CN103468136A - Environment-friendly waterproof coating - Google Patents
Environment-friendly waterproof coating Download PDFInfo
- Publication number
- CN103468136A CN103468136A CN2013103592321A CN201310359232A CN103468136A CN 103468136 A CN103468136 A CN 103468136A CN 2013103592321 A CN2013103592321 A CN 2013103592321A CN 201310359232 A CN201310359232 A CN 201310359232A CN 103468136 A CN103468136 A CN 103468136A
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- CN
- China
- Prior art keywords
- parts
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- stirring
- environment
- film coalescence
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011248 coating agent Substances 0.000 title abstract description 6
- 238000000576 coating method Methods 0.000 title abstract description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 14
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 13
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000011609 ammonium molybdate Substances 0.000 claims abstract description 7
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims abstract description 7
- 229940010552 ammonium molybdate Drugs 0.000 claims abstract description 7
- 235000018660 ammonium molybdate Nutrition 0.000 claims abstract description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 229920002379 silicone rubber Polymers 0.000 claims abstract description 7
- 239000010456 wollastonite Substances 0.000 claims abstract description 7
- 229910052882 wollastonite Inorganic materials 0.000 claims abstract description 7
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims abstract description 4
- 235000010489 acacia gum Nutrition 0.000 claims abstract description 4
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 polyoxyethylene Polymers 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 18
- 238000004581 coalescence Methods 0.000 claims description 16
- 239000003973 paint Substances 0.000 claims description 13
- 239000000839 emulsion Substances 0.000 claims description 12
- IQXJCCZJOIKIAD-UHFFFAOYSA-N 1-(2-methoxyethoxy)hexadecane Chemical compound CCCCCCCCCCCCCCCCOCCOC IQXJCCZJOIKIAD-UHFFFAOYSA-N 0.000 claims description 6
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 6
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 6
- 229950009789 cetomacrogol 1000 Drugs 0.000 claims description 6
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- 229920002689 polyvinyl acetate Polymers 0.000 claims description 6
- 239000011118 polyvinyl acetate Substances 0.000 claims description 6
- CUVLMZNMSPJDON-UHFFFAOYSA-N 1-(1-butoxypropan-2-yloxy)propan-2-ol Chemical compound CCCCOCC(C)OCC(C)O CUVLMZNMSPJDON-UHFFFAOYSA-N 0.000 claims description 3
- 229920000084 Gum arabic Polymers 0.000 claims description 3
- 241000978776 Senegalia senegal Species 0.000 claims description 3
- 239000000205 acacia gum Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 2
- 239000010426 asphalt Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 2
- 229920001971 elastomer Polymers 0.000 abstract description 2
- 239000001785 acacia senegal l. willd gum Substances 0.000 abstract 1
- 239000011247 coating layer Substances 0.000 abstract 1
- 230000007774 longterm Effects 0.000 abstract 1
- 239000004945 silicone rubber Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 238000010276 construction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses an environment-friendly waterproof coating which is composed of the following raw materials in parts by weight: 60-70 parts of asphalt, 10-15 parts of 704 silicone rubber, 2-3 parts of Arabic gum, 4-6 parts of furfural extract oil, 1-2 parts of alkylphenol polyoxyethylene, 1-2 parts of ammonium molybdate, 2-3 parts of ethyl acrylate, 10-12 parts of wollastonite powder, 10-15 parts of light calcium carbonate, 1-2 parts of 3-aminopropyl trimethoxysilane, 2-4 parts of a film coalescing aid, and a proper amount of water. The asphalt and rubber molecules are completely dissolved into a whole and cooperate with the film coalescing aid, an obtained coating layer is stable and tough, can be firmly adhered on basal planes, and generates long-term and effective waterproof protection effects.
Description
Technical field
The present invention relates generally to a kind of coating, relates in particular to a kind of environment-friendly type waterproof paint.
