CN103463739B - A kind of preparation method of far-infrared material and equipment - Google Patents
A kind of preparation method of far-infrared material and equipment Download PDFInfo
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Abstract
The present invention relates to material manufacturing technology field, particularly relate to a kind of preparation method and equipment of far-infrared material, described preparation method comprises step: S1: carry out cooling freezing processing to base material, keeps a period of time t0 after reaching minimum temperature T0; S2: hyperthermic treatment is carried out to freezing base material, and in temperature-rise period, carry out polarization process; S3: stop heating up and polarization process, naturally cool to room temperature.The wavelength that described method can make common material discharge significantly improves at the normal emittance of the far infrared of 4 μm-16 μm, close to or reach the standard of far-infrared material.
Description
Technical field
The present invention relates to material manufacturing technology field, particularly relate to a kind of preparation method and equipment of far-infrared material.
Background technology
As everyone knows, wavelength is useful to human body at the far infrared of 4 μm-16 μm, and people are " light of life " also known as the far infrared of this wave-length coverage, and the Main Function of far infrared has: the activity that 1, have activated biomacromolecule; 2, the molecule of organism is enable to be excited and to be in higher vibrational state; 3, promote and improve blood circulation; 4, metabolism is strengthened; 5, immune function of human body is improved; 6, there is antiinflammatory, the effect of detumescence; 7, analgesic activity.
Common material common on the market, the wavelength of the material such as such as stainless steel material, leather, cloth release is only 2-3% at the normal emittance of the far infrared of 4 μm-16 μm, is the highlyest also no more than 10%, so do not have far-infrared health-care function.The material that the normal emittance of far infrared is higher is also called far-infrared material, such as far infrared mineral powder, the wavelength of far infrared mineral powder release generally can reach 90% at the normal emittance of the far infrared of 4 μm-16 μm, far-infrared material can be made into far infrared health care product, this series products mainly relies on and adds far-infrared material to realize health care, such as far-infrared material is attached to substrate surface, or in base material, mix far-infrared material, but after far-infrared material comes off, this series products is lost far infrared health care effect, effect duration is shorter.
Summary of the invention
The object of the present invention is to provide a kind of preparation method and equipment of far-infrared material, the wavelength that described preparation method can make common material discharge significantly improves at the normal emittance of the far infrared of 4 μm-16 μm, close to or reach the standard of far-infrared material.
The present invention is achieved in that a kind of preparation method of far-infrared material, comprises the following steps:
S1: carry out cooling freezing processing to base material, keeps a period of time t0 after reaching minimum temperature T0;
S2: hyperthermic treatment is carried out to freezing base material, and in temperature-rise period, carry out polarization process, temperature-rise period is every raised temperature when being Δ T, keep a period of time t1, the maximum temperature heated up is T1, and the total time of temperature-rise period is t2, and polarization process comprises and utilizes wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched base material, launch high-frequency electric wave to base material, described high-frequency electrical wave frequency evenly raises in temperature-rise period from 50HZ to 500000HZ simultaneously;
S3: stop heating up and polarization process, naturally cool to room temperature.
Wherein, described base material is placed in airtight cavity and completes preparation, in step sl, also comprises the operation described cavity being carried out to evacuation; In step s 2, sealing treatment is carried out to described cavity; In step s3, venting or air-breathing return to normal pressure naturally.
Wherein, described base material is stainless steel substrates, wherein, T0=-50 DEG C ~-260 DEG C, t0=10s ~ 72H, Δ T=3 DEG C ~ 20 DEG C, t1=10s ~ 3H, T1=100 DEG C ~ 200 DEG C, t2=1H ~ 30D.Preferably, T0=-260 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=200 DEG C, t2=30D.
Wherein, described base material is leather, wherein, T0=-50 DEG C ~-100 DEG C, t0=10s ~ 72H, Δ T=3 DEG C ~ 20 DEG C, t1=10s ~ 3H, T1=40 DEG C ~ 80 DEG C, t2=1H ~ 30D.Preferably, T0=-100 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=80 DEG C, t2=30D.
Wherein, described base material is beauty treatment emulsion, wherein, T0=-50 DEG C ~-220 DEG C, t0=10s ~ 72H, Δ T=3 DEG C ~ 20 DEG C, t1=10s ~ 3H, T1=40 DEG C ~ 80 DEG C, t2=1H ~ 30D.Preferably, T0=-220 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=80 DEG C, t2=30D.
Another kind of technical scheme of the present invention is: a kind of equipment realizing above-mentioned preparation method, and comprise casing, refrigerating plant, heater, vacuum extractor, infrared generator and high-frequency electric wave emitter, described casing comprises cavity and hermatic door.
