CN103497629A - Overcoating fireproof powdery paint - Google Patents
Overcoating fireproof powdery paint Download PDFInfo
- Publication number
- CN103497629A CN103497629A CN201310395994.7A CN201310395994A CN103497629A CN 103497629 A CN103497629 A CN 103497629A CN 201310395994 A CN201310395994 A CN 201310395994A CN 103497629 A CN103497629 A CN 103497629A
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- CN
- China
- Prior art keywords
- parts
- paint
- raw material
- mixed
- aluminium nitride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000003973 paint Substances 0.000 title claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 10
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000004114 Ammonium polyphosphate Substances 0.000 claims abstract description 4
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 4
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000019826 ammonium polyphosphate Nutrition 0.000 claims abstract description 4
- 229920001276 ammonium polyphosphate Polymers 0.000 claims abstract description 4
- 239000003822 epoxy resin Substances 0.000 claims abstract description 4
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 4
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 4
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 4
- WSFQLUVWDKCYSW-UHFFFAOYSA-M sodium;2-hydroxy-3-morpholin-4-ylpropane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(O)CN1CCOCC1 WSFQLUVWDKCYSW-UHFFFAOYSA-M 0.000 claims abstract description 4
- 239000008117 stearic acid Substances 0.000 claims abstract description 4
- 239000000843 powder Substances 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 13
- 238000004079 fireproofing Methods 0.000 claims description 12
- 229910017083 AlN Inorganic materials 0.000 claims description 9
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims description 9
- 239000004135 Bone phosphate Substances 0.000 claims description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 229910001679 gibbsite Inorganic materials 0.000 claims description 6
- 229910001710 laterite Inorganic materials 0.000 claims description 6
- 239000011504 laterite Substances 0.000 claims description 6
- PIJPYDMVFNTHIP-UHFFFAOYSA-L lead sulfate Chemical compound [PbH4+2].[O-]S([O-])(=O)=O PIJPYDMVFNTHIP-UHFFFAOYSA-L 0.000 claims description 6
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 claims description 3
- TYAJHXFESOFURV-UHFFFAOYSA-N butane-1-thiol;tin Chemical compound [Sn].CCCCS TYAJHXFESOFURV-UHFFFAOYSA-N 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- -1 carbon alcohols ester Chemical class 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000000428 dust Substances 0.000 claims description 3
- 238000005984 hydrogenation reaction Methods 0.000 claims description 3
- 229940059574 pentaerithrityl Drugs 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 3
- 229960003656 ricinoleic acid Drugs 0.000 claims description 3
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 3
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 230000032683 aging Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 239000003063 flame retardant Substances 0.000 abstract description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 abstract 1
- 229920000877 Melamine resin Polymers 0.000 abstract 1
- LUZSPGQEISANPO-UHFFFAOYSA-N butyltin Chemical compound CCCC[Sn] LUZSPGQEISANPO-UHFFFAOYSA-N 0.000 abstract 1
- 239000002131 composite material Substances 0.000 abstract 1
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 abstract 1
- 229940095068 tetradecene Drugs 0.000 abstract 1
- 238000000576 coating method Methods 0.000 description 9
- 239000011248 coating agent Substances 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 1
- 239000012296 anti-solvent Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses an overcoating fireproof powdery paint. The paint comprises the following raw materials by weight: 60 to 70 parts of E-42 epoxy resin, 10 to 16 parts of diethylenetriamine, 1 to 2 parts of ammonium polyphosphate, 1 to 2 parts of melamine, 2 to 3 parts of pentaerythritol, 7 to 10 parts of aluminum nitride, 2 to 3 parts of bis-tetradecene alcohol ester, 1 to 2 parts of ammonium biphosphate, 1 to 2 parts of zinc naphthenate, 2 to 3 parts of stearic acid, 0.3 to 0.6 part of butadiene, 1 to 2 parts of butyltin mercaptide and 10 to 20 parts of a composite filling material. The paint provided by the invention has good endurance, water resistance, rub resistance and stain resistance, especially better flame-retardant and fireproof effects and ageing and attenuation resistance; formula cost and production and processing cost for the paint are low, and actual operation can be easily carried out.
