CN103453732A - Microwave drying method capable of improving quality of fermented cordyceps sinensis hypha - Google Patents
Microwave drying method capable of improving quality of fermented cordyceps sinensis hypha Download PDFInfo
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- CN103453732A CN103453732A CN2013103922016A CN201310392201A CN103453732A CN 103453732 A CN103453732 A CN 103453732A CN 2013103922016 A CN2013103922016 A CN 2013103922016A CN 201310392201 A CN201310392201 A CN 201310392201A CN 103453732 A CN103453732 A CN 103453732A
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Abstract
The invention relates to a microwave drying method capable of improving the quality of fermented cordyceps sinensis hypha. The microwave drying method comprises the following steps that wet hypha with solid-liquid separation is laid on a conveying belt, and is dried by a tunnel type microwave drying oven, the thickness of the wet hypha is controlled to be 6-8mm, the speed of the conveying belt is controlled to be 0.2-1.2m/s, the microwave frequency is controlled to be 2450+/-500MHz, and the microwave power is controlled to be 65-68KW. The microwave drying method has the advantages that the damage to the quality of a product in the microwave drying process is furthest reduced and good economic benefit is brought for labor industrialization of the cordyceps sinensis.
Description
Technical field
The present invention relates to the technical field that artificial fermentation prepares Chinese caterpillar fungus bacterial filament, be specifically related to a kind of method for microwave drying that can significantly promote the quality of fermented aweto hypha.
Background technology
Cordyceps sinensis claims again Chinese caterpillar fungus, is China tradition rare Chinese medicine, has cough-relieving, reduces phlegm, reduces serum cholesterol, adjusting and enhancing immunity, the multiple pharmacological effect such as antitumor.In recent years, both at home and abroad the Cordyceps sinensis demand is increased severely.But because Cordyceps sinensis has its strict parasitics and special growth geographical environment, the output limited, the medicine source is more in short supply.For alleviating the imbalance between supply and demand in market, artificial fermentation's product of Cordyceps sinensis is more and more important.
When artificial fermentation prepares Chinese caterpillar fungus bacterial filament, need by mycelia and separation of fermentative broth mycelia part drying and crushing after fermentation ends.Prior art is general adopts traditional oven drying, or first utilizes that to dry tunnel predrying by it, and then with fluidized drying by its bone dry.The heating-up temperature of these methods is difficult to control, very easily that Chinese caterpillar fungus bacterial filament to be dried is burned, the roasting paste, thereby reduced the medicinal effects of Cordyceps sinensis, and adopt hot blast to be heated, or utilize far infrared quartz fluorescent tube and hot blast to combine and heated, exist heat utilization rate to hang down and the low shortcoming of drying efficiency.
Patent application CN200810019788 discloses a kind of for the fermented cordyceps sinensis mycelia extracting method, it is by the heating that mutually combines of hot air circulation and far infrared fluorescent tube, compare with the extracting method of patent application CN200410037116.9, improved operating efficiency, reduced energy consumption.But the quality of the fermented aweto hypha of its extraction is had a greatly reduced quality, substantially can meet the pharmacopeia specified standard.
Also have prior art to think, adopt the freeze drying fermented aweto hypha, in whole process temperature not higher than fermentation temperature, thereby good maintenance the active principle of metabolism or accumulation in the Cordyceps sinensis sweat.
The freeze-drying method that all relates to fermented aweto hypha in patent application CN200710149371, CN200910197957, the disclosed preparation method of CN201310124056, but quality of the Chinese caterpillar fungus bacterial filament of unexposed gained all.
For solving above-mentioned deficiency, existing prior art report: adopt the microwave drying fermented aweto hypha, can make heating object also become heater, therefore homogeneous heating, can not bake and stick with paste and burned product, and efficient energy-saving, drying time is short, and good practical value and economic worth are arranged.
