CN106145108A - A kind of preparation method of medicinal carbon - Google Patents

A kind of preparation method of medicinal carbon Download PDF

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Publication number
CN106145108A
CN106145108A CN201610483361.5A CN201610483361A CN106145108A CN 106145108 A CN106145108 A CN 106145108A CN 201610483361 A CN201610483361 A CN 201610483361A CN 106145108 A CN106145108 A CN 106145108A
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Prior art keywords
preparation
retort
carbonization
dried
activation
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CN201610483361.5A
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Chinese (zh)
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凌云
赵晶晶
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Individual
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Individual
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Priority to CN201610483361.5A priority Critical patent/CN106145108A/en
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • C01P2006/82Compositional purity water content

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  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses the preparation method of a kind of medicinal carbon, it is with corncob as material, by carbonization, grind into powder, activate and drying steps make, utilize the minute aperture that activated carbon granule is covered with above, the thing cholesterol molecule of the nuisance in human body and surplus can be absorbed, become a kind of natural " filter ", the nuisance of human body and superfluous cholesterol can have been absorbed in vivo, thus play the effect of building body, eliminating toxin and beautifying the skin, blood fat reducing.

Description

A kind of preparation method of medicinal carbon
Technical field
The present invention relates to the preparation method of a kind of medicine, the preparation method of a kind of medicinal carbon Preparation method.
Background technology
By timber, the heated carbonization of xylocarp shell, then grinding as smalls, the activated carbon made is for treating hyperlipemia.Existing Generation research is thought, the minute aperture that activated carbon is covered with above, cholesterol molecule superfluous in food and in human body can be absorbed, and live Property charcoal be one " passerby " hurriedly, with the effect of digestive function of human body, excrete together with stool, can be in human body Nuisance and surplus thing cholesterol molecule absorb, become a kind of natural " filter ", having of human body can have been absorbed in vivo Pest and superfluous cholesterol, thus play the effect of building body, eliminating toxin and beautifying the skin, blood fat reducing.Its mechanism of action is, each broken Activated carbon granule surface, end has all been covered with microscopic pinholes, just because of have thousands of pores on charcoal granule, and one Natural " filter ", can filter gas and liquid so that it is becomes pure, and has no side effect.
Summary of the invention
Disclosed by the invention is a kind of medicinal carbon manufacture method, is with corncob as carbonated material, by following step Rapid preparation:
1) carbonization:
A. by the corncob after threshing, put into retort completely cuts off in air or anaerobic environment and heat, temperature control System, at 200~300 DEG C, after heating 3~4 hours, turns off thermal source, after natural cooling, obtains primary carbonization body A;
B. the primary carbonization body A obtained in step a is placed in retort and is warmed up to 600~700 DEG C and retort Fire door to be opened, and after primary carbonization body A naked light burns 30~60 minutes, retort completely cuts off air or is quickly closed by fire door Close, with cold water, naked light in retort is put out by water simultaneously, natural cooling 2~after 3 hours, obtain carbonization block B;
2) grind into powder: the carbonization block B pulverization that will obtain, sieve, obtain powdered carbon powder C;
3) activation: powdered carbon powder C is carried out activation processing, obtains activating charcoal end D;
4) it is dried: activation charcoal end D is put into and is dried process, obtain clinical active carbon powder E;
Wherein, step 1) a in, preferable temperature is 250 DEG C, and the time of heating is 4h, the primary carbonization body so obtained Just ratio is more thoroughly.
Wherein, further step 1) b in, the temperature being rapidly heated is 660 DEG C, and the time of naked light burning is 50 points Clock, till the degree then put out by water by naked light in retort with cold water is for can not see Mars.
Wherein further, step 2) in the sieve selected that sieves be 120 mesh sieve.
Wherein further, step 3) in the method for activation processing be: powdered carbon powder C is placed in steam kettle, at one Standard atmosphere is depressed, and the temperature controlled in steam kettle is 100 DEG C, distills 40~50 minutes, and that plays powdered carbon powder C is thorough Activation.
Wherein further, step 4) in the drying equipment of dried be drying baker, the temperature control of dried System is at 120~130 DEG C, and the water content of dried activated carbon end D is less than 5%.