Background technology
Emulsified bitumen coating has certain water-repellancy and preservative property, restriction due to the performance of pitch own, the work-ing life of Emulsificated asphalt water-proof painting material is short, the poor-performings such as health is strong, low temperature flexibility and thermotolerance, be applicable to classification of waterproof and be the industry of III, IV level and civil building roof covering, lavatory bathe between the construction of waterproof layer and underground protection against the tide, corrosion protection coating, be cheap low-grade waterproof paint, therefore, improving the over-all properties of Emulsificated asphalt water-proof painting material, is necessary in order to enlarge usage range.
Summary of the invention
The object of the invention just is to provide a kind of environment-friendly type waterproof paint.
The present invention is achieved by the following technical solutions:
A kind of environment-friendly type waterproof paint, it is comprised of the raw material of following weight parts:
Pitch 60-70,704 silicon rubber 10-15, gum arabic 2-3, furfural extract oil 4-6, alkylphenol polyoxyethylene 1-2, ammonium molybdate 1-2, ethyl propenoate 2-3, wollastonite powder 10-12, light calcium carbonate 10-15,3-aminopropyl trimethoxysilane 1-2, film coalescence aid 2-4, water are appropriate;
Described film coalescence aid is comprised of the raw material of following weight parts:
EVA emulsion 40-50, polyvinyl acetate emulsion 5-6, vinyltriethoxysilane 4-5, dipropylene glycol butyl ether 1-2, cetomacrogol 1000 2-3, aluminium hydroxide 2-4, tin-antiomony oxide 0.1-0.2;
Above-mentioned cetomacrogol 1000 is mixed with aluminium hydroxide, 50-60 ℃ of lower stirring reaction 10-15 minute, add tin-antiomony oxide after being cooled to normal temperature, obtain Preblend, the EVA emulsion is mixed with polyvinyl acetate emulsion, after stirring, add vinyltriethoxysilane, 400-500 rev/min of dispersed with stirring 2-4 minute, add above-mentioned Preblend and each raw material of residue, the 100-120 ℃ of standing 1-2 hour of insulation, obtain described film coalescence aid.
A kind of preparation method of environment-friendly type waterproof paint comprises the following steps:
Add 704 silicon rubber, furfural extract oil in pitch, heating rising temperature, to 150-160 ℃, is ground with colloidal mill, reach fully dispersed till, be reduced to normal temperature, obtain Preblend; Above-mentioned wollastonite powder, ammonium molybdate, light calcium carbonate are mixed, add the 3-aminopropyl trimethoxysilane, 500-600 rev/min of dispersed with stirring 4-5 minute, with above-mentioned Preblend, mix, at 60-70 ℃ of lower dispersed with stirring 20-30 minute, add each raw material of thinking except film coalescence aid, after fully stirring, add film coalescence aid, obtain described environment-friendly type waterproof paint.
Advantage of the present invention is:
The present invention is fused pitch and rubber molecule in one fully, and coordinates film coalescence aid, and the coating obtained is stable, tough and tensile, can firmly cohere on basal plane, produces permanent effectively waterproofing protection effect.
Embodiment
Embodiment 1
A kind of environment-friendly type waterproof paint, it is comprised of the raw material of following weight parts (kilogram):
Pitch 70,704 silicon rubber 10, gum arabic 3, furfural extract oil 6, alkylphenol polyoxyethylene 2, ammonium molybdate 2, ethyl propenoate 3, wollastonite powder 12, light calcium carbonate 15,3-aminopropyl trimethoxysilane 2, film coalescence aid 2-4, water are appropriate;
Described film coalescence aid is comprised of the raw material of following weight parts:
EVA emulsion 50, polyvinyl acetate emulsion 6, vinyltriethoxysilane 5, dipropylene glycol butyl ether 2, cetomacrogol 1000 3, aluminium hydroxide 4, tin-antiomony oxide 0.2;
Above-mentioned cetomacrogol 1000 is mixed with aluminium hydroxide, 60 ℃ of lower stirring reactions 15 minutes, add tin-antiomony oxide after being cooled to normal temperature, obtain Preblend, the EVA emulsion is mixed with polyvinyl acetate emulsion, after stirring, add vinyltriethoxysilane, 400 rev/mins of dispersed with stirring 4 minutes, add above-mentioned Preblend and each raw material of residue, 120 ℃ are incubated standing 2 hours, obtain described film coalescence aid.
