CN103445041A - Tea flavor swimming bladder collagen jelly and preparation method thereof - Google Patents
Tea flavor swimming bladder collagen jelly and preparation method thereof Download PDFInfo
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- CN103445041A CN103445041A CN2013100861400A CN201310086140A CN103445041A CN 103445041 A CN103445041 A CN 103445041A CN 2013100861400 A CN2013100861400 A CN 2013100861400A CN 201310086140 A CN201310086140 A CN 201310086140A CN 103445041 A CN103445041 A CN 103445041A
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Abstract
The invention relates to the technical field of food production, and provides a tea flavor swimming bladder collagen jelly which comprises components including tea juice collagen liquid, citric acid and white granulated sugar, wherein the specific proportion is as follows: the dosage of the citric acid is 0.04-0.08g and the dosage of the white granulated sugar is 4-12g in per 100ml of tea juice collagen liquid; the tea juice collagen liquid contains a swimming bladder collagen extracting solution, oolong tea juice and agar sol with the volume ratio of 1:(1-4):(2-5). The tea flavor swimming bladder collagen jelly is capable of effectively utilizing swimming bladder which is taken as waste during aquatic product processing, protects the environment, is capable of increasing the additional value of aquatic products, is good in taste, does not contain additives such as pigment, and is healthy and safe; nutritional ingredients are easily absorbed.
Description
Technical field
The present invention relates to the food production technology field, particularly a kind of tea flavour air bladder collagen protein jelly and preparation method thereof.
Background technology
Fish guts accounts for 10% of fish body weight, is the important sources of the large biological molecules such as protein and lipid.Air bladder belongs to one of fish guts, has another name called fish bubble, fish maw, the fish sperm, pressure born of the same parents, is the density controller official that the fish body weight is wanted, and aspect pressure-sensitive, sounding and breathing, is also having certain effect simultaneously.In China, edible air bladder has long history, the main nutrient composition of air bladder is the various trace elements such as senior collagen, mucopolysaccharide, multivitamin and calcium, zinc, iron, selenium, wherein protein content is generally more than 80%, and fat content is lower, be desirable high protein and low fat food.
Collagen is a kind of hmw protein, and thread collagen fabric can make skin keep solid and flexible.Foreign study shows, the collagen polypeptide of collagen hydrolysis gained not only has good digestion characteristics, but also has many functional activities, as antifatigue, anti-oxidant, anti-ageing waiting for a long time, at food, cosmetics biomedicine and pharmaceutical industry, is used widely.
Along with the development of China's fishery, the comprehensive utilization of aquatic products also more and more causes people's attention.Produce approximately 40% ~ 55% leftover bits and pieces of fish body gross weight man-hour adding; these discarded objects are the good raw material that prepare collagen; just comprise air bladder in these discarded objects; recycling to these discarded objects; not only protected environment also can improve the added value of aquatic products, this will provide to the development of aquatic products industry wide prospect.
Jelly is a kind of west sweet food, is semi-solid, adds water, sugar, fruit juice by edible gelatin and makes.Also claim gel, outward appearance is sparkling and crystal-clear, lovely luster, the soft cunning of mouthfeel.Jelly is the food that child likes, add a lot of fruity flavors and food colour in the raw material of a lot of jelly, such jelly nutritive value is not high, child's appetite is limited, edible too much jelly can take child's appetite, make child body lack enough nutritional supplementation spaces, be unfavorable for the child body growth; Simultaneously, eat too much or frequently eat jelly, also can make in child's body to accumulate thickener, sweetener, colouring agent and the anticorrisive agents etc. such as too much carragheen, the harm child's is healthy.The disclosure of the invention of CN 102132802 A a kind of collagen jelly and preparation method thereof, be mainly a kind of novel nourishing jelly of selecting a kind of gelatin and marine algae extract to be processed into by certain formula rate.The defect that this invention exists is: still adopting gelatin is primary raw material, and the collagen in gelatin is difficult for being absorbed, and enough nutritional supplementation can't be provided, contain pigment, potassium sorbate anticorrisive agent, health is bad, if gelatin is from marine animal, can, with fishy smell, affect the local flavor of jelly.