Wherein, described casing is double-deck middle vacuum insulation construction, and described casing internal layer is the metal level of surface reflection.
Beneficial effect of the present invention is: the principle that the method for the invention works is: first carry out freezing to base material, base material of the present invention is common material, refer to that the wavelength that discharges at normal temperatures is at the lower material of the normal emittance of the far infrared of 4 μm-16 μm, with far-infrared material comparatively speaking, the light wave molecular structure meeting multilated of common material at a lower temperature, destroy Sum decomposition, the temperature time that is lower and that keep at low temperatures is longer, resolution or the damage degree of light wave molecular structure are higher, and the probability of structure restoration is less, when reaching the degree requirement of light wave molecule destroys, just can carry out hyperthermic treatment to common material, in temperature-rise period, polarization process is carried out to common material, the object of polarization process is the light ware energy utilized in environment, the information such as electric energy or energy, affect the reconstruct of freezing rear material light wave molecule, the present invention's process that polarizes adopts wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched common material, after wishing the specific light ware energy of light wave molecule absorption, can be fixed up with corresponding light wave molecular structure, when common material is cooled to room temperature, the wavelength of the far infrared light wave of release just can mainly concentrate in 4 μm-16 μm these wave-length coverages, the high-frequency electric wave why while light wave is launched, base material tranmitting frequency progressively raised, mainly because high-frequency electric wave can affect the formation of common material free charge, when common material is cooled to room temperature, a large amount of free charge can make the surface of material discharge micro-electric current, namely bio electricity is formed.Through above-mentioned freezing, to heat up and after polarization process, common material just close to or become far-infrared material, the material property consistent degree processed is very high, effect duration is long, significantly promote due to all common material far-infrared functionals almost can be made, so range of application is wider, and be very applicable to post-treatment, namely after utilizing common material making product to complete, only need through the method for the invention process once, just can become the health promoting product with far-infrared health care function, wide market.
Accompanying drawing explanation
Fig. 1 is the preparation method temperature and time graph of a relation of far-infrared material of the present invention;
Fig. 2 is the structural representation preparing the embodiment of far-infrared material equipment of the present invention;
Fig. 3 is the cross-sectional view preparing the embodiment of far-infrared material equipment of the present invention.
Wherein, 1, casing; 11, hermatic door; 2, refrigerating plant; 3, heater; 4, vacuum extractor; 5, infrared generator; 6, high-frequency electric wave emitter.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with accompanying drawing and embodiment, the present invention is further elaborated.
The invention discloses a kind of preparation method of far-infrared material, as shown in Figure 1, comprise the following steps:
S1: carry out cooling freezing processing to base material, keeps a period of time t0 after reaching minimum temperature T0;
S2: hyperthermic treatment is carried out to freezing base material, and in temperature-rise period, carry out polarization process, temperature-rise period is every raised temperature when being Δ T, keep a period of time t1, the maximum temperature heated up is T1, and the total time of temperature-rise period is t2, and polarization process comprises and utilizes wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched base material, launch high-frequency electric wave to base material, described high-frequency electrical wave frequency evenly raises in temperature-rise period from 50HZ to 500000HZ simultaneously;
S3: stop heating up and polarization process, naturally cool to room temperature.
The principle that the method for the invention works is: first carry out freezing to base material, base material of the present invention is common material, refer to that the wavelength that discharges at normal temperatures is at the lower material of the normal emittance of the far infrared of 4 μm-16 μm, with far-infrared material comparatively speaking, the light wave molecular structure meeting multilated of common material at a lower temperature, destroy Sum decomposition, the temperature time that is lower and that keep at low temperatures is longer, resolution or the damage degree of light wave molecular structure are higher, and the probability of structure restoration is less, when reaching the degree requirement of light wave molecule destroys, just can carry out hyperthermic treatment to common material, in temperature-rise period, polarization process is carried out to common material, the object of polarization process is the light ware energy utilized in environment, the information such as electric energy or energy, affect the reconstruct of freezing rear material light wave molecule, the present invention's process that polarizes adopts wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched common material, after wishing the specific light ware energy of light wave molecule absorption, can be fixed up with corresponding light wave molecular structure, when common material is cooled to room temperature, the wavelength of the far infrared light wave of release just can mainly concentrate in 4 μm-16 μm these wave-length coverages, the high-frequency electric wave why while light wave is launched, base material tranmitting frequency progressively raised, mainly because high-frequency electric wave can affect the formation of common material free charge, when common material is cooled to room temperature, a large amount of free charge can make the surface of material discharge micro-electric current, namely bio electricity is formed.Through above-mentioned freezing, to heat up and after polarization process, common material just close to or become far-infrared material, the material property consistent degree processed is very high, effect duration is long, significantly promote due to all common material far-infrared functionals almost can be made, so range of application is wider, and be very applicable to post-treatment, namely after utilizing common material making product to complete, only need through the method for the invention process once, just can become the health promoting product with far-infrared health care function, wide market.
