CN103446020A - Cosmetics pigment composition containing safflower natural pigment extract and preparation method thereof - Google Patents

Cosmetics pigment composition containing safflower natural pigment extract and preparation method thereof Download PDF

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CN103446020A
CN103446020A CN2013103899749A CN201310389974A CN103446020A CN 103446020 A CN103446020 A CN 103446020A CN 2013103899749 A CN2013103899749 A CN 2013103899749A CN 201310389974 A CN201310389974 A CN 201310389974A CN 103446020 A CN103446020 A CN 103446020A
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flos carthami
water
natural pigment
hlb value
phase component
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CN103446020B (en
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章苏宁
马冬雪
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Guangzhou charm Cosmetics Co., Ltd.
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Shanghai Institute of Technology
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Abstract

The invention discloses a cosmetics pigment composition containing a safflower natural pigment extract and a preparation method thereof. The cosmetics pigment composition containing a safflower natural pigment extract comprises a water-phase component and an oil-phase component, wherein the water-phase component comprises distilled water, safflower natural pigment, coloring agent powder and a water-soluble liquid nonionic emulsifier with HLB value of greater than 7; the oil-phase component comprises an oil-soluble liquid nonionic emulsifier with HLB value of less than 7, liquid grease and a preservative. The preparation method comprises the following steps: preparing the safflower natural pigment before the water-phase component and oil-phase component; and adding the oil-phase component into the water-phase component and stirring uniformly to obtain the cosmetics pigment composition containing the safflower natural pigment extract, which is natural and safe with strong coloring and covering ability, low irritation, bright color and adjustable color as well as an antioxidant function; moreover, the preparation technology is simple and feasible, and the cosmetics pigment composition is suitable for the cosmetics pigment such as lipstick.

Description

A kind of color make-up color compositions containing Flos Carthami natural pigment extract and preparation method thereof
Technical field
The present invention relates to a kind of color make-up color compositions containing the natural pigment extract, relate in particular a kind of color make-up color compositions and preparation method containing Flos Carthami natural pigment extract.
Technical background
Coloring agent is the important source material composition of lipstick, and coloring agent commonly used has two classes: a class is water-soluble or oil-soluble dyes, by infiltrating through the outer surface of lip, makes lip painted; Another kind of is insoluble dyestuff, color lake and pigment, by pigment, forms dyed layer, forms photomask more or less, hides rough surface, makes lip surface smoothing light, thereby application is more extensive.
Generally, use the coloring agent of cosmetic material regulation and license, micro-lipstick works the mischief to health is unlikely.But lipstick contains pigment (pigment) after all, no matter be organic or inorganic pigment, mostly unhelpful to human body.Therefore, some natural edible pigments have caused people's interest gradually, and it can well solve the safety issue of coloring agent.Carthamin is beautiful in colour, can present claret-red, the different colours such as orange, yellow according to the height of concentration, there is higher nutritive value simultaneously, there is good application prospect with such pigment as the lipstick pigment but this pigment have an obvious shortcoming be exactly this pigment be water miscible, water colo(u)r is not suitable as the lipstick pigment and uses, the present invention is in order to overcome the above-mentioned shortcoming of carthamin for this reason, the stability of employing serial of methods raising pigment and the dispersibility of water-soluble pigment in lipstick raw material of the present invention are from natural, harmless.Pigment extracts from plant, loads on superfine titanic oxide or corn starch, is prepared into W/ O emulsified body, to health safety, and can improve the heat stability of pigment, makes its covering power higher.
Summary of the invention
One of purpose of the present invention is to provide a kind of color make-up color compositions containing the natural pigment extract containing a kind of color make-up color compositions containing Flos Carthami natural pigment extract, the contained Flos Carthami natural pigment that should contain the color make-up color compositions of Flos Carthami natural pigment extract is pure natural, safe, bright in luster, should be better containing the color make-up color compositions colour stability of Flos Carthami natural pigment extract, color divergence is even, and there is certain antioxidant effect, be applicable to the color make-up pigment such as lipstick.
Two of purpose of the present invention is to provide the preparation method of above-mentioned a kind of color make-up color compositions containing Flos Carthami natural pigment extract.