Description
Technical field
The present invention relates generally to a kind of coating, relates in particular to a kind of facing type fireproofing powder paint.
Background technology
Powder coating, as environmental protection, energy-conservation, economic, efficient product, replaces liquid paint gradually, becomes the fastest coating new technology of tempo and scale.In current art of powder coatings, be all common indoor decorative powder coating or outdoor weatherability powder coating basically.Functional powder coating also relates to the fields such as the heavy anti-corrosive type of epoxy, conductivity type, insulated type, the type of anti-combustion the, scumbling type, and therefore studying the novel high-performance powder coating can play better booster action for nation-building, social life.
Summary of the invention
The object of the invention is exactly for a kind of facing type fireproofing powder paint is provided.
The present invention is achieved by the following technical solutions:
A kind of facing type fireproofing powder paint is characterized in that what it was comprised of the raw material of following weight parts:
E-42 epoxy resin 60-70, diethylenetriamine 10-16, ammonium polyphosphate 1-2, trimeric cyanamide 1-2, tetramethylolmethane 2-3, aluminium nitride 7-10, two ten four carbon alcohols ester 2-3, primary ammonium phosphate 1-2, zinc naphthenate 1-2, stearic acid 2-3, divinyl 0.3-0.6, butanethiol tin 1-2, compounded mix 10-20;
Described compounded mix is comprised of the raw material of following weight parts:
Gibbsite 10-20, laterite 30-40, aluminium nitride 4-6, flower bulb alkali 3-4, ricinolic acid 1-2, oxidized polyethlene wax 3-4, lead sulfate tribasic 0.1-0.2;
Above-mentioned laterite, gibbsite are mixed, calcining 3-5 hour under 500-600 ℃, after discharging is cooling, with aluminium nitride, flower bulb alkali, lead sulfate tribasic, mix, add suitable quantity of water and grind, the hydrochloric acid adjusting PH that adds 10-20% is 4-5, being heated to system temperature is 70-90 ℃, and being ground to fineness is the 300-400 order, and the repeated hydrogenation sodium oxide is adjusted to neutrality, spraying drying, obtain powder; The gained powder is mixed with other remaining component, grind and evenly obtain described compounded mix.
A kind of preparation method of facing type fireproofing powder paint comprises the following steps:
After above-mentioned each raw material is mixed, the input forcing machine melt extrudes, air-cooled, through in pulverizer, pulverized, then abrasive dust, sieve, and obtains described facing type fireproofing powder paint.
Advantage of the present invention is:
It is better that coating of the present invention has weather resistance, water tolerance, rub resistance and contamination resistance, especially fire retardant effect and ageing resistance decay preferably, and formulation cost and process for processing cost are lower, are easy to actually operating.
Embodiment
Embodiment 1,
A kind of facing type fireproofing powder paint, it is comprised of the raw material of following weight parts (kilogram):
E-42 epoxy resin 70, diethylenetriamine 16, ammonium polyphosphate 1, trimeric cyanamide 2, tetramethylolmethane 2, aluminium nitride 10, two ten four carbon alcohols esters 2, primary ammonium phosphate 2, zinc naphthenate 2, stearic acid 2-3, divinyl 0.6, butanethiol tin 1, compounded mix 20;
Described compounded mix is comprised of the raw material of following weight parts:
Gibbsite 20, laterite 40, aluminium nitride 6, flower bulb alkali 3, ricinolic acid 1, oxidized polyethlene wax 3, lead sulfate tribasic 0.2;
Above-mentioned laterite, gibbsite are mixed, under 600 ℃, calcining is 3 hours, after discharging is cooling, with aluminium nitride, flower bulb alkali, lead sulfate tribasic, mix, add suitable quantity of water and grind, adding 20% hydrochloric acid, to regulate PH be 4-5, being heated to system temperature is 90 ℃, and being ground to fineness is 400 orders, and the repeated hydrogenation sodium oxide is adjusted to neutrality, spraying drying, obtain powder; The gained powder is mixed with other remaining component, grind and evenly obtain described compounded mix.