Due to common material huge number, the freezing minimum temperature point that each material is suitable is inconsistent, and suitable intensification peak is also inconsistent, just substantially can determine preferably scope by many experiments.
In step sl, be very difficult owing to base material being down to extremely low temperature, so too not strict requirement to the speed of cooling.In step s 2, the control heated up to pole low temperature is also very difficult, so require also not strict.
In the present invention, in order to avoid the light of other wavelength is on the impact of material light wave Molecular remodeling, preferably base material is placed in lighttight airtight cavity and completes whole preparation process, can certainly complete in unglazed airtight room, in step sl, the operation described cavity being carried out to evacuation is also comprised; In step s 2, sealing treatment is carried out to described cavity; In step s3, venting or air-breathing return to normal pressure naturally, and the object of evacuation mainly only has just can make base material temperature be down to low-down temperature under negative pressure.
As the embodiment one of the preparation method of described far-infrared material, the base material of the present embodiment is common stainless steel substrates, thickness is 1mm, concrete model is SUS304, it is the common used material making pan, vessel, water heater, time untreated, the wavelength of release is only 2-3% at the normal emittance of the far infrared of 4 μm-16 μm, and preparation method comprises the following steps:
S1: carry out cooling freezing processing to base material, keeps a period of time 10s ~ 72H after reaching minimum temperature-50 DEG C ~-260 DEG C;
S2: hyperthermic treatment is carried out to freezing base material, and in temperature-rise period, carry out polarization process, temperature-rise period is every raised temperature when being 3 DEG C ~ 20 DEG C, keep a period of time 10s ~ 3H, the maximum temperature heated up is 100 DEG C ~ 200 DEG C, the total time of temperature-rise period is 1H ~ 30D, polarization process comprises and utilizes wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched base material, launch high-frequency electric wave to base material, described high-frequency electrical wave frequency evenly raises in temperature-rise period from 50HZ to 500000HZ simultaneously;
S3: stop heating up and polarization process, naturally cool to room temperature.
Stainless steel material starts multilated, destruction and decomposition being cooled to-50 DEG C of time wavelength-division minor structures, and-100 DEG C time, destructive rate can reach 20 ~ 30%, and-230 DEG C time, destructive rate can reach 90%, and-260 DEG C time, destructive rate can reach more than 95%.Longer at cryogenic hold-time, the state that light wave molecular structure is destroyed is more stable, and be more not easy to restore, namely under same cryogenic conditions, the retention time is longer, and destructive rate can slowly rise.
When heating up, programming rate is more slow better, and thermostatically controlled temperature interval is less, and every one-phase keeps the time of constant temperature longer, and polarization effect is better, can affect the reconstruct of light wave molecular structure more up hill and dale.Generally, be a hours when the whole polarization processing procedure time, namely polarization effect can detect, polarization effect completion rate 5-10%, and 15 days time, polarization effect completion rate is about 50%, and 30 days time, polarization effect completion rate is about 90%.Above data be the applicant experimentally Data Summary form, non-theoretical derived value.
The applicant designs many experiments, and corresponding product is delivered to national authority Spot detection, and the data drawn are as follows:
| T0 | t0 | ΔT | t1 | T1 | t2 | Normal emittance | |
| Experiment 1 | -50℃ | 10S | 20℃ | 10s | 100℃ | 1H | 20％ |
| Experiment 2 | -230℃ | 24H | 10℃ | 1H | 150℃ | 15D | 52％ |
| Experiment 3 | -260℃ | 72H | 3℃ | 3H | 200℃ | 30D | 62％ |
Can draw from above form, as T0=-260 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=200 DEG C, t2=30D, effect is better, and be preferred embodiment, normal emittance, more than 60%, can be made into various health care metallic article.