Technical scheme of the present invention
A kind of color make-up color compositions containing Flos Carthami natural pigment extract comprises water component and oil phase component:
Wherein said water component is greater than 7 water-soluble liquid nonionic emulsifier, coloring agent powder, Flos Carthami natural pigment and distilled water by the HLB value and mixes, calculate in mass ratio, the water-soluble liquid nonionic emulsifier that the HLB value is greater than 7: coloring agent powder: Flos Carthami natural pigment: distilled water is 1:2:2-10:5:
It is the liquid nonionic emulsifying agent that is applicable to prepare the O/W emulsion that wherein said HLB value is greater than 7 water-soluble liquid nonionic emulsifier, is preferably TWEEN80 etc.;
Prepared by the following method by described Flos Carthami natural pigment:
After Flos Carthami is dried to pulverizing, in the ethanol water that to join mass percent concentration be 50%, the ethanol water volume ratio calculating by weight that to control Flos Carthami and mass percent concentration be 50%, i.e. Flos Carthami: mass percent concentration is to obtain mixed liquor after ratio that 50% ethanol water is 1g:4-20ml is mixed;
By the mixed liquor of gained, at power 150W, under the ultrasound condition of frequency 40kHz, and to control temperature be 25 ℃, and the time is that 15-30min carries out supersound extraction, then uses 0.45 μ m filtering with microporous membrane;
Resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution;
The Flos Carthami extract concentrated solution of gained is controlled to temperature and for-55 ℃, carry out lyophilization, obtain the Flos Carthami natural pigment;
Described coloring agent powder is the mixture that superfine titanic oxide, corn starch or superfine titanic oxide and corn starch form, and the particle diameter of described coloring agent powder is 50-500nm;
Wherein said oil phase component is less than 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat by the HLB value and mixes;
Wherein to be less than 7 oil soluble liquid nonionic emulsifier be the liquid nonionic emulsifying agent that is applicable to prepare the W/O emulsion to the HLB value, is preferably SPAN80 etc., and its consumption is 2 times of the HLB value quality that is greater than 7 water-soluble liquid nonionic emulsifier;
The consumption of liquid fat is 20 times of distilled water consumption;
The consumption of antiseptic is the 0.1-0.3% of the color make-up color compositions gross mass containing Flos Carthami natural pigment extract;
Described liquid fat is a kind of or two or more in isopropyl palmitate, Jojoba oil, iso-octyl palmitate, isopropyl myristate, Trivent OCG, tricaprin, white oil, dimethicone, synthetic squalane;
Described antiseptic is one or more in methyl hydroxybenzoate, ethyl hydroxybenzoate, propyl hydroxybenzoate, butyl hydroxybenzoate.
The preparation method of above-mentioned a kind of color make-up color compositions containing Flos Carthami natural pigment extract, comprise the following steps:
(1), the extraction of Flos Carthami natural pigment
After Flos Carthami is dried to pulverizing, in the ethanol water that to join mass percent be 50%, the ethanol water that is 50% by Flos Carthami and mass percent volume ratio by weight calculates, i.e. Flos Carthami: the ratio that the ethanol water that mass percent is 50% is 1g:4-20ml obtains mixed liquor after being mixed;
By the mixed liquor of above-mentioned gained at power 150W, under the ultrasound condition of frequency 40kHz, and the control temperature is 25 ℃, time is that 15-30min carries out supersound extraction, then use 0.45 μ m filtering with microporous membrane, resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution;
The Flos Carthami extract concentrated solution of gained is controlled to temperature and for-55 ℃, carry out lyophilization, obtain the Flos Carthami natural pigment;
(2), the preparation of water component
Distilled water, Flos Carthami natural pigment, coloring agent powder and HLB value are greater than after 7 water-soluble liquid nonionic emulsifier is mixed and obtain the water component;
(3), the preparation of oil phase component
The HLB value is less than after 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat are mixed and obtains oil phase component;
(4), biphase emulsifying mixes
The water component of step (2) gained, under the condition stirred, is poured into oil phase component in the water component, and homogenizing or stirring 5-8min, after making water component and oil phase component mix homogeneously, obtain the color make-up color compositions containing Flos Carthami natural pigment extract.
Beneficial effect of the present invention
A kind of color make-up color compositions containing Flos Carthami natural pigment extract of the present invention, due to the Flos Carthami natural pigment adopted, be natural, therefore harmless.
