CN103583613A - Insecticide for controlling Lipuphis erysimi Kaltenbach - Google Patents

Insecticide for controlling Lipuphis erysimi Kaltenbach Download PDF

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CN103583613A
CN103583613A CN201310504795.5A CN201310504795A CN103583613A CN 103583613 A CN103583613 A CN 103583613A CN 201310504795 A CN201310504795 A CN 201310504795A CN 103583613 A CN103583613 A CN 103583613A
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insecticide
ethanol
azedarach
bulk drug
lipuphis
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CN103583613B (en
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赵玉妹
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Chongqing Bochuang Intellectual Property Operations Co ltd
Shizhu Tujia Autonomous County Agricultural Characteristic Industry Development Center
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Qingdao Huaren Technology Incubator Co Ltd
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    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract

The invention provides an insecticide for controlling Lipuphis erysimi Kaltenbach. The insecticide comprises active ingredients including azedarach, persicae ramulus, peach juvenile branchlet, common cnidium fruit, radix sophorae subprostratae, pericarpium granati, coptidis rhizoma, sophorae flavescentis radix, cortex ailanthi and radix stemonae. The insecticide for controlling the Lipuphis erysimi Kaltenbach, provided by the invention, is prepared from the herb ingredients, has a function of delaying the generation of drug resistance, can be used for controlling the Lipuphis erysimi Kaltenbach in agricultural production, and serves as a new safe and efficient pesticide variety for agriculture production as well as production of green foods, fruits and vegetables.

