CN103432008A - Formed konjak mask and preparation method thereof - Google Patents
Formed konjak mask and preparation method thereof Download PDFInfo
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- CN103432008A CN103432008A CN201310386890XA CN201310386890A CN103432008A CN 103432008 A CN103432008 A CN 103432008A CN 201310386890X A CN201310386890X A CN 201310386890XA CN 201310386890 A CN201310386890 A CN 201310386890A CN 103432008 A CN103432008 A CN 103432008A
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Abstract
The invention discloses a formed konjak mask and a preparation method thereof. The mask is prepared by utilizing konjak powder as a raw material, purifying, preparing glue, and then mixing the glue with carboxymethyl cellulose and xanthan gum, adding glycerin and sodium carbonate to prepare an emulsion, curing and forming, dealkalizing and sterilizing, and finally immersing into a skin moisturizer. The formed konjak mask prepared by the preparation method disclosed by the invention is strong in toughness, good in ductility, good in adhesion and hydrophilia and capable of being closely combined with skin to provide sufficient moisture for the skin and prevent the moisture in the stratum corneum of skin from evaporating so as to enable the additional nutritional skin moisturizer to be easily absorbed, maintain the face moistness and avoid the accelerated aging the face skin; in addition, the konjak powder is a pure plant source substance, thereby being free of stimulation, safe and free of toxic or side effect to the skin. The formed konjak mask is little in pollution in the production process and liable to degrade, thereby being environmentally-friendly.
Description
Technical field
The present invention relates to a kind of cosmetic skincare product, be specially a kind of molding konjac facial mask and preparation method thereof.
Background technology
Along with scientific and technological development and growth in the living standard, people progressively increase the demand of cosmetics, and the quality of cosmetics and the requirement of safety are also improved thereupon.In recent years, the application of facial film increased gradually, and the molding facial film occupies very large market.But a lot of molding facial films are to using non-woven fabrics as carrier, and ductility is poor, can not be well and face fit, and, in the preparation process of facial film, have the safety and sanitation problem.Therefore, the research of relevant facial film is also to All Pure Nature, safety, nuisanceless type, high-quality future development.
Rhizoma amorphophalli You Cheng Rhizoma amorphophalli, latin name Amorphophalus, belong to Araeceae Amorphophallus herbaceos perennial.The main component of Rhizoma amorphophalli is glucomannan, is a kind of nonionic polysaccharide of high molecular.It is the chain molecule combined by β-Isosorbide-5-Nitrae glycosidic bond and β-1,3 glycosidic bond.Konjak glucomannan, as a kind of natural polymer substance, has extraordinary film property, and formed film toughness is strong, ductility good, particularly has good adhesiveness, can with the close combination of skin, reach the cleaning effect of expection.Glucomannan is a kind of pure plant source active substance, non-stimulated to skin, has no side effect, and at occurring in nature, easily degrades, and is one of preferably environmentally friendly natural biologic material of manufacturing by facial film.
Summary of the invention
Technical problem to be solved by this invention has been to provide a kind of molding konjac facial mask and preparation method thereof, adopt pure plant source material purification Rhizoma amorphophalli powder to prepare good, safe, the nuisanceless molding facial film of a kind of performance as main component, also solved the chemical fibre facial film simultaneously and be difficult for the problem of decomposing for environment.
Technical scheme of the present invention is achieved in that a kind of molding konjac facial mask, it is to take konjaku powder as raw material, purified glue, then with carboxymethyl cellulose and xanthan gum batch mixing, add glycerol, sodium carbonate to make emulsion, recurring molding, dealkalize, sterilizing, finally immerse that skin care liquid obtains.
Described skin care liquid consists of: propylene glycol 2.0 ~ 4.0%, and hyaluronic acid 0.2% ~ 0.5%, hydrolyzed soybean protein 1.0 ~ 5.0%, antiseptic 0.05% ~ 0.5%, essence 0.2 ~ 1.0%, surplus is deionized water.