Further, a kind of color make-up color compositions containing Flos Carthami natural pigment extract of the present invention, because the Flos Carthami natural pigment is attached on the coloring agent powder, thereby improved the Flos Carthami natural pigment at the heat stability containing in the color make-up color compositions of Flos Carthami natural pigment extract, made the higher and difficult decolouring of its covering power.
Further, the preparation method of a kind of color make-up color compositions containing Flos Carthami natural pigment extract of the present invention, because the method that adopts W/O emulsifying makes the color make-up color compositions containing Flos Carthami natural pigment extract of gained, be uniformly dispersed, and preparation technology is simple, is suitable for suitability for industrialized production.
The specific embodiment
Below by specific embodiment, the present invention is further set forth, but do not limit the present invention.
embodiment 1
A kind of color make-up color compositions containing Flos Carthami natural pigment extract comprises water component and oil phase component:
Wherein said water component is greater than 7 water-soluble liquid nonionic emulsifier, coloring agent powder, Flos Carthami natural pigment and distilled water by the HLB value and mixes, calculate in mass ratio, the water-soluble liquid nonionic emulsifier that the HLB value is greater than 7: coloring agent powder: Flos Carthami natural pigment: distilled water is 1:2:2:5:
It is TWEEN80 that wherein said HLB value is greater than 7 water-soluble liquid nonionic emulsifier;
Prepared by the following method by described Flos Carthami natural pigment:
After the 5g Flos Carthami is dried to pulverizing, in the ethanol water that the mass percent concentration that joins 20ml is 50%, the ethanol water that control Flos Carthami and mass percent concentration are 50% is volume ratio, i.e. Flos Carthami by weight: the ratio that the ethanol water that mass percent concentration is 50% is 1g:4ml obtains mixed liquor after being mixed;
By the mixed liquor of above-mentioned gained, at power 150W, under the ultrasound condition of frequency 40kHz, and to control temperature be 25 ℃, and the time is that 20min carries out supersound extraction, then uses 0.45 μ m filtering with microporous membrane;
Resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution;
The Flos Carthami extract concentrated solution of gained is controlled to temperature and for-55 ℃, carry out lyophilization, obtain 0.46g Flos Carthami natural pigment;
Described coloring agent powder is the superfine titanic oxide that particle diameter is 50-500nm;
Wherein said oil phase component is less than 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat by the HLB value and is obtained by mixing;
Wherein to be less than 7 oil soluble liquid nonionic emulsifier be SPAN-80 to the HLB value, and its consumption is 2 times of the HLB value quality that is greater than 7 water-soluble liquid nonionic emulsifier TWEEN80;
The consumption of liquid fat is 20 times of distilled water consumption;
The consumption of antiseptic is 0.145% of the color make-up color compositions gross mass containing Flos Carthami natural pigment extract;
Described liquid fat is that isopropyl palmitate, dimethicone calculate by volume, i.e. isopropyl palmitate: dimethicone is the mixture that 1:1 forms;
Described antiseptic is methyl hydroxybenzoate.
The preparation method of above-mentioned a kind of color make-up color compositions containing Flos Carthami natural pigment extract, comprise the following steps:
(1), get the 1mL distilled water, add 0.4g Flos Carthami natural pigment, the 0.4g superfine titanic oxide, the TWEEN-80 of 0.2g, obtain the water component after mix homogeneously;
(2), get 10mL dimethicone, 10mL isopropyl palmitate, 0.4gSPAN-80 and 0.03g methyl hydroxybenzoate, obtain oil phase component after mix homogeneously;
(3), by the water component of step (1) gained under the condition stirred, oil phase component is poured in the water component, homogenizing or stirring 5min, after making water component and oil phase component mix homogeneously, obtain the color make-up color compositions containing Flos Carthami natural pigment extract of 20.63g.