Description

A kind of insecticide of preventing and treating radish aphid
Technical field
The present invention relates to traditional Chinese medicine technical field, relate in particular to a kind of insecticide of preventing and treating radish aphid.
Background technology
Radish aphid Lipuphis erysimi Kaltenbach claim again turnip aphid, belongs to Homoptera Aphidiadae, and this aphid often mixes generation with black peach aphid, is one of main vegetable aphid of harm brassicaceous vegetable.At northern area, especially, on the Chinese cabbage of plantation in autumn, radish, radish aphid produces and causes serious harm vegetables as sociales.Because this aphid rate of development is fast, the generation cycle is short, breeding amount is large, cause be injured blade flavescence, dwarfing, atrophy, growth retardation, in addition this worm can also be propagated crucifers of mosaic, and its loss more overweights directly and causes harm.Because this worm be take the harm of open country brassicaceous vegetable as main, physical control, bio-control method are difficult to carry out, and chemical control is widely used as means of prevention.Because black peach aphid, radish aphid mix, occur, black peach aphid has produced higher resistance to many insecticides, and peasant often strengthens dosage and the frequent same class agricultural chemicals that uses is prevented and treated, and when causing black peach aphid resistance to improve constantly, the resistance of radish aphid also changes thereupon.
The invention provides a kind of novel radish aphid insecticide, utilize medicinal herb components to be prepared from, the generation of the antagonism property of medicine has retarding action, can be used for the control to radish aphid in agricultural production, for the production of agricultural, pollution-free food and Wu Hong sea fruits and vegetables provides pesticide new variety safely and efficiently.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of novel control radish aphid insecticide, utilize medicinal herb components to be prepared from, the generation of the antagonism property of medicine has retarding action, can be used for the control to radish aphid in agricultural production, for the production of agricultural, pollution-free food and Wu Hong sea fruits and vegetables provides pesticide new variety safely and efficiently.
For solving the problems of the technologies described above, the invention provides a kind of insecticide of preventing and treating radish aphid, its bulk drug comprises azedarach, sargentodoxa cuneata, peach branch, frutus cnidii, subprostrate sophora, granatum, the coptis, kuh-seng, bark of tree of heaven and the tuber of stemona.
Wherein, in described insecticide, the weight of each bulk drug is respectively azedarach 2lg~3kg, sargentodoxa cuneata 1.5kg~2.5kg, peach branch 3kg~4kg, frutus cnidii 6kg~7kg, subprostrate sophora 2kg~3kg, granatum 2.5kg~3.5kg, coptis 2kg~3kg, kuh-seng 1.5kg~2.5kg, bark of tree of heaven 2kg~3kg and tuber of stemona 4kg~5kg.
Wherein, in described insecticide, the weight of each bulk drug is respectively azedarach 2.5kg, sargentodoxa cuneata 2kg, peach branch 3.5kg, frutus cnidii 6.5kg, subprostrate sophora 2.5kg, granatum 3kg, coptis 2.5kg, kuh-seng 2kg, bark of tree of heaven 2.5kg and tuber of stemona 4.5kg.
The present invention also provides above-mentioned method for producing insecticide, above-mentioned raw materials medicine is mixed, the ethanol that is 70%~80% with determining alcohol dissolves, and the addition of ethanol is 3~5 times of bulk drug mixture quality, then to add the concentration with respect to 0.05 times of ethanol volume be 37% salt pickle liquor, under boiling condition, hot dipping twice is soaked 3 hours at every turn, and it soaks addition and is as the criterion to cover material, in heating process, should add at any time water purification, keep the water yield.Merge twice immersion liquid, being concentrated into density was 1.10 (being mucilage shape), the ethanol that the determining alcohol of then sneaking into equal volume is 70%~80%, and sedimentation is after 6 hours, with 100 order copper sievings, remove the dregs of a decoction, pH value is adjusted to 6, under 40 ℃ of constant temperature, adds successively 8% emulsifier polyoxyethylene ether by medicine liquid volume ratio, 4% bleeding agent sodium alkyl benzene sulfonate, 3% synergist castor oil stirs 3 hours, cooling after, rear filling with 160 order copper sieve essence filters.
Beneficial effect of the present invention:
Control radish aphid insecticide provided by the invention, utilize medicinal herb components to be prepared from, the generation of the antagonism property of medicine has retarding action, can be used for the control to radish aphid in agricultural production, for the production of agricultural, pollution-free food and Wu Hong sea fruits and vegetables provides pesticide new variety safely and efficiently.
Embodiment
The invention provides a kind of insecticide of preventing and treating radish aphid, its bulk drug comprises azedarach, sargentodoxa cuneata, peach branch, frutus cnidii, subprostrate sophora, granatum, the coptis, kuh-seng, bark of tree of heaven and the tuber of stemona.
Further, described insecticide only consists of above-mentioned raw materials medicine.
In described insecticide, the weight of each bulk drug is respectively azedarach 2kg~3kg, sargentodoxa cuneata 1.5kg~2.5kg, peach branch 3kg~4kg, frutus cnidii 6kg~7kg, subprostrate sophora 2kg~3kg, granatum 2.5kg~3.5kg, coptis 2kg~3kg, kuh-seng 1.5kg~2.5kg, bark of tree of heaven 2kg~3kg and tuber of stemona 4kg~5kg.
Further preferably, in described insecticide, the weight of each bulk drug is respectively azedarach 2.5kg, sargentodoxa cuneata 2kg, peach branch 3.5kg, frutus cnidii 6.5kg, subprostrate sophora 2.5kg, granatum 3kg, coptis 2.5kg, kuh-seng 2kg, bark of tree of heaven 2.5kg and tuber of stemona 4.5kg.
In side, the pharmacology of each bulk drug is as follows:
Sargentodoxa cuneata: bitter, property is flat, returns liver, large intestine channel, has the carbuncle that disappears that relieves internal heat, and promoting blood circulation and removing obstruction in channels, the effect of wind dispelling insecticide, cures mainly acute and chronic appendicitis, arthralgia due to wind-dampness, dysentery characterized by blood in the stool, blood drenches, irregular menstruation, infantile malnutrition due to digestive disturbances or intestinalparasites, worm pain, the cards such as injury from falling down.
Peach branch: latin name Persicae Ramulus, bitter, property is flat, and the thoughts of returning home, Liver Channel, have activating blood to promote menstruation, and the effect of removing toxic substances desinsection, for trusted subordinate's shouting pain, arthralgia due to wind-dampness, the cards such as traumatic injury.
Frutus cnidii: taste is pungent, bitter, warm in nature, enters kidney channel, the effect of there is warming kidney to invigorate yang, removing dampness and destroying parasites, dispellingging wind and arresting itching, the impotence in male causing for decline of kidney-YANG, woman Gong Leng are infertile, under cold-dampness band or the card such as waist knee crymodynia.
Azedarach: latin name Meliae Cortex, bitter, cold in nature, return liver, spleen, stomach warp, there is desinsection, treat tinea, for roundworm disease, enterobiasis, the cards such as abdominal pain due to enterositosis.
Subprostrate sophora: bitter, cold in nature, enter the heart, lung, large intestine channel, there is removing toxic substances relieve sore throat, clearing heat and promoting diuresis, the effect that desinsection is anticancer, for abscess of throat, the gum dentalgia that swells, cough with lung heat, dysentery, jaundice, the cards such as the swollen favus of the scalp of heat.
Granatum: taste acid, puckery, warm in nature, enter large intestine, kidney channel, there is relieving diarrhea with astringents, the effect of hemostasis desinsection, for rushing down for a long time protracted dysentery, hematochezia, under uterine bleeding band, the cards such as abdominal pain due to enterositosis, granatum has stronger inhibitory action to Escherichia coli.
