CN103555422A - Method for extracting plamochromic pigment in tobacco by use of subcritical extraction technology - Google Patents
Method for extracting plamochromic pigment in tobacco by use of subcritical extraction technology Download PDFInfo
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- CN103555422A CN103555422A CN201310528306.XA CN201310528306A CN103555422A CN 103555422 A CN103555422 A CN 103555422A CN 201310528306 A CN201310528306 A CN 201310528306A CN 103555422 A CN103555422 A CN 103555422A
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- extraction
- pigment
- plamochromic
- tobacco
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- 239000000049 pigment Substances 0.000 title claims abstract description 52
- 238000000605 extraction Methods 0.000 title claims abstract description 46
- 241000208125 Nicotiana Species 0.000 title claims abstract description 29
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 24
- 239000002904 solvent Substances 0.000 claims abstract description 28
- 239000000284 extract Substances 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 235000019505 tobacco product Nutrition 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 7
- 239000012530 fluid Substances 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 238000005406 washing Methods 0.000 claims description 12
- 238000005516 engineering process Methods 0.000 claims description 9
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000001556 precipitation Methods 0.000 claims description 6
- 239000003963 antioxidant agent Substances 0.000 claims description 5
- 230000003078 antioxidant effect Effects 0.000 claims description 5
- 235000006708 antioxidants Nutrition 0.000 claims description 5
- 239000006210 lotion Substances 0.000 claims description 5
- LVGUZGTVOIAKKC-UHFFFAOYSA-N 1,1,1,2-tetrafluoroethane Chemical compound FCC(F)(F)F LVGUZGTVOIAKKC-UHFFFAOYSA-N 0.000 claims description 4
- 239000001273 butane Substances 0.000 claims description 4
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 4
- 210000002706 plastid Anatomy 0.000 claims description 4
- 239000004322 Butylated hydroxytoluene Substances 0.000 claims description 3
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims description 3
- 229940095259 butylated hydroxytoluene Drugs 0.000 claims description 3
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 239000003112 inhibitor Substances 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 238000002203 pretreatment Methods 0.000 claims description 3
- 239000001294 propane Substances 0.000 claims description 3
- 238000010907 mechanical stirring Methods 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims description 2
- 238000002386 leaching Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000005086 pumping Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 description 4
- 238000000638 solvent extraction Methods 0.000 description 4
- 235000021466 carotenoid Nutrition 0.000 description 3
- 150000001747 carotenoids Chemical class 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 229930002875 chlorophyll Natural products 0.000 description 3
- 235000019804 chlorophyll Nutrition 0.000 description 3
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 235000019504 cigarettes Nutrition 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000000194 supercritical-fluid extraction Methods 0.000 description 2
- 238000002137 ultrasound extraction Methods 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009418 agronomic effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000004807 desolvation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
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Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201310528306.XA CN103555422A (en) | 2013-10-30 | 2013-10-30 | Method for extracting plamochromic pigment in tobacco by use of subcritical extraction technology |
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CN201310528306.XA CN103555422A (en) | 2013-10-30 | 2013-10-30 | Method for extracting plamochromic pigment in tobacco by use of subcritical extraction technology |
Publications (1)
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CN103555422A true CN103555422A (en) | 2014-02-05 |
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CN201310528306.XA Pending CN103555422A (en) | 2013-10-30 | 2013-10-30 | Method for extracting plamochromic pigment in tobacco by use of subcritical extraction technology |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103977595A (en) * | 2014-05-23 | 2014-08-13 | 中国烟草总公司郑州烟草研究院 | Method for reducing content of heavy metal in extract for cigarettes by subcritical extraction technology |
CN105132176A (en) * | 2015-09-28 | 2015-12-09 | 中国烟草总公司郑州烟草研究院 | Preparation method of Mao cigarette extract and application of Mao cigarette extract to cigarette filter stick |
