 0.000 title claims abstract description 18
- 230000005855 radiation Effects 0.000 title claims abstract description 14
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 12
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 12
- 235000006708 antioxidants Nutrition 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims description 10
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 39
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000000843 powder Substances 0.000 claims abstract description 15
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 12
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 9
- 239000004411 aluminium Substances 0.000 claims abstract description 9
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 claims abstract description 7
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 claims abstract description 7
- 238000004581 coalescence Methods 0.000 claims abstract description 7
- IUNMPGNGSSIWFP-UHFFFAOYSA-N dimethylaminopropylamine Chemical compound CN(C)CCCN IUNMPGNGSSIWFP-UHFFFAOYSA-N 0.000 claims abstract description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Substances O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 claims abstract description 7
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229920005989 resin Polymers 0.000 claims abstract description 7
- 239000011347 resin Substances 0.000 claims abstract description 7
- 229910017083 AlN Inorganic materials 0.000 claims abstract description 6
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 6
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 6
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 6
- MOMKYJPSVWEWPM-UHFFFAOYSA-N 4-(chloromethyl)-2-(4-methylphenyl)-1,3-thiazole Chemical compound C1=CC(C)=CC=C1C1=NC(CCl)=CS1 MOMKYJPSVWEWPM-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000019983 sodium metaphosphate Nutrition 0.000 claims abstract description 4
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 21
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 9
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 6
- -1 alcohol ester Chemical class 0.000 claims description 6
- 239000010977 jade Substances 0.000 claims description 6
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 6
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 6
- 229960003656 ricinoleic acid Drugs 0.000 claims description 6
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 229910052731 fluorine Inorganic materials 0.000 claims description 3
- 239000011737 fluorine Substances 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000005502 peroxidation Methods 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- VXHFNALHLRWIIU-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropanoate Chemical compound CC(C)(C)OC(=O)C(C)(C)C VXHFNALHLRWIIU-UHFFFAOYSA-N 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 239000008096 xylene Substances 0.000 claims description 3
- 230000032683 aging Effects 0.000 abstract description 5
- 230000003647 oxidation Effects 0.000 abstract description 4
- 238000007254 oxidation reaction Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 230000017525 heat dissipation Effects 0.000 abstract description 3
- 239000003112 inhibitor Substances 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 description 2
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 1
- 102100024304 Protachykinin-1 Human genes 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
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- Paints Or Removers (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
Abstract
For an anti-oxidant heat radiation coating for meter housing, be made up of the raw material of following weight part: terpolycyantoamino-formaldehyde resin 40-45, nanometer aluminium powder 2-3, dimethylaminopropylamine 4-6, polyvinyl butyral acetal 40-45, methylethylketone 20-23, ethyl acetate 10-12, acetic acid 2-3, irgasfos 168? 1-2, norbide 2-3, aluminium nitride 15-18, magnesium oxide 1-2, tributyl phosphate 0.2-0.7, sodium-metaphosphate 1-2,1-Methoxy-2-propyl acetate 12-15, film coalescence aid 4-5.The present invention is by adding nanometer aluminium powder, and heat conduction rate is high, good heat dissipation effect; By adding norbide, aluminium nitride, magnesium oxide, improve hardness and wear resistance; And coating of the present invention adds oxidation inhibitor, resistance to oxidation; Oilness is good, easily constructs, cohesive force is large, difficult drop-off, ageing-resistant, long service life.
Description
Technical field
The invention belongs to technical field of coatings, relate to a kind of heat radiation coating, more particularly, is a kind of anti-oxidant heat radiation coating for meter housing and preparation method thereof.
Background technology
Along with science and technology progress, all kinds of instrument is also arisen at the historic moment, and the heat that instrument is distributed generally can not be very fast, but because instrument can long term operation, put aside a lot of heat, if distribute heat not in time, instrument can be caused overheated, and impact normally works, and also easily damages.Coating design for the performance characteristics of instrument is at present fewer, and can not meet the requirement of productive life, heat dissipation problem is also just more and more focused on by people.There is heatproof and ageing-resistant poor and little to substrate bonding power, the not good and unhandy technical problem of radiating effect in the material that current instrument heat radiation coating uses, is difficult to the requirement meeting heat radiation.
Summary of the invention
The object of this invention is to provide a kind of anti-oxidant heat radiation coating for meter housing and preparation method thereof, coating of the present invention has the advantage that cohesive force is large, anti-oxidant, heat extraction coefficient is large.