Prepare the method for above-mentioned molding konjac facial mask, specifically comprise the following steps:
1) purification: adopt alcoholic solution to carry out repeatedly submergence washing konjaku powder, and then grind with colloid mill, centrifugal filtration, filtering residue dry glucomannan at the Konjac glucomannan more than 90%;
2) batch mixing: by weight, get the step 1) gained 60 ~ 80 parts of Konjac glucomannan, with 10 ~ 40 parts of carboxymethyl celluloses, 5 ~ 10 parts of xanthan gum, mix homogeneously;
3) batch mixing 2.5-5 part emulsion preparation: by weight, get step 2), glycerol 0.05-0.5 part, sodium carbonate 0.1-0.3 part, add 75-100 part water emulsion that stirs to obtain;
4) facial mask shaping: emulsion is poured in the facial film mould, first standing 10 ~ 16 hours, then in steamer, steam ripening molding in 35 ~ 60 minutes, more freezing 3 ~ 5 days in-20 ℃ ~-30 ℃;
5) demoulding dealkalize: by the demoulding of thawing of the product of step 4), and washed, until the pH value of water is 6.0-8.0, spin-dry;
6) sterilizing: the facial film after drying is soaked in Ozone Water and carries out sterilization treatment, ozone concentration 0.5 ~ 1.5ppm, sterilization time 10 ~ 40 minutes;
7), immerse skin care liquid: the film after sterilizing is soaked in skin care liquid and soaks 0.5 ~ 1 hour, obtain the molding konjac facial mask.
In described purification step, adopt the alcoholic solution of 30 ~ 50wt% to be washed, wash altogether 3 times.
In described step 4), the temperature of steamer is 100 ~ 108 ℃.
The present invention adopts repeatedly cyclic washing konjaku powder of ethanol, and the impurity such as the starch in the removal konjaku powder, alkaloid, make glucomannan content more than 90%.
Novelty of the present invention by purification Rhizoma amorphophalli powder and carboxymethyl cellulose, xanthan gum, undertaken composite, adding of carboxymethyl cellulose will be carried out crosslinked with the purification Rhizoma amorphophalli powder under hot conditions, the network structure densification, therefore formed film mechanical performance is significantly improved, hot strength increases, make product be difficult for fracture, and concerted reaction can occur in xanthan gum and Rhizoma amorphophalli powder at normal temperatures, form jelly, make product molding preferably, while pouring emulsion into the facial film mould, not there will be hangover wire drawing situation, thereby avoid burr occurring on the facial film limit.When prepared at emulsion by this facial film, adding glycerol, is mainly to prevent from forming large ice crystal in refrigerating process, makes its sponge structure evenly fine and smooth, can alleviate the harsh feeling of simple Rhizoma amorphophalli product formation, improves the flexibility of product.
The present invention is when film carries out sterilization treatment over there, adopt the soak with ozone solution sterilizing, it is good that it compares traditional sterilizing methods sterilization effect, can not bring destruction to product as high temperature sterilize, irradiation sterilization brings residual, have extremely strong oxidisability, can effectively kill the antibacterial of facial film etc., ozone can resolve into oxygen at short notice fully, and can not produce secondary pollution, noresidue, on product without impact, safety.
Molding konjac facial mask prepared by the present invention, toughness is strong, ductility good, there is good adhesiveness and hydrophilic, can with the close combination of skin, for skin provides sufficient moisture and prevents that the moisture evaporation in keratodermatitis from reducing, make additional nutrition skin-protection liquid composition be easy to absorb, keep face to moisten, avoid the skin of face accelerated ageing; In addition, its konjaku powder is the pure plant source material, non-stimulated to skin, safely, have no side effect.Production process is polluted less, easily degraded, is environmentally friendly facial film.
The specific embodiment
further illustrate the present invention below in conjunction with embodiment, but the scope of protection of present invention is not limited to the scope of embodiment statement.
Embodiment 1:
A kind of preparation method of molding konjac facial mask specifically comprises the following steps:
1) purification: adopt the alcoholic solution of 30wt% to carry out the submergence washing konjaku powder, wash altogether 3 times, and then grind with colloid mill, centrifugal filtration, dry to obtain Konjac glucomannan;
2) batch mixing: get the step 1) gained 60 parts of Konjac glucomannan, with 30 parts of carboxymethyl celluloses, 10 parts of xanthan gum, mix homogeneously;
3) 2.5 parts of batch mixings emulsion preparation: get step 2), 0.05 part of glycerol, 0.25 part of sodium carbonate, 75 parts of emulsion that stir to obtain of water;
4) facial mask shaping: emulsion is poured in the facial film mould, first standing 10 hours, then in the steamer of 100 ℃, steam ripening molding in 60 minutes, more freezing 3 days in-20 ℃ ~-30 ℃;
5) demoulding dealkalize: by the demoulding of thawing of the product of step 4), and washed, until pH value is between 6.0-8.0, spin-dry;
6) sterilizing: the facial film after drying is soaked in Ozone Water and carries out sterilization treatment, ozone concentration 1ppm, sterilization time 30 minutes;
7), immerse skin care liquid: the film after sterilizing is soaked in skin care liquid and soaks 0.5 hour, obtain the molding konjac facial mask.