Summary of the invention
The object of the present invention is to provide a kind of tea flavour air bladder collagen protein jelly, can effectively utilize processing of aquatic products discarded object air bladder, not only protected environment also can improve the added value of aquatic products; nutritional labeling is easy to absorb; taste flavor is good, containing additives such as pigments, not healthy and safe.
Another object of the present invention is to provide a kind of preparation method of tea flavour air bladder collagen protein jelly.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of tea flavour air bladder collagen protein jelly, the component of described tea flavour air bladder collagen protein jelly raw material comprises tea juice collagen solution, citric acid and white granulated sugar, concrete proportioning is: every 100ml tea juice collagen solution, and the consumption of citric acid is 0.04-0.08g, the consumption of white granulated sugar is 4-12g; Described tea juice collagen solution is comprised of air bladder collagen protein extract, oolong tea juice and agar colloidal sol, and the volume ratio of air bladder collagen protein extract, oolong tea juice and agar colloidal sol is 1:1-4:2-5.
The present invention utilizes air bladder to extract the air bladder collagen protein extract of acquisition as primary raw material; can effectively utilize processing of aquatic products discarded object air bladder; not only protected environment also can improve the added value of aquatic products; simultaneously; adopt air bladder collagen protein extract and unconventional gelatin, collagen absorbs easily like this.
Oolong tea, also referred to as blue or green tea, semi-fermented tea, be one of China's six large teas, pharmacological research shows: oolong tea has hypoglycemic, reducing blood lipid, anti-inflammatory sterilization and the effect such as anti-oxidant.The main component that wherein has pharmacological action is Tea Polyphenols, theabrownin and tea polysaccharide etc.There is a defect in air bladder collagen protein extract (being collagen) from air bladder, be that it has larger fishy smell, be difficult to like this be applied to jelly production, in order to overcome this defect, the present invention adopts oolong tea juice to coordinate with air bladder collagen protein extract, oolong tea juice can effectively be removed the fishy smell of air bladder collagen protein extract, can also make jelly possess the health-care efficacy of certain oolong tea, and the while does not affect the whole mouthfeel of jelly yet.In addition, the effects such as that oolong tea has is anti-oxidant, sterilization, also can avoid the use of anticorrisive agent, extends the shelf-life of product.
Citric acid is mainly used in giving product tart flavour, regulates product special flavour, and reduces pH, bacteria growing inhibiting.
As preferably, the preparation method of described oolong tea juice is: the 2-3g oolong tea adds 100ml 95-100 ℃ hot water, soaks 3-10min, cooling rear acquisition oolong tea juice.The concentration of oolong tea juice and soak time are influential to jelly local flavor and color and luster, therefore, need better to control the preparation parameter of oolong tea juice.
As preferably, described agar colloidal sol obtains for 0.5-1.5g agar being dissolved in to heating for dissolving in 100ml water.
As preferably, the preparation method of described air bladder collagen protein extract is: under 2-4 ℃ of environmental condition, carry out, getting the 100g air bladder joins in 0.1-0.2mol/L NaOH solution and stirs 4-6h, after cleaning with distilled water, air bladder is joined in 2wt%-3 wt% NaCl solution and stirs 4-6h, with distilled water flushing to neutrality; Air bladder is added in the 0.4-0.6mol/L acetum, the acetum consumption is 1g air bladder 5-8ml acetum, homogenate, magnetic agitation 40-50h, the centrifugal 25-35min of 10000-12000r/min, obtain supernatant, in supernatant, add NaCl to the solution final concentration be 0.8-1mol/L, standing over night, centrifugal, the collecting precipitation thing, sediment is dissolved in the 0.4-0.6mol/L acetum, with 0.1-0.2mol/L acetum dialysis 20-30h, distilled water continues dialysis 40-50h, obtains air bladder collagen protein extract.
As preferably, the NaOH solution usage is 15-25ml NaOH solution for the 1g air bladder.