The color make-up color compositions containing Flos Carthami natural pigment extract of above-mentioned gained, through more than 80 ℃, heating 2h, color is without significant change.
embodiment 2
A kind of color make-up color compositions containing Flos Carthami natural pigment extract comprises water component and oil phase component:
Wherein said water component is greater than 7 water-soluble liquid nonionic emulsifier, coloring agent powder, Flos Carthami natural pigment and distilled water by the HLB value and mixes, calculate in mass ratio, the water-soluble liquid nonionic emulsifier that the HLB value is greater than 7: coloring agent powder: Flos Carthami natural pigment: distilled water is 1:2:2:5:
It is TWEEN80 that wherein said HLB value is greater than 7 water-soluble liquid nonionic emulsifier;
Prepared by the following method by described Flos Carthami natural pigment:
After the Flos Carthami of 5g is dried to pulverizing, in the ethanol water that the mass percent concentration that joins 50ml is 50%, control the ethanol water volume ratio calculating by weight that Flos Carthami and mass percent concentration are 50%, i.e. Flos Carthami: the ethanol water that mass percent concentration is 50% is to obtain mixed liquor after 1g:10ml is mixed;
By the mixed liquor of gained, at power 150W, under the ultrasound condition of frequency 40kHz, and to control temperature be 25 ℃, and the time is that 15-30min carries out supersound extraction and then uses 0.45 μ m filtering with microporous membrane;
Resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution;
The Flos Carthami extract concentrated solution of gained is controlled to temperature and for-55 ℃, carry out lyophilization, obtain the Flos Carthami natural pigment of 0.53g;
Described coloring agent powder is that the corn starch that the particle diameter superfine titanic oxide that is 50-500nm and particle diameter are 50-500nm calculates in mass ratio, i.e. superfine titanic oxide: the mixture that the ratio that corn starch is 1:1 forms;
Wherein said oil phase component is less than 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat by the HLB value and mixes;
Wherein to be less than 7 oil soluble liquid nonionic emulsifier be SPAN-80 to the HLB value, and its consumption is 2 times of the HLB value quality that is greater than 7 water-soluble liquid nonionic emulsifier TWEEN80;
The consumption of liquid fat is 20 times of distilled water consumption;
The consumption of antiseptic is 0.145% of the color make-up color compositions gross mass containing Flos Carthami natural pigment extract;
Described liquid fat is that isopropyl palmitate and dimethicone calculate by volume, i.e. isopropyl palmitate: dimethicone is the mixture that 1:1 forms;
Described antiseptic is methyl hydroxybenzoate.
The preparation method of above-mentioned a kind of color make-up color compositions containing Flos Carthami natural pigment extract, comprise the following steps:
(1), get the 1mL distilled water, add 0.4g Flos Carthami natural pigment, the 0.2g superfine titanic oxide, the 0.2g corn starch, the TWEEN-80 of 0.2g, obtain the water component after mix homogeneously;
(2), get 10mL dimethicone, 10mL isopropyl palmitate, 0.4g SPAN-80 and 0.03g methyl hydroxybenzoate, obtain oil phase component after mix homogeneously;
(3), by the water component of step (1) gained under the condition stirred, oil phase component is poured in the water component, homogenizing or stirring 8min, after making water component and oil phase component mix homogeneously, obtain the color make-up color compositions containing Flos Carthami natural pigment extract of 20.63g.
The color make-up color compositions containing Flos Carthami natural pigment extract of above-mentioned gained, through more than 80 ℃, heating 2h, color is without significant change.
embodiment 3
A kind of color make-up color compositions containing Flos Carthami natural pigment extract comprises water component and oil phase component:
Wherein said water component is greater than 7 water-soluble liquid nonionic emulsifier, coloring agent powder, Flos Carthami natural pigment and distilled water by the HLB value and mixes, calculate in mass ratio, the water-soluble liquid nonionic emulsifier that the HLB value is greater than 7: coloring agent powder: Flos Carthami natural pigment: distilled water is 1:2:5:5;
It is TWEEN80 that wherein said HLB value is greater than 7 water-soluble liquid nonionic emulsifier;
Prepared by the following method by described Flos Carthami natural pigment:
After the Flos Carthami of 10g is dried to pulverizing, in the ethanol water that the mass percent concentration that adds 200ml is 50%, the ethanol water that control Flos Carthami and mass percent concentration are 50% is volume ratio, i.e. Flos Carthami by weight: the ratio that the ethanol water that mass percent concentration is 50% is 1g:20ml obtains mixed liquor after being mixed;
By the mixed liquor of gained, at power 150W, under the ultrasound condition of frequency 40kHz, and to control temperature be 25 ℃, and the time is that 20min carries out supersound extraction, then uses 0.45 μ m filtering with microporous membrane;
Resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution;
The Flos Carthami extract concentrated solution of gained is controlled to temperature and for-55 ℃, carry out lyophilization, obtain the Flos Carthami natural pigment of 1.46g;
Described coloring agent powder is the superfine titanic oxide that particle diameter is 50-500nm;
Wherein said oil phase component is less than 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat by the HLB value and is obtained by mixing;
Wherein to be less than 7 oil soluble liquid nonionic emulsifier be SPAN-80 to the HLB value, and its consumption is 2 times that the HLB value is greater than 7 water-soluble liquid nonionic emulsifier TWEEN80;
The consumption of liquid fat is 20 times of distilled water consumption;
The consumption of antiseptic is 0.141% of the color make-up color compositions gross mass containing Flos Carthami natural pigment extract;
Described liquid fat is that isopropyl palmitate and dimethicone calculate by volume, i.e. isopropyl palmitate: dimethicone is the mixture that 1:1 forms;
Described antiseptic is methyl hydroxybenzoate.