Above-mentioned skin care liquid consists of: propylene glycol 2.0%, and hyaluronic acid 0.2%, hydrolyzed soybean protein 5.0%, antiseptic 0.5%, essence 0.2, surplus is deionized water.This skin care liquid formula is only cited for improving the present invention, also can adopt the skin care liquid of other formula in production application.
Embodiment 2:
A kind of preparation method of molding konjac facial mask specifically comprises the following steps:
1) purification: adopt the alcoholic solution of 40wt% to carry out the submergence washing konjaku powder, wash altogether 3 times, and then grind with colloid mill, centrifugal filtration, dry to obtain Konjac glucomannan;
2) batch mixing: get the step 1) gained 80 parts of Konjac glucomannan, with 15 parts of carboxymethyl celluloses, 5 parts of xanthan gum, mix homogeneously;
3) 5 parts of batch mixings emulsion preparation: get step 2), 5 parts of glycerol, 0.1 part of sodium carbonate, 100 parts of emulsion that stir to obtain of water;
4) facial mask shaping: emulsion is poured in the facial film mould, first standing 16 hours, then in the steamer of 108 ℃, steam ripening molding in 35 minutes, more freezing 4 days in-20 ℃ ~-30 ℃;
5) demoulding dealkalize: by the demoulding of thawing of the product of step 4), and washed, until pH value is between 6.0-8.0, spin-dry;
6) sterilizing: the facial film after drying is soaked in Ozone Water and carries out sterilization treatment, ozone concentration 1.5ppm, sterilization time 10 minutes;
7), immerse skin care liquid: the film after sterilizing is soaked in skin care liquid and soaks 1 hour, obtain the molding konjac facial mask.
Above-mentioned skin care liquid consists of: propylene glycol 4.0%, and hyaluronic acid 0.5%, hydrolyzed soybean protein 1.0, antiseptic 0.05%, essence 1.0%, surplus is deionized water.This skin care liquid formula is only cited for improving the present invention, also can adopt the skin care liquid of other formula in production application.
Embodiment 3:
A kind of preparation method of molding konjac facial mask specifically comprises the following steps:
1) purification: adopt the alcoholic solution of 50wt% to carry out the submergence washing konjaku powder, wash altogether 3 times, and then grind with colloid mill, centrifugal filtration, dry to obtain Konjac glucomannan;
2) batch mixing: get the step 1) gained 70 parts of Konjac glucomannan, with 20 parts of carboxymethyl celluloses, 10 parts of xanthan gum, mix homogeneously;
3) 5 parts of batch mixings emulsion preparation: get step 2), 0.25 part of glycerol, 0.3 part of sodium carbonate, 85 parts of emulsion that stir to obtain of water;
4) facial mask shaping: emulsion is poured in the facial film mould, first standing 13 hours, then in the steamer of 105 ℃, steam ripening molding in 50 minutes, more freezing 5 days in-20 ℃ ~-30 ℃;
5) demoulding dealkalize: by the demoulding of thawing of the product of step 4), and washed, until pH value is between 6.0-8.0, spin-dry;
6) sterilizing: the facial film after drying is soaked in Ozone Water and carries out sterilization treatment, ozone concentration 0.5ppm, sterilization time 40 minutes;
7), immerse skin care liquid: the film after sterilizing is soaked in skin care liquid and soaks 0.8 hour, obtain the molding konjac facial mask.
Above-mentioned skin care liquid consists of: propylene glycol 3.0%, and hyaluronic acid 0.3%, hydrolyzed soybean protein 3%, antiseptic 0.25%, essence 0.5%, surplus is deionized water.This skin care liquid formula is only cited for improving explanation the present invention, also can adopt the skin care liquid of other formula in production application, as have the skin care liquid of white-skinned face function or moisturizing effect.