As preferably, the NaCl solution usage is 15-25ml NaCl solution for the 1g air bladder.
A kind of preparation method of tea flavour air bladder collagen protein jelly, agar colloidal sol is mixed with white granulated sugar, heating for dissolving, be cooled to 68-72 ℃, adds citric acid and oolong tea juice, be cooled to again 48-52 ℃ and add air bladder collagen protein extract, after mixing, filling, degassed, sterilization, after cooling finished product.
Being cooled to 68-72 ℃ and adding citric acid, avoid the harmful effect of citric acid to gel, be cooled to 48-52 ℃ and add air bladder collagen protein extract, is in order to prevent the collagen sex change.
The invention has the beneficial effects as follows:
1, adopt air bladder collagen protein extract as primary raw material, can effectively utilize processing of aquatic products discarded object air bladder, not only protected environment also can improve the added value of aquatic products, nutritional labeling is easy to absorb.
2, adopt oolong tea juice to coordinate with air bladder collagen protein extract, can effectively remove the fishy smell of air bladder collagen protein extract, can also make jelly possess the health-care efficacy of certain oolong tea, do not affect the whole mouthfeel of jelly simultaneously yet, the jelly taste flavor is good, containing additives such as pigments, not healthy and safe.
The specific embodiment
Below by specific embodiment, technical scheme of the present invention is described in further detail.
In the present invention, if not refer in particular to, the raw material adopted and equipment etc. all can be buied from market or this area is commonly used.Method in following embodiment, if no special instructions, be the conventional method of this area.
Air bladder is purchased from Zhoushan Dinghai District Nan Zhen market, Zhejiang Province; Oolong tea is commercially available; Agar, white granulated sugar, citric acid are food stage.
Embodiment 1:
(1) preparation of oolong tea juice: the 2g oolong tea adds 95 ℃ of hot water of 100ml, soaks 10min, cooling rear acquisition oolong tea juice.
(2) preparation of agar colloidal sol: 0.5g agar is dissolved in to heating for dissolving in 100ml water and obtains.
(3) preparation of air bladder collagen protein extract: carry out under 2 ℃ of environmental conditions, get 100g large yellow croaker air bladder and join (air bladder: NaOH solution=1:15 in 0.2mol/L NaOH solution, m/v) stir 4h, after cleaning with distilled water, air bladder is joined to (air bladder: NaCl solution=1:15 in 3wt% NaCl solution, m/v) stir 4h, with distilled water flushing to neutrality; Air bladder is added to (air bladder: acetum=1:5 in the 0.6mol/L acetum, m/v), homogenate, magnetic agitation 40h, the centrifugal 35min of 10000r/min, obtain supernatant, adding NaCl in supernatant is 1mol/L to the solution final concentration, standing over night, centrifugal, the collecting precipitation thing, sediment is dissolved in the 0.6mol/L acetum, with 0.2mol/L acetum dialysis 20h(volume ratio 1:15, every 4h changes extracellular fluid dialysis), distilled water continues dialysis 40h(volume ratio 1:15, and every 4h changes extracellular fluid dialysis), obtain air bladder collagen protein extract.
(4) allotment: agar colloidal sol 50ml is mixed with white granulated sugar 4g, and heating for dissolving, be cooled to 72 ℃, adds citric acid 0.04g and oolong tea juice 25ml, then be cooled to 52 ℃ and add air bladder collagen protein extract 25ml, mixes.
(5) post processing: deployed rear filling, in 85 ℃ of hot water, carry out degassed, pasteurize 10-15min, after cooling finished product.
Embodiment 2:
(1) preparation of oolong tea juice: the 3g oolong tea adds 100 ℃ of hot water of 100ml, soaks 3min, cooling rear acquisition oolong tea juice.
(2) preparation of agar colloidal sol: 1.5g agar is dissolved in to heating for dissolving in 100ml water and obtains.