A kind of preparation method of environment-friendly type waterproof paint comprises the following steps:
Add 704 silicon rubber, furfural extract oil in pitch, heating rising temperature to 150 ℃, grind with colloidal mill, reach fully dispersed till, be reduced to normal temperature, obtain Preblend; Above-mentioned wollastonite powder, ammonium molybdate, light calcium carbonate are mixed, add the 3-aminopropyl trimethoxysilane, 600 rev/mins of dispersed with stirring 5 minutes, with above-mentioned Preblend, mix, 70 ℃ of lower dispersed with stirring 30 minutes, add each raw material of thinking except film coalescence aid, after fully stirring, add film coalescence aid, obtain described environment-friendly type waterproof paint.
Performance test:
Extensibility: 876%;
Cohesive strength: 2.63MPa;
Watertightness (0.3MPa, 40min): waterproof.
Claims (2)
1. an environment-friendly type waterproof paint is characterized in that what it was comprised of the raw material of following weight parts:
Pitch 60-70,704 silicon rubber 10-15, gum arabic 2-3, furfural extract oil 4-6, alkylphenol polyoxyethylene 1-2, ammonium molybdate 1-2, ethyl propenoate 2-3, wollastonite powder 10-12, light calcium carbonate 10-15,3-aminopropyl trimethoxysilane 1-2, film coalescence aid 2-4, water are appropriate;
Described film coalescence aid is comprised of the raw material of following weight parts:
EVA emulsion 40-50, polyvinyl acetate emulsion 5-6, vinyltriethoxysilane 4-5, dipropylene glycol butyl ether 1-2, cetomacrogol 1000 2-3, aluminium hydroxide 2-4, tin-antiomony oxide 0.1-0.2;
Above-mentioned cetomacrogol 1000 is mixed with aluminium hydroxide, 50-60 ℃ of lower stirring reaction 10-15 minute, add tin-antiomony oxide after being cooled to normal temperature, obtain Preblend, the EVA emulsion is mixed with polyvinyl acetate emulsion, after stirring, add vinyltriethoxysilane, 400-500 rev/min of dispersed with stirring 2-4 minute, add above-mentioned Preblend and each raw material of residue, the 100-120 ℃ of standing 1-2 hour of insulation, obtain described film coalescence aid.
2. the preparation method of an environment-friendly type waterproof paint as claimed in claim 1 is characterized in that comprising the following steps:
Add 704 silicon rubber, furfural extract oil in pitch, heating rising temperature, to 150-160 ℃, is ground with colloidal mill, reach fully dispersed till, be reduced to normal temperature, obtain Preblend; Above-mentioned wollastonite powder, ammonium molybdate, light calcium carbonate are mixed, add the 3-aminopropyl trimethoxysilane, 500-600 rev/min of dispersed with stirring 4-5 minute, with above-mentioned Preblend, mix, at 60-70 ℃ of lower dispersed with stirring 20-30 minute, add each raw material of thinking except film coalescence aid, after fully stirring, add film coalescence aid, obtain described environment-friendly type waterproof paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310359232.1A CN103468136B (en) | 2013-08-16 | 2013-08-16 | A kind of Environmental-protecwaterproof waterproof paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310359232.1A CN103468136B (en) | 2013-08-16 | 2013-08-16 | A kind of Environmental-protecwaterproof waterproof paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103468136A true CN103468136A (en) | 2013-12-25 |
| CN103468136B CN103468136B (en) | 2016-06-15 |
Family
ID=49793187
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310359232.1A Expired - Fee Related CN103468136B (en) | 2013-08-16 | 2013-08-16 | A kind of Environmental-protecwaterproof waterproof paint |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103468136B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103965784A (en) * | 2014-05-23 | 2014-08-06 | 南通恒隆化工有限公司 | Asphalt waterproof coating material |
| CN104119749A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Waterproof paint for architectural roofing waterproof layer |