The technical solution adopted in the present invention is:
For an anti-oxidant heat radiation coating for meter housing, it is characterized in that being made up of the raw material of following weight part: terpolycyantoamino-formaldehyde resin 40-45, nanometer aluminium powder 2-3, dimethylaminopropylamine 4-6, polyvinyl butyral acetal 40-45, methylethylketone 20-23, ethyl acetate 10-12, acetic acid 2-3, irgasfos 168 1-2, norbide 2-3, aluminium nitride 15-18, magnesium oxide 1-2, tributyl phosphate 0.2-0.7, sodium-metaphosphate 1-2,1-Methoxy-2-propyl acetate 12-15, film coalescence aid 4-5;
Described film coalescence aid is obtained by the raw material of following weight part: nanometer jade powder 2-4, linking agent TAC2-3, alcohol ester 12 4-5, Silane coupling agent KH550 1-2, vinylbenzene 3-4, ricinolic acid 1-2, MALEIC ANHYDRIDE 2-3, morpholine 2-3, peroxidation trimethylacetic acid tert-butyl ester 0.3-0.4, different fluorine that ketone 1-2, dimethylbenzene 4-5, ethyl acetate 12-13; Preparation method is: by nanometer jade powder, morpholine, vinylbenzene, ricinolic acid mixing, join in ethyl acetate and xylene mixture solvent, stir 5-10 minute, be heated to 65-70 DEG C, under 800-1200 rev/min, stir 15-30 minute, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 15-30 minute, add other remaining component again, stirring reaction 45-60 minute, to obtain final product.
The preparation method of the described anti-oxidant heat radiation coating for meter housing, it is characterized in that comprising the following steps: by nanometer aluminium powder, methylethylketone, ethyl acetate, 1-Methoxy-2-propyl acetate mixes, be heated to 60-70 DEG C, at 1000-1400 rev/min of lower stirring reaction 30-40 minute, then, be warming up to 70-75 DEG C, add and have terpolycyantoamino-formaldehyde resin, dimethylaminopropylamine, polyvinyl butyral acetal, continue to stir 30-40 minute under 1300-1800 rev/min, add other remaining component again, continuous stirring reaction 60-80 minute under 1300-1800 rev/min, grinding obtains slurry, obtain.
Beneficial effect of the present invention
The present invention is by adding nanometer aluminium powder, and heat conduction rate is high, good heat dissipation effect; By adding norbide, aluminium nitride, magnesium oxide, improve hardness and wear resistance; And coating of the present invention adds oxidation inhibitor, resistance to oxidation; Oilness is good, easily constructs, cohesive force is large, difficult drop-off, ageing-resistant, long service life.
Embodiment
For an anti-oxidant heat radiation coating for meter housing, be made up of the raw material of following weight part (kilogram): terpolycyantoamino-formaldehyde resin 43, nanometer aluminium powder 2, dimethylaminopropylamine 4-6, polyvinyl butyral acetal 42, methylethylketone 21, ethyl acetate 11, acetic acid 2, irgasfos 168 1.5, norbide 2, aluminium nitride 16, magnesium oxide 1, tributyl phosphate 0.5, sodium-metaphosphate 1,1-Methoxy-2-propyl acetate 13, film coalescence aid 4;
Described film coalescence aid is obtained by the raw material of following weight part (kilogram): nanometer jade powder 3, linking agent TAC2, alcohol ester 12, Silane coupling agent KH550 1, vinylbenzene 3, ricinolic acid 1, MALEIC ANHYDRIDE 2, morpholine 2, the peroxidation trimethylacetic acid tert-butyl ester 0.3, different fluorine that ketone 1, dimethylbenzene 4, ethyl acetate 12; Preparation method is: by nanometer jade powder, morpholine, vinylbenzene, ricinolic acid mixing, join in ethyl acetate and xylene mixture solvent, stir 8 minutes, be heated to 65 DEG C, stir 20 minutes under 1000 revs/min, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 20 minutes, add other remaining component again, stirring reaction 50 minutes, to obtain final product.
The preparation method of the described anti-oxidant heat radiation coating for meter housing, comprise the following steps: by nanometer aluminium powder, methylethylketone, ethyl acetate, 1-Methoxy-2-propyl acetate mixing, be heated to 65 DEG C, 1200 revs/min of lower stirring reactions 35 minutes, then, be warming up to 70 DEG C, add and have terpolycyantoamino-formaldehyde resin, dimethylaminopropylamine, polyvinyl butyral acetal, stirring is continued 36 minutes under 1600 revs/min, add other remaining component again, under 1600 revs/min, continue stirring reaction 70 minutes, grinding obtains slurry, to obtain final product.
Coating of the present invention is applied on meter housing, artificial accelerated aging test under 80 DEG C and 300W ultraviolet light irradiation condition, 5000 hours ageing-resistant time, heatproof high temperature 280 DEG C, bonding shearing force 18MPa., thermal conductivity 270W/(mK).
