CN103497629B - A kind of facing type fireproofing powder paint - Google Patents
A kind of facing type fireproofing powder paint Download PDFInfo
- Publication number
- CN103497629B CN103497629B CN201310395994.7A CN201310395994A CN103497629B CN 103497629 B CN103497629 B CN 103497629B CN 201310395994 A CN201310395994 A CN 201310395994A CN 103497629 B CN103497629 B CN 103497629B
- Authority
- CN
- China
- Prior art keywords
- powder paint
- facing type
- raw material
- aluminium nitride
- mix
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000000843 powder Substances 0.000 title claims abstract description 23
- 239000003973 paint Substances 0.000 title claims abstract description 18
- 238000004079 fireproofing Methods 0.000 title claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 19
- PIGFYZPCRLYGLF-UHFFFAOYSA-N aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
- QIQXTHQIDYTFRH-UHFFFAOYSA-N Stearic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- WXZMFSXDPGVJKK-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims abstract description 4
- LFVGISIMTYGQHF-UHFFFAOYSA-N Ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims abstract description 4
- WQAQPCDUOCURKW-UHFFFAOYSA-N Butanethiol Chemical compound CCCCS WQAQPCDUOCURKW-UHFFFAOYSA-N 0.000 claims abstract description 4
- RPNUMPOLZDHAAY-UHFFFAOYSA-N DETA Chemical class NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims abstract description 4
- JDSHMPZPIAZGSV-UHFFFAOYSA-N Melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 4
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims abstract description 4
- KAKZBPTYRLMSJV-UHFFFAOYSA-N butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 4
- -1 carbon alcohols esters Chemical class 0.000 claims abstract description 4
- 239000003822 epoxy resin Substances 0.000 claims abstract description 4
- 235000019837 monoammonium phosphate Nutrition 0.000 claims abstract description 4
- 229960001735 pentaerythritol Drugs 0.000 claims abstract description 4
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 4
- 239000008117 stearic acid Substances 0.000 claims abstract description 4
- ATJFFYVFTNAWJD-UHFFFAOYSA-N tin hydride Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims abstract description 4
- DPQXAUXLLDWUMQ-UHFFFAOYSA-L zinc;naphthalene-2-carboxylate Chemical compound [Zn+2].C1=CC=CC2=CC(C(=O)[O-])=CC=C21.C1=CC=CC2=CC(C(=O)[O-])=CC=C21 DPQXAUXLLDWUMQ-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229920001276 Ammonium polyphosphate Polymers 0.000 claims abstract description 3
- 239000004135 Bone phosphate Substances 0.000 claims description 6
- LWIHDJKSTIGBAC-UHFFFAOYSA-K Tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 claims description 6
- 229910001679 gibbsite Inorganic materials 0.000 claims description 6
- 229910001710 laterite Inorganic materials 0.000 claims description 6
- 239000011504 laterite Substances 0.000 claims description 6
- PIJPYDMVFNTHIP-UHFFFAOYSA-L Lead sulfate Chemical compound [PbH4+2].[O-]S([O-])(=O)=O PIJPYDMVFNTHIP-UHFFFAOYSA-L 0.000 claims description 5
- 239000004115 Sodium Silicate Substances 0.000 claims description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N Sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 4
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 3
- 235000019438 castor oil Nutrition 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000005984 hydrogenation reaction Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 abstract description 5
- 238000000576 coating method Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 230000032683 aging Effects 0.000 abstract description 2
- 239000003063 flame retardant Substances 0.000 abstract description 2
- 238000009472 formulation Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 101710041953 ApepP Proteins 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 230000003260 anti-sepsis Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- SMBGWMJTOOLQHN-UHFFFAOYSA-N lead;sulfuric acid Chemical compound [Pb].OS(O)(=O)=O SMBGWMJTOOLQHN-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
Abstract
The invention discloses a kind of facing type fireproofing powder paint, it is made up of the raw material of following weight parts: E 42 epoxy resin 60 70, diethylenetriamines 10 16, APP 12, tripolycyanamide 12, tetramethylolmethane 23, aluminium nitride 7 10, double ten four carbon alcohols esters 23, ammonium dihydrogen phosphate 12, zinc naphthenate 12, stearic acid 23, butadiene 0.3 0.6, butanethiol stannum 12, compounded mix 10 20；The coating of the present invention has the decay of preferable durability, resistance to water, rub resistance and stain resistance, especially fire retardant effect and ageing resistance more preferably, and formulation cost and production and processing cost are relatively low, are prone to practical operation.