The invention discloses the preparation method of a kind of medicinal carbon, be with corncob as material, by carbonization, grind into powder, Activation and drying steps make, and utilize the minute aperture that activated carbon granule is covered with above, can be the nuisance in human body and surplus Thing cholesterol molecule absorbs, and has become a kind of natural " filter ", and nuisance and the superfluous gallbladder that can absorb human body in vivo are solid Alcohol, thus play the effect of building body, eliminating toxin and beautifying the skin, blood fat reducing.
Detailed description of the invention
Elaborating embodiments of the invention below, the present embodiment is carried out under premised on technical solution of the present invention Implement, give detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to following enforcement Example.
Embodiment 1
The material selected is the corncob after threshing, including following preparation process:
1) carbonization:
A. by the corncob after threshing, putting into isolation air in retort and heat, temperature controls at 200 DEG C, heats 3 After hour, turn off thermal source, after natural cooling, obtain primary carbonization body A;
B. the primary carbonization body A obtained in step a is placed in retort and is warmed up to 600 DEG C, primary carbonization body A naked light After burning 30 minutes, retort being completely cut off air, put out by water by naked light in retort with cold water simultaneously, the degree put out by water is for can not see Till Mars, then natural cooling is after 2 hours, obtains carbonization block B;
2) grind into powder: the carbonization block B mortar pulverization that will obtain, sieve and use 120 mesh sieve, obtain powdered carbon powder C;
3) activation: powdered carbon powder C is carried out activation processing, and the method for activation processing is: powdered carbon powder C is placed in steam kettle In, to depress at a standard atmosphere, the temperature controlled in steam kettle is 100 DEG C, distills and within 40 minutes, obtains activating charcoal end D;
4) it is dried: being put into by activation charcoal end D and be dried process, the equipment of dried is drying baker, dried Temperature control at 120 DEG C, the water content of dried activated carbon end D be less than 5%, obtain clinical active carbon powder E;
Embodiment 2
The material selected is the corncob after threshing, including following preparation process:
1) carbonization:
A. by the corncob after threshing, putting into isolation air in retort and heat, temperature controls at 300 DEG C, heats 4 After hour, turn off thermal source, after natural cooling, obtain primary carbonization body A;
B. the primary carbonization body A obtained in step a is placed in retort and is warmed up to 700 DEG C, described primary carbonization body A After naked light burns 60 minutes, by retort fire door quick closedown, with cold water, naked light in retort is put out by water, with cold water by charcoal simultaneously Till the degree that in change stove, naked light is put out by water is for can not see Mars, then natural cooling is after 3 hours, obtains carbonization block B;
2) grinding into powder: the carbonization block B pulverization that will obtain, sieve, the sieve of selection is 120 mesh sieve, obtains powdered carbon powder End C;
3) activation: powdered carbon powder C is carried out activation processing, and the method for activation processing is: powdered carbon powder C is placed in steam kettle In, to depress at a standard atmosphere, the temperature controlled in steam kettle is 100 DEG C, distills 50 minutes, obtains activating charcoal end D;
4) it is dried: being put into by activation charcoal end D and be dried process, the equipment of dried is drying baker, dried Temperature control at 130 DEG C, the water content of dried activated carbon end D be less than 5%, obtain clinical active carbon powder E;
Embodiment 3
The material selected is the corncob after threshing, including following preparation process:
1) carbonization:
A. by the corncob after threshing, putting into isolation air in retort and heat, temperature controls at 250 DEG C, heats 4 After hour, turn off thermal source, after natural cooling, obtain primary carbonization body A;
B. the primary carbonization body A obtained in step a is placed in retort and is warmed up to 660 DEG C, described primary carbonization body A After naked light burns 50 minutes, retort is completely cut off air, with cold water, naked light in retort is put out by water, with cold water by retort simultaneously Till the degree that interior naked light is put out by water is for can not see Mars, then natural cooling is after 3 hours, obtains carbonization block B;
2) grinding into powder: the carbonization block B pulverization that will obtain, sieve, the sieve sieved is 120 mesh sieve, obtains powdered carbon Powder C;
3) activation: powdered carbon powder C is carried out activation processing, and the method for activation processing is: powdered carbon powder C is placed in steam kettle In, to depress at a standard atmosphere, the temperature controlled in steam kettle is 100 DEG C, distills 40~50 minutes, obtains activating charcoal end D;
4) it is dried: being put into by activation charcoal end D and be dried process, dried is drying baker, the temperature of dried Degree controls at 120 DEG C, and the water content of dried activated carbon end D is less than 5%, obtains clinical active carbon powder E.

Claims (6)

1. the preparation method of a medicinal carbon, it is characterised in that with corncob as carbonated material, by following steps system Standby:
1) carbonization:
A. by the corncob after threshing, putting into isolation air in retort and heat, temperature controls at 200~300 DEG C, heating After 3~4 hours, turn off thermal source, after natural cooling, obtain primary carbonization body A;
B. the primary carbonization body A obtained in step a is placed in retort and is warmed up to 600~700 DEG C, described primary carbonization body After A naked light burns 30~60 minutes, described retort is completely cut off air, with cold water, naked light in retort is put out by water simultaneously, natural After cooling down 2~3 hours, obtain carbonization block B;
2) grind into powder: the carbonization block B pulverization that will obtain, sieve, obtain powdered carbon powder C;
3) activation: powdered carbon powder C is carried out activation processing, obtains activating charcoal end D;
4) it is dried: activation charcoal end D is put into and is dried process, obtain clinical active carbon powder E.
The preparation method of a kind of medicinal carbon the most as claimed in claim 1, it is characterised in that step 1) a in, described temperature Degree is 250 DEG C, and the time of described heating is 4h.
The preparation method of a kind of medicinal carbon the most as claimed in claim 1, it is characterised in that described step 1) b in, institute Stating temperature is 660 DEG C, and the time of described naked light burning is 50 minutes, and the degree that naked light in retort is put out by water by described cold water is Till can not see Mars.
The preparation method of a kind of medicinal carbon the most as claimed in claim 1, it is characterised in that step 2) in described in sieve Sieve be 120 mesh sieve.
The preparation method of a kind of medicinal carbon the most as claimed in claim 1, it is characterised in that described step 3) at activation The method of reason is: be placed in steam kettle by powdered carbon powder C, depresses at a standard atmosphere, and the temperature controlled in steam kettle is 100 DEG C, distill 40~50 minutes.
The preparation method of a kind of medicinal carbon the most as claimed in claim 1, it is characterised in that step 4) in described be dried Process is drying baker, and the temperature of described dried controls at 120~130 DEG C, the water content of dried activated carbon end D Less than 5%.
CN201610483361.5A 2016-06-24 2016-06-24 A kind of preparation method of medicinal carbon Pending CN106145108A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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CN106145108A true CN106145108A (en) 2016-11-23

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106865544A (en) * 2017-03-27 2017-06-20 上海金湖活性炭有限公司 A kind of repeatable medical activated carbon for utilizing and its production method
CN107827105A (en) * 2017-12-05 2018-03-23 程庸堂 A kind of activated carbon for treating hyperlipemia

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1475439A (en) * 2002-08-15 2004-02-18 钱积才 Grain base medicine active carbon
CN101643208A (en) * 2009-01-16 2010-02-10 徐克文 Composite biological activated carbon and rapid preparation method thereof
CN102050446A (en) * 2010-12-18 2011-05-11 江苏技术师范学院 Method for preparing activated carbon by using corn cob
CN102442666A (en) * 2011-09-28 2012-05-09 青岛科技大学 Preparation method for biomass medicinal charcoal

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1475439A (en) * 2002-08-15 2004-02-18 钱积才 Grain base medicine active carbon
CN101643208A (en) * 2009-01-16 2010-02-10 徐克文 Composite biological activated carbon and rapid preparation method thereof
CN102050446A (en) * 2010-12-18 2011-05-11 江苏技术师范学院 Method for preparing activated carbon by using corn cob
CN102442666A (en) * 2011-09-28 2012-05-09 青岛科技大学 Preparation method for biomass medicinal charcoal

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
马宝岐等: "《半焦的利用》", 30 June 2014 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106865544A (en) * 2017-03-27 2017-06-20 上海金湖活性炭有限公司 A kind of repeatable medical activated carbon for utilizing and its production method
CN107827105A (en) * 2017-12-05 2018-03-23 程庸堂 A kind of activated carbon for treating hyperlipemia

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Application publication date: 20161123

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