Claims (1)
1., for an anti-oxidant heat radiation coating for meter housing, it is characterized in that being made up of the raw material of following weight part: terpolycyantoamino-formaldehyde resin 40-45, nanometer aluminium powder 2-3, dimethylaminopropylamine 4-6, polyvinyl butyral acetal 40-45, methylethylketone 20-23, ethyl acetate 10-12, acetic acid 2-3, irgasfos 168 1-2, norbide 2-3, aluminium nitride 15-18, magnesium oxide 1-2, tributyl phosphate 0.2-0.7, sodium-metaphosphate 1-2,1-Methoxy-2-propyl acetate 12-15, film coalescence aid 4-5;
Described film coalescence aid is obtained by the raw material of following weight part: nanometer jade powder 2-4, linking agent TAC2-3, alcohol ester 12 4-5, Silane coupling agent KH550 1-2, vinylbenzene 3-4, ricinolic acid 1-2, MALEIC ANHYDRIDE 2-3, morpholine 2-3, peroxidation trimethylacetic acid tert-butyl ester 0.3-0.4, different fluorine that ketone 1-2, dimethylbenzene 4-5, ethyl acetate 12-13;
Preparation method is: by nanometer jade powder, morpholine, vinylbenzene, ricinolic acid mixing, join in ethyl acetate and xylene mixture solvent, stir 5-10 minute, be heated to 65-70 DEG C, under 800-1200 rev/min, stir 15-30 minute, then add alcohol ester 12, Silane coupling agent KH550, MALEIC ANHYDRIDE, stirring reaction 15-30 minute, add other remaining component again, stirring reaction 45-60 minute, to obtain final product;
The preparation method of the described anti-oxidant heat radiation coating for meter housing, comprise the following steps: by nanometer aluminium powder, methylethylketone, ethyl acetate, 1-Methoxy-2-propyl acetate mixes, be heated to 60-70 DEG C, at 1000-1400 rev/min of lower stirring reaction 30-40 minute, then, be warming up to 70-75 DEG C, add and have terpolycyantoamino-formaldehyde resin, dimethylaminopropylamine, polyvinyl butyral acetal, continue to stir 30-40 minute under 1300-1800 rev/min, add other remaining component again, stirring reaction 60-80 minute is continued under 1300-1800 rev/min, grinding obtains slurry, obtain.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310474841.1A CN103589269B (en) | 2013-10-12 | 2013-10-12 | A kind of anti-oxidant heat radiation coating for meter housing and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310474841.1A CN103589269B (en) | 2013-10-12 | 2013-10-12 | A kind of anti-oxidant heat radiation coating for meter housing and preparation method thereof |
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| CN103589269A CN103589269A (en) | 2014-02-19 |
| CN103589269B true CN103589269B (en) | 2016-04-20 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3257906A1 (en) * | 2016-06-13 | 2017-12-20 | Xerox Corporation | Interlayer composition for electronic printing |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104845460A (en) * | 2015-05-27 | 2015-08-19 | 湖州大周高分子材料有限公司 | Wear-resistant fireproof paint |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1324902A (en) * | 2000-05-24 | 2001-12-05 | 武汉市新联化工有限公司 | Aqueous silicon steel sheet paint |
| CN101407655A (en) * | 2008-11-14 | 2009-04-15 | 上海维凯化学品有限公司 | Environment-friendly type aqueous aluminum foil protecting agent and preparation thereof |
| EP2441794A2 (en) * | 2010-10-07 | 2012-04-18 | Lanxess Elastomers B.V. | Foamable elastomeric composition |
| CN102816519A (en) * | 2012-07-25 | 2012-12-12 | 江苏科技大学 | Inorganic-organic high temperature-resistant coating and preparation method thereof |
-
2013
- 2013-10-12 CN CN201310474841.1A patent/CN103589269B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1324902A (en) * | 2000-05-24 | 2001-12-05 | 武汉市新联化工有限公司 | Aqueous silicon steel sheet paint |
| CN101407655A (en) * | 2008-11-14 | 2009-04-15 | 上海维凯化学品有限公司 | Environment-friendly type aqueous aluminum foil protecting agent and preparation thereof |
| EP2441794A2 (en) * | 2010-10-07 | 2012-04-18 | Lanxess Elastomers B.V. | Foamable elastomeric composition |
| CN102816519A (en) * | 2012-07-25 | 2012-12-12 | 江苏科技大学 | Inorganic-organic high temperature-resistant coating and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3257906A1 (en) * | 2016-06-13 | 2017-12-20 | Xerox Corporation | Interlayer composition for electronic printing |
| US10208224B2 (en) | 2016-06-13 | 2019-02-19 | Xerox Corporation | Interlayer composition for electronic printing |
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| CN103589269A (en) | 2014-02-19 |
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Denomination of invention: Anti-oxidant radiating paint used for meter housing and preparation method thereof Effective date of registration: 20190925 Granted publication date: 20160420 Pledgee: Tianchang Science and Technology Financing Guarantee Co.,Ltd. Pledgor: ANHUI AUTOMATION INSTRUMENT Co.,Ltd. Registration number: Y2019340000085 |
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Denomination of invention: An antioxidant heat dissipation coating for instrument case and its preparation method Effective date of registration: 20200918 Granted publication date: 20160420 Pledgee: Tianchang Science and Technology Financing Guarantee Co.,Ltd. Pledgor: ANHUI AUTOMATION INSTRUMENT Co.,Ltd. Registration number: Y2020980006198 |
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Effective date of registration: 20240125 Address after: No. 01, Liuzhimiao Industrial Zone, Jing County, Hengshui City, Hebei Province, 053500 Patentee after: HEBEI BAOYUAN ENGINEERING PLASTICS Co.,Ltd. Country or region after: China Address before: No. 188 Weiyi Road, Tianchang Economic Development Zone, Chuzhou City, Anhui Province, 239300 Patentee before: ANHUI AUTOMATION INSTRUMENT Co.,Ltd. Country or region before: China |