(3) preparation of air bladder collagen protein extract: carry out under 4 ℃ of environmental conditions, get 100g large yellow croaker air bladder and join (air bladder: NaOH solution=1:25 in 0.1mol/L NaOH solution, m/v) stir 6h, after cleaning with distilled water, air bladder is joined to (air bladder: NaCl solution=1:25 in 2wt% NaCl solution, m/v) stir 6h, with distilled water flushing to neutrality; Air bladder is added to (air bladder: acetum=1:8 in the 0.4mol/L acetum, m/v), homogenate, magnetic agitation 50h, the centrifugal 25min of 12000r/min, obtain supernatant, adding NaCl in supernatant is 0.8mol/L to the solution final concentration, standing over night, centrifugal, the collecting precipitation thing, sediment is dissolved in the 0.4mol/L acetum, with 0.1mol/L acetum dialysis 30h(volume ratio 1:15, every 4h changes extracellular fluid dialysis), distilled water continues dialysis 50h(volume ratio 1:15, and every 4h changes extracellular fluid dialysis), obtain air bladder collagen protein extract.
(4) allotment: agar colloidal sol 50ml is mixed with white granulated sugar 12g, and heating for dissolving, be cooled to 68 ℃, adds citric acid 0.08g and oolong tea juice 40ml, then be cooled to 48 ℃ and add air bladder collagen protein extract 10ml, mixes.
(5) post processing: deployed rear filling, in 85 ℃ of hot water, carry out degassed, pasteurize 10-15min, after cooling finished product.
Embodiment 3:
(1) preparation of oolong tea juice: the 2g oolong tea adds 95 ℃ of hot water of 100ml, soaks 5min, cooling rear acquisition oolong tea juice.
(2) preparation of agar colloidal sol: 1g agar is dissolved in to heating for dissolving in 100ml water and obtains.
(3) preparation of air bladder collagen protein extract: carry out under 4 ℃ of environmental conditions, get 100g large yellow croaker air bladder and join (air bladder: NaOH solution=1:20 in 0.1mol/L NaOH solution, m/v) stir 4h, after cleaning with distilled water, air bladder is joined to (air bladder: NaCl solution=1:20 in 2.5wt%NaCl solution, m/v) stir 4h, with distilled water flushing to neutrality; Air bladder is added to (air bladder: acetum=1:6 in the 0.5mol/L acetum, m/v), homogenate, magnetic agitation 48h, the centrifugal 30min of 10000r/min, obtain supernatant, adding NaCl in supernatant is 0.9mol/L to the solution final concentration, standing over night, centrifugal, the collecting precipitation thing, sediment is dissolved in the 0.5mol/L acetum, with 0.1mol/L acetum dialysis 24h(volume ratio 1:15, every 4h changes extracellular fluid dialysis), distilled water continues dialysis 48h(volume ratio 1:15, and every 4h changes extracellular fluid dialysis), obtain air bladder collagen protein extract.
(4) allotment: agar colloidal sol 50ml is mixed with white granulated sugar 8g, and heating for dissolving, be cooled to 70 ℃, adds citric acid 0.07g and oolong tea juice 39ml, then be cooled to 50 ℃ and add air bladder collagen protein extract 11ml, mixes.
(5) post processing: deployed rear filling, in 85 ℃ of hot water, carry out degassed, pasteurize 10-15min, after cooling finished product.
Test method
1, elasticity measurement
By feel, be analyzed: the pressure that press...withes one's finger, and with the hands slowly evenly pull at and reach gel and break.
2, retentiveness is measured
Push its gel with filter cloth, by the amount of extruding water, carry out comparative analysis.
3, subjective appreciation
Take four of color and luster, local flavor, tissue morphology and mouthfeels is evaluated (judgment criteria is in Table 1) to the quality of jelly as the subjective appreciation index, full marks are 100 minutes, wherein color and luster and tissue morphology are each 20 minutes, other two each 30 minutes, be divided into three groups by 30 personnel with subjective appreciation basic quality, every group of 10 people, marked according to above index, and evaluation result is averaged.
Table 1 subjective appreciation standard
Product of the present invention is light brown yellow, translucent, has strong oolong tea perfume (or spice), sour and sweet palatability, and without fishy smell, tissue is fine and smooth, high resilience and bite, through subjective appreciation, its integrate score divides at 80-90.
4, the selection of oolong tea juice extraction time
From table 2, extraction time has considerable influence to oolong tea color and luster and mouthfeel.Oolong tea belongs to semi-fermented tea, and brewing rear tea juice is light brown yellow, and when lixiviate 5min, the color and luster of millet paste and mouthfeel all reach optimum state.
5, the agar collosol concentration is determined
The size of agar collosol concentration is influential to the gelation of jelly, and the agar colloidal sol of variable concentrations is compared to (table 3).Result shows, along with the concentration of agar increases, its hardness increases, and molding effect is also become better and better, but elasticity and transparency reduce.Relatively determine that the agar collosol and gel that concentration is 1g/100 mL is best.
6, the ratio-dependent of air bladder collagen protein extract and oolong tea juice
The ratio of air bladder collagen protein extract and oolong tea juice has considerable influence to local flavor and the color and luster of jelly, select respectively the different proportion of the two to carry out single factor experiment, thereby determine optimal proportion (table 4). test and show, when the ratio of air bladder collagen protein extract and oolong tea juice is 1:3, arranging effect is best.
7, the white granulated sugar addition determines
The white granulated sugar consumption has a direct impact the local flavor of jelly, agar colloidal sol with 50ml 2g/100mL, 50ml tea juice collagen solution (oolong tea juice 2g/100mL wherein, air bladder collagen protein extract: oolong tea juice ratio 1:3), citric acid 0.05g is basis, and the white granulated sugar that adds respectively different quality carries out single factor experiment, carries out subjective appreciation (table 5), result shows, when the white granulated sugar addition is 8g, effect is best.
8, the citric acid addition determines
Citric acid is mainly used in giving product tart flavour, regulates product special flavour, and reduces pH, bacteria growing inhibiting.The variation of PH can affect the gelation of agar, especially very large on the hardness impact.In order to avoid the harmful effect of citric acid addition to gelation as far as possible, add again citric acid in the time of the temperature of glue must being dropped to 68-72 ℃.Select the best proportioning of other factors to carry out the single factor experiment (table 6) of citric acid Different adding amount.When the citric acid addition is 0.06g, effect is best.
Draw technical scheme of the present invention through these experiments, then passed through orthogonal experiment, obtained best-of-breed technology scheme of the present invention: every 100ml tea juice collagen solution, the consumption of citric acid is 0.07g, the consumption of white granulated sugar is 8g; Tea juice collagen solution forms: air bladder collagen protein extract 11ml, oolong tea juice 39ml and agar colloidal sol 50ml.
Above-described embodiment is a kind of preferably scheme of the present invention, not the present invention is done to any pro forma restriction, also has other variant and remodeling under the prerequisite that does not exceed the technical scheme that claim puts down in writing.
Claims (7)
1. a tea flavour air bladder collagen protein jelly, it is characterized in that: the component of described tea flavour air bladder collagen protein jelly raw material comprises tea juice collagen solution, citric acid and white granulated sugar, concrete proportioning is: every 100ml tea juice collagen solution, the consumption of citric acid is 0.04-0.08g, and the consumption of white granulated sugar is 4-12g; Described tea juice collagen solution is comprised of air bladder collagen protein extract, oolong tea juice and agar colloidal sol, and the volume ratio of air bladder collagen protein extract, oolong tea juice and agar colloidal sol is 1:1-4:2-5.
2. a kind of tea flavour air bladder collagen protein jelly according to claim 1, it is characterized in that: the preparation method of described oolong tea juice is: the 2-3g oolong tea adds 100ml 95-100 ℃ hot water, soaks 3-10min, cooling rear acquisition oolong tea juice.
3. a kind of tea flavour air bladder collagen protein jelly according to claim 1, it is characterized in that: described agar colloidal sol obtains for 0.5-1.5g agar being dissolved in to heating for dissolving in 100ml water.
4. according to claim 1 or 2 or 3 described a kind of tea flavour air bladder collagen protein jellies, it is characterized in that: the preparation method of described air bladder collagen protein extract is: under 2-4 ℃ of environmental condition, carry out, getting the 100g air bladder joins in 0.1-0.2mol/L NaOH solution and stirs 4-6h, after cleaning with distilled water, air bladder is joined in 2wt%-3 wt% NaCl solution and stirs 4-6h, with distilled water flushing to neutrality; Air bladder is added in the 0.4-0.6mol/L acetum, the acetum consumption is 1g air bladder 5-8ml acetum, homogenate, magnetic agitation 40-50h, the centrifugal 25-35min of 10000-12000r/min, obtain supernatant, in supernatant, add NaCl to the solution final concentration be 0.8-1mol/L, standing over night, centrifugal, the collecting precipitation thing, sediment is dissolved in the 0.4-0.6mol/L acetum, with 0.1-0.2mol/L acetum dialysis 20-30h, distilled water continues dialysis 40-50h, obtains air bladder collagen protein extract.
5. a kind of tea flavour air bladder collagen protein jelly according to claim 4 is characterized in that: the NaOH solution usage is 15-25ml NaOH solution for the 1g air bladder.
6. a kind of tea flavour air bladder collagen protein jelly according to claim 4 is characterized in that: the NaCl solution usage is 15-25ml NaCl solution for the 1g air bladder.
7. the preparation method of a kind of tea flavour air bladder collagen protein jelly as claimed in claim 1, it is characterized in that: agar colloidal sol is mixed with white granulated sugar, heating for dissolving, be cooled to 68-72 ℃, adds citric acid and oolong tea juice, be cooled to again 48-52 ℃ and add air bladder collagen protein extract, after mixing, filling, degassed, sterilization, after cooling finished product.
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Cited By (7)
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| CN104171776A (en) * | 2014-07-16 | 2014-12-03 | 胡美君 | Health jelly containing mantis shrimp heads and mantis shrimp shells and preparation method thereof |
| CN105558965A (en) * | 2015-12-18 | 2016-05-11 | 林秋健 | Oolong jellies and preparation method thereof |
| CN107242474A (en) * | 2017-06-09 | 2017-10-13 | 大连工业大学 | The preparation method of globe fish fish-skin nutrition pudding |
| CN110613070A (en) * | 2019-10-18 | 2019-12-27 | 汕尾市维明生物科技股份有限公司 | Collagen beverage and preparation method thereof |
| CN110692982A (en) * | 2019-10-17 | 2020-01-17 | 深圳市海能达实业有限公司 | Production process method of gel jelly and black tea collagen jelly |
| CN112826059A (en) * | 2021-01-22 | 2021-05-25 | 中南林业科技大学 | Camellia extract-collagen health jelly and preparation method thereof |
| CN114041584A (en) * | 2022-01-04 | 2022-02-15 | 中国海洋大学 | Preparation method of fish skin collagen peptide jelly capable of being stored and transported at normal temperature |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104171776A (en) * | 2014-07-16 | 2014-12-03 | 胡美君 | Health jelly containing mantis shrimp heads and mantis shrimp shells and preparation method thereof |
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| CN110692982A (en) * | 2019-10-17 | 2020-01-17 | 深圳市海能达实业有限公司 | Production process method of gel jelly and black tea collagen jelly |
| CN110613070A (en) * | 2019-10-18 | 2019-12-27 | 汕尾市维明生物科技股份有限公司 | Collagen beverage and preparation method thereof |
| CN112826059A (en) * | 2021-01-22 | 2021-05-25 | 中南林业科技大学 | Camellia extract-collagen health jelly and preparation method thereof |
| CN114041584A (en) * | 2022-01-04 | 2022-02-15 | 中国海洋大学 | Preparation method of fish skin collagen peptide jelly capable of being stored and transported at normal temperature |
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| CN103445041B (en) | 2014-11-05 |
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