The preparation method of above-mentioned a kind of color make-up color compositions containing Flos Carthami natural pigment extract, comprise the following steps:
(1), get the 1mL distilled water, add 1.0g Flos Carthami natural pigment, the 0.4g superfine titanic oxide, the TWEEN-80 of 0.2g, obtain the water component after mix homogeneously;
(2), get 10mL dimethicone, 10mL isopropyl palmitate, 0.4g SPAN-80 and 0.03g methyl hydroxybenzoate, obtain oil phase component after mix homogeneously;
(3), by the water component of step (1) gained under the condition stirred, oil phase component is poured in the water component, homogenizing or stirring 8min, after making water component and oil phase component mix homogeneously, obtain the color make-up color compositions containing Flos Carthami natural pigment extract of 21.23g.
The color make-up color compositions containing Flos Carthami natural pigment extract of above-mentioned gained, through more than 80 ℃, heating 2h, color is without significant change.
Above said content is the basic explanation under conceiving for the present invention only, and, according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.

Claims (4)

1. the color make-up color compositions containing Flos Carthami natural pigment extract, is characterized in that the described color make-up color compositions containing Flos Carthami natural pigment extract comprises water component and oil phase component;
Wherein said water component is greater than 7 water-soluble liquid nonionic emulsifier, coloring agent powder, Flos Carthami natural pigment and distilled water by the HLB value and mixes, calculate in mass ratio, the water-soluble liquid nonionic emulsifier that the HLB value is greater than 7: coloring agent powder: Flos Carthami natural pigment: distilled water is 1:2:2-10:5:
Prepared by the following method by described Flos Carthami natural pigment:
After Flos Carthami is dried to pulverizing, in the ethanol water that to join mass percent concentration be 50%, control the ethanol water volume ratio calculating by weight that Flos Carthami and mass percent concentration are 50%, i.e. Flos Carthami: the ethanol water that mass percent concentration is 50% is to obtain mixed liquor after 1g:4-20ml is mixed;
By the mixed liquor of gained, at power 150W, under the ultrasound condition of frequency 40kHz, and to control temperature be 25 ℃, and the time is that 15-30min carries out supersound extraction, then uses 0.45 μ m filtering with microporous membrane;
Resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution, concentrated solution is controlled to temperature and for-55 ℃, carry out lyophilization, obtain the Flos Carthami natural pigment;
Described coloring agent powder is the mixture that superfine titanic oxide, corn starch or superfine titanic oxide and corn starch form, and the particle diameter of described coloring agent powder is 50-500nm;
Wherein said oil-phase component is less than 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat by the HLB value and mixes;
Wherein to be less than the consumption of 7 oil soluble liquid nonionic emulsifier be 2 times of the above-mentioned HLB value quality that is greater than 7 water-soluble liquid nonionic emulsifier to the HLB value;
The consumption of liquid fat is 20 times of distilled water consumption;
The consumption of antiseptic is the 0.1-0.3% of the color make-up color compositions gross mass containing Flos Carthami natural pigment extract;
Described liquid fat is a kind of or two or more in isopropyl palmitate, Jojoba oil, iso-octyl palmitate, isopropyl myristate, Trivent OCG, tricaprin, white oil, dimethicone, synthetic squalane;
Described antiseptic is one or more in methyl hydroxybenzoate, ethyl hydroxybenzoate, propyl hydroxybenzoate, butyl hydroxybenzoate.
2. a kind of color make-up color compositions containing Flos Carthami natural pigment extract as claimed in claim 1, is characterized in that it is TWEEN80 that wherein said HLB value is greater than 7 water-soluble liquid nonionic emulsifier;
Described coloring agent powder is superfine titanic oxide;
It is SPAN80 that described HLB value is less than 7 oil soluble liquid nonionic emulsifier;
Described liquid fat is that isopropyl palmitate and dimethicone calculate by volume, i.e. isopropyl palmitate: dimethicone is the mixture that 1:1 forms;
Described antiseptic is methyl hydroxybenzoate.
3. a kind of color make-up color compositions containing Flos Carthami natural pigment extract as claimed in claim 1, is characterized in that it is TWEEN80 that wherein said HLB value is greater than 7 water-soluble liquid nonionic emulsifier;
Described coloring agent powder is that superfine titanic oxide and corn starch calculate in mass ratio, i.e. superfine titanic oxide: the mixture that the ratio that corn starch is 1:1 forms;
It is SPAN80 that described HLB value is less than 7 oil soluble liquid nonionic emulsifier;
Described liquid fat is that isopropyl palmitate and dimethicone calculate by volume, i.e. isopropyl palmitate: dimethicone is the mixture that 1:1 forms;
Described antiseptic is methyl hydroxybenzoate.
4. as the preparation method of claim 1,2 or 3 described a kind of color make-up color compositions containing Flos Carthami natural pigment extract, it is characterized in that specifically comprising the steps:
(1), the extraction of Flos Carthami natural pigment
After Flos Carthami is dried to pulverizing, in the ethanol water that to join mass percent be 50%, the ethanol water that is 50% by Flos Carthami and mass percent volume ratio by weight calculates, i.e. Flos Carthami: the ratio that the ethanol water that mass percent is 50% is 1:4-20 obtains mixed liquor after being mixed;
By the mixed liquor of above-mentioned gained at power 150W, under the ultrasound condition of frequency 40kHz, and the control temperature is 25 ℃, time is that 15-30min carries out supersound extraction, then use 0.45 μ m filtering with microporous membrane, resulting filtrate after filtering is controlled under the condition that vacuum is 0.094-0.096MPa and carried out rotary evaporation in vacuo, obtain the Flos Carthami extract concentrated solution;
The Flos Carthami extract concentrated solution of gained is controlled to temperature and for-55 ℃, carry out lyophilization, obtain the Flos Carthami natural pigment;
(2), the preparation of water component
Distilled water, Flos Carthami natural pigment, coloring agent powder and HLB value are greater than after 7 water-soluble liquid nonionic emulsifier is mixed and obtain the water component;
(3), the preparation of oil phase component
The HLB value is less than after 7 oil soluble liquid nonionic emulsifier, antiseptic and liquid fat are mixed and obtains oil phase component;
(4), biphase emulsifying mixes
Water component and oil phase component are separately after mix homogeneously, stir the water component on one side, slowly oil phase component is poured in the water component on one side, homogenizing or stir 5-8min make the water component and the oil phase component mixing and emulsifying even, obtain the color make-up color compositions containing Flos Carthami natural pigment extract.
CN201310389974.9A 2013-09-02 2013-09-02 Cosmetics pigment composition containing safflower natural pigment extract and preparation method thereof Active CN103446020B (en)

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CN106418131A (en) * 2016-11-22 2017-02-22 云南瑞宝生物科技股份有限公司 Preparation method of oil-soluble natural pigment
CN107412065A (en) * 2017-08-15 2017-12-01 刘后伟 A kind of lipstick of the pigment containing dragon fruit and preparation method thereof
CN107412065B (en) * 2017-08-15 2020-08-28 刘后伟 Lipstick containing pitaya pigment and preparation method thereof
CN109233394A (en) * 2018-09-26 2019-01-18 张惠柳 The method for preparing red drawing pigment using safflower
CN110522688A (en) * 2019-09-03 2019-12-03 上海应用技术大学 A kind of preparation and its application of alkannin powder

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