Description
Technical field
The invention mainly relates to a kind of coating, particularly relate to a kind of facing type fireproofing powder paint.
Background technology
Powdery paints, as environmental protection, product energy-conservation, economic, efficient, gradually replaces liquid paint, become development speed and
The coating new technique that scale is the fastest.In current art of powder coatings, it is essentially all common indoor decorative powdery paints or family
Outer weather-resistance powder coatings.Functional powder coating also relates to epoxy heavy antisepsis type, conductivity type, insulated type, the type of resistance to combustion, scumbling
The fields such as type, therefore research novel high-performance powdery paints can act as preferably assisting for nation-building, social life
Effect.
Summary of the invention
The object of the invention is contemplated to provide a kind of facing type fireproofing powder paint.
The present invention is achieved by the following technical solutions:
A kind of facing type fireproofing powder paint, it is characterised in that it is made up of the raw material of following weight parts:
E-42 epoxy resin 60-70, diethylenetriamines 10-16, APP 1-2, tripolycyanamide 1-2, tetramethylolmethane
2-3, aluminium nitride 7-10, double ten four carbon alcohols ester 2-3, ammonium dihydrogen phosphate 1-2, zinc naphthenate 1-2, stearic acid 2-3, butadiene 0.3-
0.6, butanethiol stannum 1-2, compounded mix 10-20；
Described compounded mix is made up of the raw material of following weight parts:
Gibbsite 10-20, laterite 30-40, aluminium nitride 4-6, sodium silicate 3-4, castor oil acid 1-2, OPE
3-4, lead sulfate tribasic 0.1-0.2；
By above-mentioned laterite, gibbsite mixing, at 500-600 DEG C calcine 3-5 hour, discharging cooling after, with aluminium nitride,
Sodium silicate, lead sulfate tribasic mix, and add suitable quantity of water and grind, and the hydrochloric acid regulation PH adding 10-20% is 4-5, is heated to system temperature
For 70-90 DEG C, being ground to fineness is 300-400 mesh, and repeated hydrogenation sodium oxide is adjusted to neutrality, is spray-dried, obtains powder；By gained
Powder mixes with other residual components, grinds and uniformly i.e. obtains described compounded mix.
The preparation method of a kind of facing type fireproofing powder paint, comprises the following steps:
By above-mentioned each raw material mix after, input extruder melt extrude, air-cooled, pulverize in pulverizer, then
Pulverizing, sieves, and obtains described facing type fireproofing powder paint.
The invention have the advantage that
The coating of the present invention has preferable durability, resistance to water, rub resistance and stain resistance, especially fire-retardant fireproof
More preferably, formulation cost and production and processing cost are relatively low, are prone to practical operation for effect and ageing resistance decay.
Detailed description of the invention
Embodiment 1,
A kind of facing type fireproofing powder paint, it is made up of the raw material of following weight parts (kilogram):
E-42 epoxy resin 70, diethylenetriamines 16, APP 1, tripolycyanamide 2, tetramethylolmethane 2, aluminium nitride 10,
Double ten four carbon alcohols esters 2, ammonium dihydrogen phosphate 2, zinc naphthenate 2, stearic acid 2-3, butadiene 0.6, butanethiol stannum 1, compounded mix
20；
Described compounded mix is made up of the raw material of following weight parts:
Gibbsite 20, laterite 40, aluminium nitride 6, sodium silicate 3, castor oil acid 1, OPE 3, tribasic sulphuric acid
Lead 0.2；
By above-mentioned laterite, gibbsite mixing, calcine 3 hours at 600 DEG C, after discharging cooling, with aluminium nitride, flower bulb
Alkali, lead sulfate tribasic mix, and add suitable quantity of water and grind, and the hydrochloric acid regulation PH adding 20% is 4-5, and being heated to system temperature is 90 DEG C,
Being ground to fineness is 400 mesh, and repeated hydrogenation sodium oxide is adjusted to neutrality, is spray-dried, obtains powder；Gained powder is remained with other
Composition mixes, and grinds and uniformly i.e. obtains described compounded mix.