Patent application CN200710308029 discloses a kind of method for microwave drying of Chinese caterpillar fungus bacterial filament powder, the method is to separate aweto strain from natural cordyceps, final bacterium liquid after repeatedly cultivating, remove filtrate after final bacterium liquid filters and obtain filter cake, it is characterized in that filter cake is removed to moisture with micro-wave drying method, the microwave drying condition is 2450 ± 500Hz, drying time 7-20 minute.But this patent has just roughly been introduced the method for microwave drying of fermented aweto hypha, and wherein the technological parameters such as device therefor, temperature, mode of heating are all undeclared, and the also quality of unexposed gained Chinese caterpillar fungus bacterial filament.
Patent application CN200910101753 discloses a kind of method for microwave drying of fermented cordyceps sinensis mycelia, it is by design tunnel type micro wave baking oven and Drying Technology Parameter thereof, comprise moisture etc. after baking temperature, drying time, hydrofuge frequency and discharging, make the fermented cordyceps sinensis mycelia drying efficiency high, reduce the advantages such as energy consumption and raising end product quality.Although this patent have been described in detail the technological parameter of microwave drying, the quality of the Chinese caterpillar fungus bacterial filament that this technique makes also can meet the pharmacopeia specified standard substantially.Method for microwave drying under this technological parameter still has certain destruction to the quality of Chinese caterpillar fungus bacterial filament as can be seen here.
Summary of the invention
For overcoming the deficiencies in the prior art, the present inventor finds by great many of experiments, method for microwave drying is the workload (kJ/g) that unit sample bears to the core influence factor of fermented aweto hypha, thereby again optimized the method for microwave drying of fermented aweto hypha, obtained that a kind of process stabilizing, drying efficiency are high, product quality is able to the method for microwave drying significantly promoted.
The present invention realizes by the following method:
A kind of method for microwave drying that can significantly promote the quality of fermented aweto hypha, it is characterized in that, after fermentation ends, Cordyceps fermented liquid, through Separation of Solid and Liquid, is got to the solid wet mycelia and is laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 6~8mm, the speed of described conveyer belt is controlled at 0.2~1.2m/s, and microwave frequency is controlled at 2450 ± 500MHz, and microwave power is controlled at 65~68KW.
Preferably, in above-mentioned method for microwave drying, the THICKNESS CONTROL of described wet mycelia is at 71mm.
Preferably, in above-mentioned method for microwave drying, the speed of described conveyer belt is controlled at 0.5~1.0m/s; 0.8m/s more preferably.
Preferably, in above-mentioned method for microwave drying, described microwave frequency is controlled at 2450MHz.
Preferably, in above-mentioned method for microwave drying, described microwave power is controlled at 66KW.
The invention has the advantages that: in the microwave drying process of fermented aweto hypha, the workload born by the control unit sample is to optimal conditions, thereby farthest reduce the destruction of microwave drying process to product quality, brought good economic benefit to the artificial industrialization of Cordyceps sinensis.
The specific embodiment
Embodiment 1
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 6mm, and the speed of described conveyer belt is controlled at 0.2m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 65KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
Embodiment 2
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 8mm, and the speed of described conveyer belt is controlled at 1.2m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 68KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
Embodiment 3
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 7mm, and the speed of described conveyer belt is controlled at 0.8m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 66KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
Reference examples 1
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 7mm, and the speed of described conveyer belt is controlled at 0.8m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 100KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
Reference examples 2
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 7mm, and the speed of described conveyer belt is controlled at 0.8m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 50KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
Reference examples 3
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 4mm, and the speed of described conveyer belt is controlled at 0.8m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 66KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
Reference examples 4
Cultured 28 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilized the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid.Get the solid wet mycelia and be laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 10mm, and the speed of described conveyer belt is controlled at 0.8m/s, and microwave frequency is controlled at 2450MHz, and microwave power is controlled at 66KW.Measure the water content of dry rear Chinese caterpillar fungus bacterial filament, make fermented aweto hypha.
The impact of the fermented aweto hypha that test example 1 microwave power makes microwave drying
Product according to following index to control group 1-2, embodiment 1-3 is contrasted, and wherein total amino acid, sweet mellow wine, adenosine content are the weight percentage in the Chinese caterpillar fungus bacterial filament dry product, concrete outcome see the following form (average that each numerical value is 10 batch samples):
Index | Standards of pharmacopoeia | Control group 1 | Control group 2 | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Total amino acid content (%) | ≥30 | 29.2 | 30.8 | 35.9 | 36.5 | 38.2 |
Mannitol content (%) | ≥7.0 | 7.3 | 6.7 | 9.7 | 9.9 | 11.5 |
Adenosine content (%) | ≥0.08 | 0.09 | 0.07 | 0.24 | 0.26 | 0.31 |
The impact of the fermented aweto hypha that the thickness of test example 2 wet mycelia makes microwave drying
Product according to following index to control group 3-4, embodiment 1-3 is contrasted, and wherein total amino acid, sweet mellow wine, adenosine content are the weight percentage in the Chinese caterpillar fungus bacterial filament dry product, concrete outcome see the following form (average that each numerical value is 10 batch samples):
Index | Standards of pharmacopoeia | Control group 3 | Control group 4 | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Total amino acid content (%) | ≥30 | 30.2 | 28.9 | 35.9 | 36.5 | 38.2 |
Mannitol content (%) | ≥7.0 | 7.0 | 7.1 | 9.7 | 9.9 | 11.5 |
Adenosine content (%) | ≥0.08 | 0.07 | 0.07 | 0.24 | 0.26 | 0.31 |
Reference examples 5
The fermented aweto tablet made according to the condition of embodiment 1 in patent application CN200910101753, process is:
Cultured 30 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilize the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid, the solid of gained is fermentation Cordyceps sinensis humidity strip, it is predrying that humidity strip utilizes the tunnel type micro wave drying oven to carry out, this baking oven length is 35 meters, wide is 1.4 meters, microwave frequency is 2450MHz, microwave complete machine general power is 200KW, baking temperature is 60 ℃ of left and right, be 5min drying time, the hydrofuge frequency is 45Hz, discharging after fermentation Cordyceps sinensis humidity strip moisture is 65%, then be cut into the humidity strip of about 1cm*1cm through slicer, it is put in the fluidized drying case again, while just dropping into, in the fluidized drying case, temperature is 50 ℃, temperature rises gradually, after 10min, temperature rises to 110 ℃, now, the moisture of fermented aweto tablet is 4% left and right, in the fluidized drying process, blower fan frequency basic controlling is at 45Hz.
Reference examples 6
The fermented aweto tablet made according to the condition of embodiment 1 in patent application CN200810019788, process is:
Cultured 30 tons of Cordyceps fermented liquids are squeezed in the high-order storage tank of 6 tons, utilize the pressure of potential difference and by by-pass valve control, zymotic fluid squeezed into to rotary drum with the speed of 10 tons/hour, utilize rotary drum that zymotic fluid is carried out to Separation of Solid and Liquid, the solid of gained ferment the Cordyceps sinensis humidity strip with the speed of 2m/min by drying tunnel, drying tunnel length is 18 meters left and right, wide is 0.8 meter left and right, the temperature of drying in tunnel is 60 ℃, be about 10min drying time, the hydrofuge frequency is 50Hz simultaneously, discharging after fermentation Cordyceps sinensis humidity strip moisture is about 78%, then be cut into the humidity strip of about 1cm*1cm through slicer, it is put in the fluidized drying case again, the EAT of fluidized drying case is 120 ℃, while just dropping into, in the fluidized drying case, temperature is 60 ℃, after 20min, temperature rises gradually, after 50min, temperature rises to 120 ℃, now, the moisture of fermented aweto tablet is 4.5% left and right, in the fluidized drying process, blower fan frequency basic controlling is at 50Hz.
Reference examples 7
The fermented aweto hypha made according to the condition of embodiment 1 in patent application CN200710308029, process is: isolate aweto strain from natural cordyceps, again the aweto strain of these separation is cultivated in culture medium, again these bacterial classifications after cultivating, the amplification of 2 grades are obtained to final bacterium liquid subsequently, final bacterium liquid is removed the filter cake of filtrate by the method for filtering, and filter cake is to obtain Chinese caterpillar fungus bacterial filament powder under the condition of 1950HZ left and right after dry 20 minutes at microwave condition.