A kind of preparation method of facing type fireproofing powder paint comprises the following steps:
After above-mentioned each raw material is mixed, the input forcing machine melt extrudes, air-cooled, through in pulverizer, pulverized, then abrasive dust, sieve, and obtains described facing type fireproofing powder paint.
Performance test:
Anti-solvent: 240 hours, unchanged;
Salt-fog test (1000h): unchanged.
Claims (2)
1. a facing type fireproofing powder paint is characterized in that what it was comprised of the raw material of following weight parts:
E-42 epoxy resin 60-70, diethylenetriamine 10-16, ammonium polyphosphate 1-2, trimeric cyanamide 1-2, tetramethylolmethane 2-3, aluminium nitride 7-10, two ten four carbon alcohols ester 2-3, primary ammonium phosphate 1-2, zinc naphthenate 1-2, stearic acid 2-3, divinyl 0.3-0.6, butanethiol tin 1-2, compounded mix 10-20;
Described compounded mix is comprised of the raw material of following weight parts:
Gibbsite 10-20, laterite 30-40, aluminium nitride 4-6, flower bulb alkali 3-4, ricinolic acid 1-2, oxidized polyethlene wax 3-4, lead sulfate tribasic 0.1-0.2;
Above-mentioned laterite, gibbsite are mixed, calcining 3-5 hour under 500-600 ℃, after discharging is cooling, with aluminium nitride, flower bulb alkali, lead sulfate tribasic, mix, add suitable quantity of water and grind, the hydrochloric acid adjusting PH that adds 10-20% is 4-5, being heated to system temperature is 70-90 ℃, and being ground to fineness is the 300-400 order, and the repeated hydrogenation sodium oxide is adjusted to neutrality, spraying drying, obtain powder; The gained powder is mixed with other remaining component, grind and evenly obtain described compounded mix.
2. the preparation method of a facing type fireproofing powder paint as claimed in claim 1 is characterized in that comprising the following steps:
After above-mentioned each raw material is mixed, the input forcing machine melt extrudes, air-cooled, through in pulverizer, pulverized, then abrasive dust, sieve, and obtains described facing type fireproofing powder paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310395994.7A CN103497629B (en) | 2013-09-04 | A kind of facing type fireproofing powder paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310395994.7A CN103497629B (en) | 2013-09-04 | A kind of facing type fireproofing powder paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103497629A true CN103497629A (en) | 2014-01-08 |
| CN103497629B CN103497629B (en) | 2016-11-30 |
Family
ID=
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105238215A (en) * | 2015-11-02 | 2016-01-13 | 华北理工大学 | Decorative fireproof powder paint |
| CN105567024A (en) * | 2015-11-25 | 2016-05-11 | 国网辽宁省电力有限公司阜新供电公司 | Insulated fireproof coating for optical cables |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434804A (en) * | 2007-11-17 | 2009-05-20 | 徐州正菱涂装有限公司 | Facing type fireproofing powder paint |
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434804A (en) * | 2007-11-17 | 2009-05-20 | 徐州正菱涂装有限公司 | Facing type fireproofing powder paint |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105238215A (en) * | 2015-11-02 | 2016-01-13 | 华北理工大学 | Decorative fireproof powder paint |
| CN105567024A (en) * | 2015-11-25 | 2016-05-11 | 国网辽宁省电力有限公司阜新供电公司 | Insulated fireproof coating for optical cables |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Xiao Xiaomei Inventor before: Song Yuchun |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20161008 Address after: 362417 Anxi County, Quanzhou Province peach boat township I Pei Pei Pei Village, No. 23 Applicant after: Xiao Xiaomei Address before: 233000 No. 404 South Daqing Road, hi tech Zone, Anhui, Bengbu Applicant before: Anhui Topusen Battery Co., Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Liu Zhiying Inventor before: Xiao Xiaomei |
|
| CB03 | Change of inventor or designer information | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170505 Address after: 100076 Beijing city Daxing District town of Xihongmen Xinhe Road No. 1 Patentee after: Beijing Cheonan Puning fire fighting material factory Address before: 362417 Anxi County, Quanzhou Province peach boat township I Pei Pei Pei Village, No. 23 Patentee before: Xiao Xiaomei |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161130 Termination date: 20190904 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |