CN103450979A - Volatile solvent type antirust oil and preparation method thereof - Google Patents
Volatile solvent type antirust oil and preparation method thereof Download PDFInfo
- Publication number
- CN103450979A CN103450979A CN2012101729999A CN201210172999A CN103450979A CN 103450979 A CN103450979 A CN 103450979A CN 2012101729999 A CN2012101729999 A CN 2012101729999A CN 201210172999 A CN201210172999 A CN 201210172999A CN 103450979 A CN103450979 A CN 103450979A
- Authority
- CN
- China
- Prior art keywords
- oil
- volatile solvent
- solvent type
- acid ester
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Lubricants (AREA)
Abstract
The invention discloses a kind of volatile solvent type antirust oil and a preparation method thereof, and aims to provides a kind of volatile solvent type antirust oil, which has stable properties, a strong salt smog resistance property, and an excellent antirust property. To achieve the goals mentioned above, the volatile solvent type antirust oil is composed of petroleum antirust agent, dodecenylsuccinic acid ester, triazole, diisobutyl phthalate, long carbon chain alkanolamide, high carbon oxidized aliphatic ester, mineral base oil, and solvent oil.
Description
Technical field
The present invention relates to the slushing oil field, espespecially a kind of volatile solvent type slushing oil and preparation method thereof.
Background technology
Along with industrial expansion, the kind of steel product and kind are more and more, and along with the increase of outlet component, demand is increasing, also more and more higher to the performance requriements of slushing oil simultaneously.
The automobile component such as brake flange and brake facing, deposit the service requirements with the later stage because relating to the stock, mainly use solvent-borne type slushing oil and thin-layer rust-preventative oil, and existing solvent-borne type slushing oil, because of the restriction of its film forming properties, rust-preventive agent and film forming material are difficult to dissolve fully in solvent, and layering and deposited phenomenon easily occur after storing, and also there is certain deficiency in its salt fog resistance ability, also can't meet actual requirement fully to a certain extent.
Summary of the invention
A kind of volatile solvent type of the present invention slushing oil and preparation method thereof, is characterized in that, overcomes the deficiency of above-mentioned technology, and a kind of stable performance is provided, and the salt fog resistance performance is high, the volatile solvent type slushing oil of rustless property excellence.
Long carbochain alkylolamide has makes other rust inhibitors fully disperse in metallic surface, allow various rust inhibitors adsorb well in metallic surface with the acid amides bond energy of self and form the characteristic of fine and close adsorption layer in metallic surface, the high-adhesiveness of recycling high-carbon oxidation fatty acid ester, various inhibiter are fixed on to metallic surface firmly, thereby effectively stop corrosive medium to be immersed in metallic surface, obviously improved the salt fog resistance performance of slushing oil.
To achieve these goals, technology solution of the present invention is put case and is: described volatile solvent type slushing oil is by being comprised of oil rust-preventive agent, dodecenylsuccinic acid ester, 124 Triazole, diisobutyl phthalate, long carbochain alkylolamide, high-carbon oxidation fatty acid ester, mineral base oil and solvent oil, and each component and quality percentage composition thereof are:
Oil rust-preventive agent 12～18%
Dodecenylsuccinic acid ester 2～4%
124 Triazole 0.2～0.5%
Diisobutyl phthalate 0.5～1.5%
Long carbochain alkylolamide 0.5～1.5%
High-carbon oxidation fatty acid ester 1～2%
Mineral base oil 3～5%
Solvent oil 70～80%
Described oil rust-preventive agent, be selected from one or more in petroleum sodium sulfonate, barium mahogany sulfonate and calcium mahogany sulfonate, petroleum oxidate barium soap, dinonyl naphthalene sulfonate barium.
Described long carbochain alkylolamide is a kind of oiliness antirust function agent NEUF182.
Described high-carbon oxidation fatty acid ester is oxide ester MAXR23 a kind of light color, that adhesivity is good, resistance to abrasion is high.
Described mineral base oil, be selected from one or more in 75SN mineral base oil, 100SN mineral base oil and 150SN mineral base oil.
Described solvent oil, be selected from 120 ﹟ solvent oils or 200 ﹟ solvent oils.
The preparation method of volatile solvent type slushing oil is:
The mineral base oil of quality percentage composition is joined in still, be warming up to 80～90 ℃, add oil rust-preventive agent, after it dissolves fully, under the condition stirred, add successively dodecenylsuccinic acid ester, 124 Triazole, diisobutyl phthalate, long carbochain alkylolamide and the high-carbon oxidation fatty acid ester of quality percentage composition, stir 1～2 hour, each component is dissolved fully, stop stirring, be cooled to below 60 ℃, add the solvent oil of quality percentage composition, continue to stir, after mixing fully, stop stirring, filter, packing gets final product.
Embodiment
Embodiment 1
Salt fog resistance thin layer soft film anti-rust oil each component of composition and quality percentage composition thereof are:
Petroleum sodium sulfonate 7%
Petroleum oxidate barium soap 6.2%
Dinonyl naphthalene sulfonate barium 3.2%
Dodecenylsuccinic acid ester 3%
124 Triazole 0.2%
Diisobutyl phthalate 1%
Long carbochain alkylolamide 1%
High-carbon oxidation fatty acid ester 1.4%
Mineral base oil 5%
Solvent oil 72%
Wherein, long carbochain alkylolamide, be oiliness antirust function agent NEUF182; High-carbon oxidation fatty acid ester is the oxide ester MAXR23 that adhesivity is good, resistance to abrasion is high; Mineral base oil is the 75SN mineral base oil, 100SN mineral base oil and 150SN mineral base oil; Solvent oil is 120 ﹟ solvent oils (winter), 200 ﹟ solvent oils (summer).
The mineral base oil of 8.5 ㎏ is joined in still, be warming up to 80～90 ℃, the petroleum oxidate barium soap that adds 10.54 ㎏, 5.44 the petroleum sodium sulfonate of the dinonyl naphthalene sulfonate barium of ㎏ and 11.9 ㎏, after it dissolves fully, under the condition stirred, the dodecenylsuccinic acid ester that adds successively 5.1 ㎏, 0.34 the 124 Triazole of ㎏, 1.7 the diisobutyl phthalate of ㎏, 1.7 the long carbochain alkylolamide of ㎏ and the high-carbon oxidation fatty acid ester of 2.38 ㎏, stir 1～2 hour, each component is dissolved fully, stop stirring, be cooled to below 60 ℃, the solvent oil that adds 122.4 ㎏, continue to stir, after mixing fully, stop stirring, filter, packing gets final product.
Embodiment 1 is applicable to sealing up for safekeeping and deposit for a long time of ironcasting.
Embodiment 2
Salt fog resistance thin layer soft film anti-rust oil each component of composition and quality percentage composition thereof are:
Petroleum sodium sulfonate 4%
Barium mahogany sulfonate 2%
Petroleum oxidate barium soap 4%
Dinonyl naphthalene sulfonate barium 2.5%
Dodecenylsuccinic acid ester 2.2%
124 Triazole 0.2%
Diisobutyl phthalate 1%
Long carbochain alkylolamide 0.6%
High-carbon oxidation fatty acid ester 1%
Mineral base oil 4%
Solvent oil 78.5%
Wherein, long carbochain alkylolamide, be oiliness antirust function agent NEUF182; High-carbon oxidation fatty acid ester is the oxide ester MAXR23 that adhesivity is good, resistance to abrasion is high; Mineral base oil is 75SN mineral base oil, 100SN mineral base oil and 150SN mineral base oil.
The mineral base oil of 13.6 ㎏ is joined in still, be warming up to 80～90 ℃, the petroleum oxidate barium soap that adds 13.6 ㎏, 6.8 the barium mahogany sulfonate of ㎏, 8.5 the petroleum sodium sulfonate of the dinonyl naphthalene sulfonate barium of ㎏ and 13.6 ㎏, after it dissolves fully, under the condition stirred, the dodecenylsuccinic acid ester that adds successively 7.48 ㎏, 0.68 the 124 Triazole of ㎏, 3.4 the diisobutyl phthalate of ㎏, 2.04 the long carbochain alkylolamide of ㎏ and the high-carbon oxidation fatty acid ester of 3.4 ㎏, stir 1～2 hour, each component is dissolved fully, stop stirring, be cooled to below 60 ℃, the solvent oil that adds 266.9 ㎏, continue to stir, after mixing fully, stop stirring, filter, packing gets final product.
Embodiment 2 is applicable to sealing up for safekeeping and deposit for a long time of steel part or alloy steel piece.
The above; embodiment is only that the preferred embodiment of the present invention is described; not scope of the present invention is limited; under the prerequisite of the spirit that does not break away from the technology of the present invention; various distortion and improvement that this area engineering technical personnel make technical scheme of the present invention, all should fall in the definite protection domain of claims of the present invention.
Claims (3)
1. volatile solvent type slushing oil and preparation method thereof is characterized in that: overcome the deficiency of above-mentioned technology, a kind of stable performance is provided, the salt fog resistance performance is high, the volatile solvent type slushing oil of rustless property excellence.
2. a kind of volatile solvent type slushing oil according to claim 1 and preparation method thereof is characterized in that: described volatile solvent type slushing oil is by being comprised of oil rust-preventive agent, dodecenylsuccinic acid ester, 124 Triazole, diisobutyl phthalate, long carbochain alkylolamide, high-carbon oxidation fatty acid ester, mineral base oil and solvent oil.
3. a kind of volatile solvent type slushing oil according to claim 1 and preparation method thereof, it is characterized in that: the preparation method of described volatile solvent type slushing oil is: the mineral base oil of quality percentage composition is joined in still, be warming up to 80～90 ℃, add oil rust-preventive agent, after it dissolves fully, under the condition stirred, the dodecenylsuccinic acid ester that adds successively the quality percentage composition, 124 Triazole, diisobutyl phthalate, long carbochain alkylolamide and high-carbon oxidation fatty acid ester, stir 1～2 hour, each component is dissolved fully, stop stirring, be cooled to below 60 ℃, the solvent oil that adds the quality percentage composition, continue to stir, after mixing fully, stop stirring, filter, packing gets final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101729999A CN103450979A (en) | 2012-05-30 | 2012-05-30 | Volatile solvent type antirust oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101729999A CN103450979A (en) | 2012-05-30 | 2012-05-30 | Volatile solvent type antirust oil and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103450979A true CN103450979A (en) | 2013-12-18 |
Family
ID=49733823
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012101729999A Pending CN103450979A (en) | 2012-05-30 | 2012-05-30 | Volatile solvent type antirust oil and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103450979A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110283641A (en) * | 2019-05-24 | 2019-09-27 | 清华大学天津高端装备研究院 | A kind of cold-rolled steel sheet is electrostatically sprayed antirust oil and its preparation and performance test methods |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101892116A (en) * | 2010-07-21 | 2010-11-24 | 广西大学 | Environmentally friendly car parts antirust oil |
| CN102071088A (en) * | 2011-01-21 | 2011-05-25 | 山东卡松科技有限公司 | Antirust oil and preparation method thereof |
| CN102218530A (en) * | 2011-05-06 | 2011-10-19 | 烟台市牟平区留德润滑油销售有限公司 | Special anti-rust oil for iron powder stamping part |
-
2012
- 2012-05-30 CN CN2012101729999A patent/CN103450979A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101892116A (en) * | 2010-07-21 | 2010-11-24 | 广西大学 | Environmentally friendly car parts antirust oil |
| CN102071088A (en) * | 2011-01-21 | 2011-05-25 | 山东卡松科技有限公司 | Antirust oil and preparation method thereof |
| CN102218530A (en) * | 2011-05-06 | 2011-10-19 | 烟台市牟平区留德润滑油销售有限公司 | Special anti-rust oil for iron powder stamping part |
Non-Patent Citations (1)
| Title |
|---|
| 陆静等: "长碳链烷醇酰胺在防锈油中的应用研究", 《材料保护》, vol. 44, no. 10, 31 October 2011 (2011-10-31), pages 38 - 39 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110283641A (en) * | 2019-05-24 | 2019-09-27 | 清华大学天津高端装备研究院 | A kind of cold-rolled steel sheet is electrostatically sprayed antirust oil and its preparation and performance test methods |
| CN110283641B (en) * | 2019-05-24 | 2022-03-01 | 清华大学天津高端装备研究院 | Electrostatic spraying anti-rust oil for cold-rolled steel sheets and preparation and performance test methods thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103450969A (en) | Salt mist-resistant thin-layer soft film anti-rust oil composition | |
| CN103087808B (en) | Quick-drying hard film rust preventive oil and preparation method thereof | |
| CN101643683B (en) | Environmentally-friendly barium-free thixotropic antirust oil | |
| CN101475868B (en) | Sea environment green antirust grease | |
| CN108774574A (en) | A kind of total synthesis water-base antirust complexing agent and its evaluation method and application | |
| CN102994194B (en) | Synthetic multiple-effect lubricant additive and preparation method thereof | |
| CN100357415C (en) | Ultra-thin layered wax film antirust composition for firearm | |
| CN103525527B (en) | Film-cleaning anti-rust oil for automobile connecting rod, preparation method therefor and applications | |
| CN103374451B (en) | A kind of Food grade industrial gear oil composition | |
| CN104263475A (en) | Environment-friendly electrostatic spraying antirust oil and preparation method thereof | |
| CN102041149B (en) | Thin-layer antirust oil and preparation method thereof | |
| CN102344848A (en) | Bearing anti-corrosive oil composition | |
| CN104449970A (en) | Lubricating oil | |
| CN102585977A (en) | Maintaining grease for steel wire rope and production method of maintaining grease | |
| CN102337174B (en) | Gasholder sealing oil composition with high corrosion resistance and oxidation resistance | |
| KR20210005903A (en) | Environmentally friendly lubrication grease for steel ropes | |
| JP2728708B2 (en) | Corrosion inhibiting composition | |
| CN103450979A (en) | Volatile solvent type antirust oil and preparation method thereof | |
| CN105219483A (en) | A kind of spirit thinned type soft film anti-rust oil | |
| CN107474905A (en) | A kind of modified extruder lubricating oil | |
| RU2720004C1 (en) | Protective grease | |
| CN107353994A (en) | A kind of fully synthetic shaping dope of coating steel pipe | |
| CN104450013A (en) | Environmental-friendly long-acting sealing anti-rust oil composition and preparation method thereof | |
| CN104120439A (en) | Environment-friendly type water-based metal cleaning agent and manufacturing method thereof | |
| CN103450998A (en) | Hard-water resistance completely-synthesized cutting fluid and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20131218 |
|
| RJ01 | Rejection of invention patent application after publication |