Test example 3
Product according to following index to control group 5-7, embodiment 1-3 is contrasted, and wherein total amino acid, sweet mellow wine, adenosine content are the weight percentage in the Chinese caterpillar fungus bacterial filament dry product, concrete outcome see the following form (average that each numerical value is 10 batch samples):
Index | Standards of pharmacopoeia | Control group 5 | Control group 6 | Control group 7 | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Total amino acid content (%) | ≥30 | 32.1 | 32.2 | 30.3 | 35.9 | 36.5 | 38.2 |
Mannitol content (%) | ≥7.0 | 8.5 | 7.9 | 7.1 | 9.7 | 9.9 | 11.5 |
Adenosine content (%) | ≥0.08 | 0.16 | 0.15 | 0.09 | 0.24 | 0.26 | 0.31 |
By above-mentioned test example 1-3, can be drawn, the workload that unit sample bears is the central factor that affects the fermented aweto hypha method for microwave drying.With the workload of prior art or other numerical value, compare, the present invention optimizes the workload obtained can farthest reduce the destruction of microwave drying process to product quality, thereby obtained, a kind of process stabilizing, drying efficiency are high, product quality is able to the method for microwave drying significantly promoted, and bring good economic benefit to the artificial industrialization of Cordyceps sinensis.
Finally it should be noted that, the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment, the present invention is had been described in detail, for a person skilled in the art, its technical scheme that still can put down in writing aforementioned each embodiment is modified, or part technical characterictic wherein is equal to replacement.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (7)
1. the method for microwave drying that can significantly promote the quality of fermented aweto hypha, it is characterized in that, after fermentation ends, Cordyceps fermented liquid, through Separation of Solid and Liquid, is got to the solid wet mycelia and is laid on conveyer belt, by the tunnel type micro wave drying oven, carry out drying, the THICKNESS CONTROL of described wet mycelia is at 6~8mm, the speed of described conveyer belt is controlled at 0.2~1.2m/s, and microwave frequency is controlled at 2450+500MHz, and microwave power is controlled at 65~68KW.
2. method for microwave drying according to claim 1, is characterized in that, the THICKNESS CONTROL of described wet mycelia is at 7mm.
3. method for microwave drying according to claim 1, is characterized in that, the speed of described conveyer belt is controlled at 0.5~1.0m/s.
4. method for microwave drying according to claim 3, is characterized in that, the speed of described conveyer belt is controlled at 0.8m/s.
5. method for microwave drying according to claim 1, is characterized in that, described microwave frequency is controlled at 2450MHz.
6. method for microwave drying according to claim 1, is characterized in that, described microwave power is controlled at 66KW.
7. the fermented aweto hypha made by the described method for microwave drying of claim 1-6 any one.
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Citations (4)
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US6524539B1 (en) * | 1999-07-07 | 2003-02-25 | Helmut Katschnig | Microwave sterilization device |
CN101216237A (en) * | 2008-01-15 | 2008-07-09 | 天津市工业微生物研究所 | Method for drying high viscosity polymer by microwave |
CN101828751A (en) * | 2010-03-16 | 2010-09-15 | 天津实发中科百奥工业生物技术有限公司 | Method for drying natto |
CN101995145A (en) * | 2009-08-11 | 2011-03-30 | 杭州中美华东制药有限公司 | Method for drying fermented cordyceps sinensis mycelia |
-
2013
- 2013-08-27 CN CN2013103922016A patent/CN103453732A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6524539B1 (en) * | 1999-07-07 | 2003-02-25 | Helmut Katschnig | Microwave sterilization device |
CN101216237A (en) * | 2008-01-15 | 2008-07-09 | 天津市工业微生物研究所 | Method for drying high viscosity polymer by microwave |
CN101995145A (en) * | 2009-08-11 | 2011-03-30 | 杭州中美华东制药有限公司 | Method for drying fermented cordyceps sinensis mycelia |
CN101828751A (en) * | 2010-03-16 | 2010-09-15 | 天津实发中科百奥工业生物技术有限公司 | Method for drying natto |
Non-Patent Citations (1)
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