The preparation method of a kind of facing type fireproofing powder paint, comprises the following steps:
By above-mentioned each raw material mix after, input extruder melt extrude, air-cooled, pulverize in pulverizer, then
Pulverizing, sieves, and obtains described facing type fireproofing powder paint.
Performance test:
Solvent resistant: 240 hours, unchanged；
Salt spray test (1000h): unchanged.
Claims (2)
1. a facing type fireproofing powder paint, it is characterised in that it is made up of the raw material of following weight parts:
E-42 epoxy resin 60-70, diethylenetriamines 10-16, APP 1-2, tripolycyanamide 1-2, tetramethylolmethane 2-3,
Aluminium nitride 7-10, double ten four carbon alcohols ester 2-3, ammonium dihydrogen phosphate 1-2, zinc naphthenate 1-2, stearic acid 2-3, butadiene 0.3-0.6,
Butanethiol stannum 1-2, compounded mix 10-20；
Described compounded mix is made up of the raw material of following weight parts:
Gibbsite 10-20, laterite 30-40, aluminium nitride 4-6, sodium silicate 3-4, castor oil acid 1-2, OPE 3-4,
Lead sulfate tribasic 0.1-0.2；
By above-mentioned laterite, gibbsite mixing, calcine 3-5 hour at 500-600 DEG C, after discharging cooling, with aluminium nitride, flower bulb
Alkali, lead sulfate tribasic mix, and add suitable quantity of water and grind, and the salt acid for adjusting pH adding 10-20% is 4-5, is heated to system temperature and is
70-90 DEG C, being ground to fineness is 300-400 mesh, and repeated hydrogenation sodium oxide is adjusted to neutrality, is spray-dried, obtains powder；By gained powder
End mixes with other residual components, grinds and uniformly i.e. obtains described compounded mix.
2. the preparation method of a facing type fireproofing powder paint as claimed in claim 1, it is characterised in that include following step
Rapid:
By above-mentioned each raw material mix after, input extruder melt extrude, air-cooled, pulverize in pulverizer, then pulverizing,
Sieve, obtain described facing type fireproofing powder paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310395994.7A CN103497629B (en) | 2013-09-04 | A kind of facing type fireproofing powder paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310395994.7A CN103497629B (en) | 2013-09-04 | A kind of facing type fireproofing powder paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103497629A CN103497629A (en) | 2014-01-08 |
| CN103497629B true CN103497629B (en) | 2016-11-30 |
Family
ID=
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434804A (en) * | 2007-11-17 | 2009-05-20 | 徐州正菱涂装有限公司 | Facing type fireproofing powder paint |
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434804A (en) * | 2007-11-17 | 2009-05-20 | 徐州正菱涂装有限公司 | Facing type fireproofing powder paint |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Xiao Xiaomei Inventor before: Song Yuchun |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20161008 Address after: 362417 Anxi County, Quanzhou Province peach boat township I Pei Pei Pei Village, No. 23 Applicant after: Xiao Xiaomei Address before: 233000 No. 404 South Daqing Road, hi tech Zone, Anhui, Bengbu Applicant before: Anhui Topusen Battery Co., Ltd. |
|
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Liu Zhiying Inventor before: Xiao Xiaomei |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20170505 Address after: 100076 Beijing city Daxing District town of Xihongmen Xinhe Road No. 1 Patentee after: Beijing Cheonan Puning fire fighting material factory Address before: 362417 Anxi County, Quanzhou Province peach boat township I Pei Pei Pei Village, No. 23 Patentee before: Xiao Xiaomei |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161130 Termination date: 20190904 |