In addition, the micro-electric current adopting the substrate surface after above parameter processing to discharge, at about 0.1-5mA, can produce good health-care effect to human body.Traditional medicine thinks that the meridians of human body have the effect of certainly life and death, place's all kinds of diseases and ailments, and the disease of human body is all by making human body obtain rehabilitation to the conditioning of meridians in other words.Bio electricity channel collateral therapy is exactly take science of arteries and veins as principle, based on physiology, ancient Chinese medicine with modern Western medicine reflexology, combine electrobiology technology creation, the electric energy exported is after human body regulation and control, position residing for the trend of collaterals of human and disease, suitable electricity is adopted to use various maneuver, meridians are stimulated with electric energy, electric energy is conducted rapidly, get through that human body is impaired, the meridians of atrophy instantaneously, make energy and blood of human body unimpeded, body's immunity strengthens, the object of reach diseases prevention, curing the disease.
As the embodiment two of the preparation method of described far-infrared material, the base material of the present embodiment is the leather shoes finished product that the common leather of two pairs of different brands is made, and preparation method comprises the following steps:
S1: carry out cooling freezing processing to leather shoes, keeps a period of time 10s ~ 72H after reaching minimum temperature-50 DEG C ~-100 DEG C;
S2: hyperthermic treatment is carried out to freezing leather shoes, and in temperature-rise period, carry out polarization process, temperature-rise period is every raised temperature when being 3 DEG C ~ 20 DEG C, keep a period of time 10s ~ 3H, the maximum temperature heated up is 40 DEG C ~ 80 DEG C, the total time of temperature-rise period is 1H ~ 30D, polarization process comprises and utilizes wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched leather shoes, launch high-frequency electric wave to leather shoes, described high-frequency electrical wave frequency evenly raises in temperature-rise period from 50HZ to 500000HZ simultaneously;
S3: stop heating up and polarization process, naturally cool to room temperature.
Leather substance starts multilated, destruction and decomposition being cooled to-50 DEG C of time wavelength-division minor structures,-100 DEG C time, destructive rate can reach more than 50%, in order to prevent leather substance from obtaining irreversible destruction, minimum temperature should control more than-100 DEG C, and same maximum temperature should more than 80 DEG C.
The applicant designs many experiments, and corresponding product is delivered to national authority Spot detection, and the data drawn are as follows:
| T0 | t0 | ΔT | t1 | T1 | t2 | Normal emittance | |
| Experiment 1 | -50℃ | 10S | 20℃ | 10s | 40℃ | 1H | 32％ |
| Experiment 2 | -70℃ | 24H | 10℃ | 1H | 60℃ | 15D | 76％ |
| Experiment 3 | -100℃ | 72H | 3℃ | 3H | 80℃ | 30D | 87％ |
The test result of two pairs of leather shoes is very consistent, also illustrates that the stability of the method for the invention is very high.Can draw from above form, as T0=-100 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=80 DEG C, t2=30D, effect is better, is preferred embodiment.
In addition, the micro-electric current adopting the substrate surface after above parameter processing to discharge, at about 0.1-5mA, can produce good health-care effect to human body.
As the embodiment three of the preparation method of described far-infrared material, the base material of the present embodiment is beauty treatment emulsion on the market, and preparation method comprises the following steps:
S1: cooling freezing processing is carried out to beauty treatment emulsion, keeps a period of time 10s ~ 72H after reaching minimum temperature-50 DEG C ~-220 DEG C;
S2: hyperthermic treatment is carried out to freezing beauty treatment emulsion, and in temperature-rise period, carry out polarization process, temperature-rise period is every raised temperature when being 3 DEG C ~ 20 DEG C, keep a period of time 10s ~ 3H, the maximum temperature heated up is 40 DEG C ~ 80 DEG C, the total time of temperature-rise period is 1H ~ 30D, polarization process comprise utilize wavelength band be 4 μm-16 μm far infrared light wave to beauty treatment emulsion launch, launch high-frequency electric wave to beauty treatment emulsion, described high-frequency electrical wave frequency evenly raises in temperature-rise period from 50HZ to 500000HZ simultaneously;
S3: stop heating up and polarization process, naturally cool to room temperature.
Beauty treatment emulsion starts multilated, destruction and decomposition being cooled to-50 DEG C of time wavelength-division minor structures,-180 DEG C time, destructive rate can reach 50%, can more than 80% be reached at-220 DEG C of destructive rates, irreversible destruction is obtained in order to prevent beauty treatment emulsion, minimum temperature should control more than-220 DEG C, and same maximum temperature should more than 80 DEG C.
The applicant designs many experiments, and corresponding product is delivered to national authority Spot detection, and the data drawn are as follows:
| T0 | t0 | ΔT | t1 | T1 | t2 | Normal emittance | |
| Experiment 1 | -50℃ | 10S | 20℃ | 10s | 40℃ | 1H | 28％ |
| Experiment 2 | -180℃ | 24H | 10℃ | 1H | 60℃ | 15D | 67％ |
| Experiment 3 | -220℃ | 72H | 3℃ | 3H | 80℃ | 30D | 87％ |
Can draw from above form, as T0=-220 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=80 DEG C, t2=30D, effect is better, is preferred embodiment.