CN107033626A (en) * | 2017-04-28 | 2017-08-11 | 常德华馥生物技术有限公司 | A kind of method that subcritical abstraction is combined separate tobacco natural pigment with molecular distillation |
CN107057855A (en) * | 2017-01-13 | 2017-08-18 | 河南工业大学 | A kind of ultrasound removal is subcritical to produce the residual molten method of giving off a strong fragrance chilli seed crude oil |
CN112755142A (en) * | 2021-02-25 | 2021-05-07 | 河南骨痹中医研究院(有限合伙) | Skin treatment cream and preparation method thereof |
CN112755156A (en) * | 2021-02-25 | 2021-05-07 | 河南骨痹中医研究院(有限合伙) | External traditional Chinese medicine preparation for treating HPV infection and preparation method thereof |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101487820A (en) * | 2008-01-18 | 2009-07-22 | 河南中烟工业公司 | Fast extraction and measurement method for plastid pigment in tobacco and tobacco products |
-
2013
- 2013-10-30 CN CN201310528306.XA patent/CN103555422A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101487820A (en) * | 2008-01-18 | 2009-07-22 | 河南中烟工业公司 | Fast extraction and measurement method for plastid pigment in tobacco and tobacco products |
Non-Patent Citations (1)
Title |
---|
刘月蓉等: "天然植物精油提取技术——亚临界流体萃取", 《莆田学院学报》, vol. 18, no. 2, 30 April 2011 (2011-04-30), pages 67 - 70 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103977595A (en) * | 2014-05-23 | 2014-08-13 | 中国烟草总公司郑州烟草研究院 | Method for reducing content of heavy metal in extract for cigarettes by subcritical extraction technology |
CN103977595B (en) * | 2014-05-23 | 2015-11-18 | 中国烟草总公司郑州烟草研究院 | A kind of method utilizing subcritical abstraction technology to reduce tobacco extract content of beary metal |
CN105132176A (en) * | 2015-09-28 | 2015-12-09 | 中国烟草总公司郑州烟草研究院 | Preparation method of Mao cigarette extract and application of Mao cigarette extract to cigarette filter stick |
CN107057855A (en) * | 2017-01-13 | 2017-08-18 | 河南工业大学 | A kind of ultrasound removal is subcritical to produce the residual molten method of giving off a strong fragrance chilli seed crude oil |
CN107033626A (en) * | 2017-04-28 | 2017-08-11 | 常德华馥生物技术有限公司 | A kind of method that subcritical abstraction is combined separate tobacco natural pigment with molecular distillation |
CN112755142A (en) * | 2021-02-25 | 2021-05-07 | 河南骨痹中医研究院(有限合伙) | Skin treatment cream and preparation method thereof |
CN112755156A (en) * | 2021-02-25 | 2021-05-07 | 河南骨痹中医研究院(有限合伙) | External traditional Chinese medicine preparation for treating HPV infection and preparation method thereof |
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Owner name: ZHENGZHOU UNIVERSITY CHINA TOBACCO HENAN INDUSTRY Free format text: FORMER OWNER: ZHENGZHOU UNIVERSITY Effective date: 20140928 |
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C41 | Transfer of patent application or patent right or utility model | ||
C53 | Correction of patent of invention or patent application | ||
CB03 | Change of inventor or designer information |
Inventor after: Pang Huili Inventor after: Ma Yuping Inventor after: Wang Wenling Inventor after: Qin Guangyong Inventor after: Qi Kun Inventor before: Pang Huili Inventor before: Qin Guangyong Inventor before: Qi Kun Inventor before: Wang Wenling Inventor before: Ma Yuping |
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COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: PANG HUILI QIN GUANGYONG QI KUN WANG WENLING MA YUPING TO: PANG HUILI MA YUPING WANG WENLING QIN GUANGYONG QI KUN |
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TA01 | Transfer of patent application right |
Effective date of registration: 20140928 Address after: 455000 Henan Anyang Development Zone advanced technology equipment Park Applicant after: HENAN YALINJIE BIOLOGICAL TECHNOLOGY Co.,Ltd. Applicant after: Zhengzhou University Applicant after: CHINA TOBACCO HENAN INDUSTRIAL Co.,Ltd. Address before: 455000 Henan Anyang Development Zone advanced technology equipment Park Applicant before: HENAN YALINJIE BIOLOGICAL TECHNOLOGY Co.,Ltd. Applicant before: Zhengzhou University |
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CI01 | Publication of corrected invention patent application |
Correction item: Applicant|Address|Applicant Correct: Henan Yalinjie Biological Technology Co., Ltd.|455000 Henan Anyang Development Zone advanced technology equipment Park|Zhengzhou University|China Tobacco Henan Industrial Co., Ltd. False: HENAN YALINJIE BIOLOGICAL TECHNOLOGY CO., LTD.|455000 Henan Anyang Development Zone advanced technology equipment Park|Zhengzhou University|China Tobacco Henan Industrial Co., Ltd. Number: 43 Volume: 30 |
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C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
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Application publication date: 20140205 |