The coptis: bitter, cold in nature, the thoughts of returning home, spleen, stomach, liver, courage, large intestine channel, have the effect of clearing heat and detoxicating, purging intense heat and detonicating, desinsection, full for damp and hot ruffian, vomiting acid regurgitation, rushes down dysentery, jaundice, unconsciousness due to high fever, heart-fire hyperactivity, dysphoria and insomnia, blood-head is told nosebleed, hot eyes, toothache, quenches one's thirst, the carbuncle furunculosis that swells, control eczema outward, wet sore, the duct card such as suppurate.
Kuh-seng: latin name Sophorae Flavescentis Radix, bitter, cold in nature, enter the heart, stomach, large intestine, urinary bladder channel, there is the effect of heat-clearing and damp-drying drug, wind dispelling insecticide, be mainly used in damp-heat dysentery, jaundice, stranguria, kuh-seng has obvious inhibitory action to shigella dysenteriae, Escherichia coli, proteus, beta streptococcus and staphylococcus aureus.
Bark of tree of heaven: bitter, puckery, cold in nature, enter large intestine, stomach, Liver Channel, there is heat-clearing and damp-drying drug, puckery intestines are band only, hemostasis, the effect of desinsection, for damp-heat dysentery, rushes down protracted dysentery for a long time, and uterine bleeding, has blood in stool, blood under hemorrhoid, under band, the cards such as hematochezia.
The tuber of stemona: taste is sweet, bitter, slightly warm in nature enters lung channel, have and moisten the lung and relieve the cough, the effect of delousing desinsection, tuber of stemona temperature embellishes but not dry, and property is kept and is not walked, the merit that has out again drop-down gas, be mainly used in new all coughing for a long time, be especially suitable for the hot chronic cough person of labor, the modern times are used for preventing and treating the cough of chronic bronchitis, the dry cough of pulmonary tuberculosis, the cards such as pertussis.
The present invention also provides above-mentioned method for producing insecticide, above-mentioned raw materials medicine is mixed, the ethanol that is 70%~80% with determining alcohol dissolves, and the addition of ethanol is 3~5 times of bulk drug mixture quality, then to add the concentration with respect to 0.05 times of ethanol volume be 37% salt pickle liquor, under boiling condition, hot dipping twice is soaked 3 hours at every turn, and it soaks addition and is as the criterion to cover material, in heating process, should add at any time water purification, keep the water yield.Merge twice immersion liquid, being concentrated into density was 1.10 (being mucilage shape), the ethanol that the determining alcohol of then sneaking into equal volume is 70%~80%, and sedimentation is after 6 hours, with 100 order copper sievings, remove the dregs of a decoction, pH value is adjusted to 6, under 40 ℃ of constant temperature, adds successively 8% emulsifier polyoxyethylene ether by medicine liquid volume ratio, 4% bleeding agent sodium alkyl benzene sulfonate, 3% synergist castor oil stirs 3 hours, cooling after, rear filling with 160 order copper sieve essence filters.
Below adopt embodiment to describe embodiments of the present invention in detail, to the present invention, how application technology means solve technical problem whereby, and the implementation procedure of reaching technique effect can fully understand and implement according to this.
Preparation Example 1
Azedarach 2.5kg, sargentodoxa cuneata 2kg, peach branch 3.5kg, frutus cnidii 6.5kg, subprostrate sophora 2.5kg, granatum 3kg, coptis 2.5kg, kuh-seng 2kg, bark of tree of heaven 2.5kg and tuber of stemona 4.5kg are mixed, the ethanol that is 80% with determining alcohol dissolves, the addition of ethanol is 5 times of bulk drug mixture quality, adding the concentration with respect to 0.05 times of ethanol volume is 37% salt pickle liquor again, under boiling condition, twice of hot dipping, each immersion 3 hours, it soaks addition and is as the criterion to cover material, in heating process, should add at any time water purification, keep the water yield.Merge twice immersion liquid, being concentrated into density was 1.10 (being mucilage shape), the ethanol that the determining alcohol of then sneaking into equal volume is 80%, and sedimentation is after 6 hours, with 100 order copper sievings, remove the dregs of a decoction, pH value is adjusted to 6, under 40 ℃ of constant temperature, adds successively 8% emulsifier polyoxyethylene ether by medicine liquid volume ratio, 4% bleeding agent sodium alkyl benzene sulfonate, 3% synergist castor oil stirs 3 hours, cooling after, rear filling with 160 order copper sieve essence filters.
Indoor virulence experiment
Indoor virulence and mixed synergies thereof are with reference to routine techniques, the present embodiment adopts following methods to carry out: will pick up from solarium without the fresh cabbage leaves of using any agricultural chemicals, with running water, rinse and use after paper handkerchief suck dry moisture, with the card punch that diameter is 2cm, make leaf dish, and immerse in the liquid prepare approximately 5 seconds, take out, naturally dry stand-by.The blade of processing is put into culture dish, and every ware is put 3~4 leaf dish, and 10 examination worms of every ware access, are allowed to condition on leaf and take food.Every ware is 1 repetition, and every concentration is established 4 repetitions; Contrast is processed with the aqueous acetone solution with amount.Each death condition of processing of 48h investigation.Be calculated as follows lethality, Abbott formula calculation correction lethality.
Figure BDA0000401024590000051
Abbott formula computing formula is as follows:
Figure BDA0000401024590000052
Test method adopt Sun Yun abundant wait that nineteen sixty proposes by toxicity index, calculate the method for Mixed Pharmacy co-toxicity.First with conventional method, record mixture and form mixture each single dose virulence regression equation and obtain LD50, take again the toxicity index of a kind of single dose as each single dose of criterion calculation, the actual toxicity index of mixture and theoretical toxicity index, finally calculate its co-toxicity coefficient (co-toxicity coefficient, CTC).Its formula of reduction is as follows:
If confection is M, the single dose that forms M is A, B, and percentage composition is P,
Figure BDA0000401024590000053
Criterion: if the toxicity test co-toxicity coefficient of mixture approaches 100 expression summation actions, be obviously greater than 100 expression synergistic effects, be significantly less than 100 expression antagonisms.
The insecticide of preparing at the present embodiment to 2 age radish aphid indoor virulence result, the fill a prescription LC of 72h of the present invention 502.34mg/L.
1000 times of the insecticide dilutions of the present embodiment 1 preparation are processed radish aphid spraying, and contrast agents is 1000 times of liquid of 50% Tea Saponin aqua.After medication the 7th day to the preventive effect of radish aphid in Table 1, the insecticide that the present invention prepares is as can be seen from the test results compared with former agricultural chemicals, and the control efficiency of insect is significantly strengthened.
Table 1
Medicine Control efficiency
50% Tea Saponin aqua (diluting 1000 times of liquid) 69.38%
The insecticide of embodiment 1 preparation 92.29%
All above-mentioned these intellectual properties of primary enforcement, do not set restriction this new product of other forms of enforcement and/or new method.Those skilled in the art will utilize this important information, and foregoing is revised, to realize similar implementation status.But all modifications or transformation belong to the right of reservation based on new product of the present invention.
The above, be only preferred embodiment of the present invention, is not the present invention to be done to the restriction of other form, and any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the equivalent embodiment of equivalent variations.But every technical solution of the present invention content that do not depart from, any simple modification, equivalent variations and the remodeling above embodiment done according to technical spirit of the present invention, still belong to the protection domain of technical solution of the present invention.