Applicant is also to the process that the multiple common materials such as glass, plastics, cloth are similar in addition, and the conclusion drawn is also substantially close, and the far-infrared effect of common material has and significantly significantly promotes.
The invention also discloses a kind of equipment of above-mentioned preparation method, as shown in Figures 2 and 3, comprise casing 1, refrigerating plant 2, heater 3, vacuum extractor 4, infrared generator 5 and high-frequency electric wave emitter 6, described casing 1 comprises cavity and openable hermatic door 11.Described refrigerating plant 2, for refrigeration, makes that the temperature in casing is minimum is down to-260 DEG C, and described heater 3 heats up for making base material, and described vacuum extractor 4 can make the cavity of casing 1 form negative pressure, is more conducive to lower the temperature.Described far infrared generator 5 can emission wavelength at the far infrared of 4 μm-16 μm, described high-frequency electric wave emitter 6 can control wave frequency and evenly raise in 50HZ-500000HZ, base material can be put into from described hermatic door 11 or take out, described equipment can carry out temperature and time control according to the program preset, and automatically completes all processing steps.
In the present embodiment, in order to better insulation, described casing 1 is double-deck middle vacuum insulation construction, and described casing 1 internal layer is the metal level of surface reflection, can the reflect heat of heater 3 on base material.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, several any amendment done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. a preparation method for far-infrared material, comprises the following steps:
S1: carry out cooling freezing processing to base material, keeps a period of time t0 after reaching minimum temperature T0;
S2: hyperthermic treatment is carried out to freezing base material, and in temperature-rise period, carry out polarization process, temperature-rise period is every raised temperature when being Δ T, keep a period of time t1, the maximum temperature heated up is T1, and the total time of temperature-rise period is t2, and polarization process comprises and utilizes wavelength band to be that the far infrared light wave of 4 μm-16 μm is launched base material, launch high-frequency electric wave to base material, described high-frequency electrical wave frequency evenly raises in temperature-rise period from 50HZ to 500000HZ simultaneously;
S3: stop heating up and polarization process, naturally cool to room temperature.
2. the preparation method of far-infrared material according to claim 1, it is characterized in that, described base material is stainless steel substrates, wherein, T0=-50 DEG C ~-260 DEG C, t0=10s ~ 72H, Δ T=3 DEG C ~ 20 DEG C, t1=10s ~ 3H, T1=100 DEG C ~ 200 DEG C, t2=1H ~ 30D.
3. the preparation method of far-infrared material according to claim 2, is characterized in that, T0=-260 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=200 DEG C, t2=30D.
4. the preparation method of far-infrared material according to claim 1, it is characterized in that, described base material is leather, wherein, and T0=-50 DEG C ~-100 DEG C, t0=10s ~ 72H, Δ T=3 DEG C ~ 20 DEG C, t1=10s ~ 3H, T1=40 DEG C ~ 80 DEG C, t2=1H ~ 30D.
5. the preparation method of far-infrared material according to claim 4, is characterized in that, T0=-100 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=80 DEG C, t2=30D.
6. the preparation method of far-infrared material according to claim 1, is characterized in that, described base material is beauty treatment emulsion, wherein, T0=-50 DEG C ~-220 DEG C, t0=10s ~ 72H, Δ T=3 DEG C ~ 20 DEG C, t1=10s ~ 3H, T1=40 DEG C ~ 80 DEG C, t2=1H ~ 30D.
7. the preparation method of far-infrared material according to claim 6, is characterized in that, T0=-220 DEG C, t0=72H, Δ T=3 DEG C, t1=3H, T1=80 DEG C, t2=30D.
8. realize an equipment for preparation method described in claim 1, it is characterized in that, comprise casing, refrigerating plant, heater, vacuum extractor, infrared generator and high-frequency electric wave emitter, described casing comprises cavity and hermatic door.
9. equipment according to claim 8, is characterized in that, described casing is double-deck middle vacuum insulation construction, and described casing internal layer is the metal level of surface reflection.
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| CN1315735A (en) * | 2000-03-26 | 2001-10-03 | 董元源 | Health-care far infrared magnet metal-base composite |
| CN101928554A (en) * | 2010-08-03 | 2010-12-29 | 王冰 | Magnetic energy-storage composite material, preparation method and application thereof |
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