| CN106010436A (en) * | 2016-07-29 | 2016-10-12 | 马书文 | Elastic waterproof glue and preparation method thereof |
| CN109251542A (en) * | 2018-08-16 | 2019-01-22 | 马鞍山市永固防水科技有限公司 | A kind of waterproof roll and preparation method thereof with compared with high-elongation |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1170022A (en) * | 1996-06-27 | 1998-01-14 | 耿耀宗 | Water based coating for automotive preventing stone hitting |
| JP3313255B2 (en) * | 1995-01-13 | 2002-08-12 | 株式会社ヤスヰ | Coating agent used for automatic application method |
| CN1613939A (en) * | 2004-09-16 | 2005-05-11 | 王耀波 | Waterproof sealing compound for asphalt road surface, production and applied constructing process |
| US20090275679A1 (en) * | 2008-04-30 | 2009-11-05 | Flanigan Theodore P | System and method for the pre-treatment of rubber-modified asphalt cement, and emulsions thereof |
| CN102936460A (en) * | 2012-09-20 | 2013-02-20 | 吴江市天源塑胶有限公司 | Asphalt rubber waterproof coating material |
-
2013
- 2013-08-16 CN CN201310359232.1A patent/CN103468136B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3313255B2 (en) * | 1995-01-13 | 2002-08-12 | 株式会社ヤスヰ | Coating agent used for automatic application method |
| CN1170022A (en) * | 1996-06-27 | 1998-01-14 | 耿耀宗 | Water based coating for automotive preventing stone hitting |
| CN1613939A (en) * | 2004-09-16 | 2005-05-11 | 王耀波 | Waterproof sealing compound for asphalt road surface, production and applied constructing process |
| US20090275679A1 (en) * | 2008-04-30 | 2009-11-05 | Flanigan Theodore P | System and method for the pre-treatment of rubber-modified asphalt cement, and emulsions thereof |
| CN102936460A (en) * | 2012-09-20 | 2013-02-20 | 吴江市天源塑胶有限公司 | Asphalt rubber waterproof coating material |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103965784A (en) * | 2014-05-23 | 2014-08-06 | 南通恒隆化工有限公司 | Asphalt waterproof coating material |
| CN104119749A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Waterproof paint for architectural roofing waterproof layer |
| CN106010436A (en) * | 2016-07-29 | 2016-10-12 | 马书文 | Elastic waterproof glue and preparation method thereof |
| CN106010436B (en) * | 2016-07-29 | 2017-11-03 | 马书文 | A kind of elastic water-proof glue and preparation method thereof |
| CN109251542A (en) * | 2018-08-16 | 2019-01-22 | 马鞍山市永固防水科技有限公司 | A kind of waterproof roll and preparation method thereof with compared with high-elongation |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103468136B (en) | 2016-06-15 |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP02 | Change in the address of a patent holder |
Address after: 236800 3 building 207, Hai Jing building, Qiaocheng District, Bozhou, Anhui Patentee after: ANHUI KUAILAI WATERPROOFING & ANTI-CORROSION Co.,Ltd. Address before: No.18, Shaoji Ershi Road, Banta Town, Laian County, Chuzhou City, Anhui Province Patentee before: ANHUI KUAILAI WATERPROOFING & ANTI-CORROSION Co.,Ltd. |
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| CP02 | Change in the address of a patent holder | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20201223 Address after: 236800 3 building 207, Hai Jing building, Qiaocheng District, Bozhou, Anhui Patentee after: BOZHOU WOYE INTELLECTUAL PROPERTY SERVICE Co.,Ltd. Address before: No.18, Shaoji Ershi Road, Banta Town, Laian County, Chuzhou City, Anhui Province Patentee before: ANHUI KUAILAI WATERPROOFING & ANTI-CORROSION Co.,Ltd. |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220616 Address after: 510640 room 2615, building 4, Qihe business park, No.4, Xintang street, Tianhe District, Guangzhou City, Guangdong Province Patentee after: Li Chao Address before: 236800 3 building 207, Hai Jing building, Qiaocheng District, Bozhou, Anhui Patentee before: BOZHOU WOYE INTELLECTUAL PROPERTY SERVICE Co.,Ltd. |
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| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160615 |