Claims (4)

1. an insecticide of preventing and treating radish aphid, is characterized in that: bulk drug comprises azedarach, sargentodoxa cuneata, peach branch, frutus cnidii, subprostrate sophora, granatum, the coptis, kuh-seng, bark of tree of heaven and the tuber of stemona.
2. insecticide as claimed in claim 1, is characterized in that: the weight of each bulk drug is respectively azedarach 2kg~3kg, sargentodoxa cuneata 1.5kg~2.5kg, peach branch 3kg~4kg, frutus cnidii 6kg~7kg, subprostrate sophora 2kg~3kg, granatum 2.5kg~3.5kg, coptis 2kg~3kg, kuh-seng 1.5kg~2.5kg, bark of tree of heaven 2kg~3kg and tuber of stemona 4kg~5kg.
3. insecticide as claimed in claim 1 or 2, is characterized in that: in described insecticide, the weight of each bulk drug is respectively azedarach 2.5kg, sargentodoxa cuneata 2kg, peach branch 3.5kg, frutus cnidii 6.5kg, subprostrate sophora 2.5kg, granatum 3kg, coptis 2.5kg, kuh-seng 2kg, bark of tree of heaven 2.5kg and tuber of stemona 4.5kg.
4. method for producing insecticide described in claims 1 to 3, it is characterized in that: above-mentioned raw materials medicine is mixed, the ethanol that is 70%~80% with determining alcohol dissolves, and the addition of ethanol is 3~5 times of bulk drug mixture quality, then to add the concentration with respect to 0.05 times of ethanol volume be 37% salt pickle liquor, under boiling condition, hot dipping twice is soaked 3 hours at every turn, and it soaks addition and is as the criterion to cover material, in heating process, should add at any time water purification, keep the water yield.Merge twice immersion liquid, being concentrated into density was 1.10 (being mucilage shape), the ethanol that the determining alcohol of then sneaking into equal volume is 70%~80%, and sedimentation is after 6 hours, with 100 order copper sievings, remove the dregs of a decoction, pH value is adjusted to 6, under 40 ℃ of constant temperature, adds successively 8% emulsifier polyoxyethylene ether by medicine liquid volume ratio, 4% bleeding agent sodium alkyl benzene sulfonate, 3% synergist castor oil stirs 3 hours, cooling after, rear filling with 160 order copper sieve essence filters.
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