Claims (5)
1. a molding konjac facial mask, it is characterized in that: it is to take konjaku powder as raw material, purified glue, then with carboxymethyl cellulose and xanthan gum batch mixing, add glycerol, sodium carbonate to make emulsion, recurring molding, dealkalize, sterilizing, finally immerse that skin care liquid obtains.
2. molding konjac facial mask according to claim 1, it is characterized in that: described skin care liquid consists of: propylene glycol 2.0 ~ 4.0%, hyaluronic acid 0.2% ~ 0.5%, hydrolyzed soybean protein 1.0 ~ 5.0%, antiseptic 0.05% ~ 0.5%, essence 0.2 ~ 1.0%, surplus is deionized water.
3. prepare the method for the described molding konjac facial mask of claim 1 or 2, it is characterized in that, specifically comprise the following steps:
1) purification: adopt alcoholic solution to carry out repeatedly submergence washing konjaku powder, and then grind with colloid mill, centrifugal filtration, filtering residue dry glucomannan at the Konjac glucomannan more than 90%;
2) batch mixing: by weight, get the step 1) gained 60 ~ 80 parts of Konjac glucomannan, with 10 ~ 40 parts of carboxymethyl celluloses, 5 ~ 10 parts of xanthan gum, mix homogeneously;
3) batch mixing 2.5-5 part emulsion preparation: by weight, get step 2), glycerol 0.05-0.5 part, sodium carbonate 0.1-0.3 part, add 75-100 part water emulsion that stirs to obtain;
4) facial mask shaping: emulsion is poured in the facial film mould, first standing 10 ~ 16 hours, then in steamer, steam ripening molding in 35 ~ 60 minutes, more freezing 3 ~ 5 days in-20 ℃ ~-30 ℃;
5) demoulding dealkalize: by the demoulding of thawing of the product of step 4), and washed, until the pH value of water is 6.0-8.0, spin-dry;
6) sterilizing: the facial film after drying is soaked in Ozone Water and carries out sterilization treatment, ozone concentration 0.5 ~ 1.5ppm, sterilization time 10 ~ 40 minutes;
7), immerse skin care liquid: the film after sterilizing is soaked in skin care liquid and soaks 0.5 ~ 1 hour, obtain the molding konjac facial mask.
4. the preparation method of molding konjac facial mask according to claim 3, is characterized in that: in described purification step, adopt the alcoholic solution of 30 ~ 50wt% to be washed, wash altogether 3 times.
5. the preparation method of molding konjac facial mask according to claim 3, it is characterized in that: in described step 4), the temperature of steamer is 100 ~ 108 ℃.
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Cited By (10)
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| CN104523443A (en) * | 2014-12-17 | 2015-04-22 | 湖北一致魔芋生物科技有限公司 | Preparation method of lycopene and konjak cleansing cotton |
| CN104546540A (en) * | 2015-01-12 | 2015-04-29 | 武汉芘芘薇莎生物科技有限公司 | Preparation method of compound polysaccharide biological masks |
| CN105054565A (en) * | 2015-07-03 | 2015-11-18 | 福建农林大学 | Konjac glucomannan double eyelid sticker and preparation method thereof |
| CN105213248A (en) * | 2015-08-07 | 2016-01-06 | 袁朝宁 | A kind of ecosystem fruit-vegetable facial mask pastes |
| CN107184456A (en) * | 2017-05-22 | 2017-09-22 | 福建农林大学 | A kind of konjaku glucomannan eye mask and preparation method thereof |
| CN110151579A (en) * | 2019-06-12 | 2019-08-23 | 陈敏 | A kind of application of plant component in terms of the cosmetics that preparation promotes skin repair, anti-aging |
| CN110200885A (en) * | 2019-06-26 | 2019-09-06 | 武汉芘芘薇莎生物科技有限公司 | A kind of konjac facial mask base fabric and preparation method thereof and konjac facial mask |
| CN110693727A (en) * | 2019-10-15 | 2020-01-17 | 武汉芘芘薇莎生物科技有限公司 | Preparation method of konjak hydrogel eye mask |
| CN111686058A (en) * | 2020-07-13 | 2020-09-22 | 富源县金地魔芋种业有限公司 | Formed konjak mask and preparation method thereof |
| CN112391837A (en) * | 2020-11-30 | 2021-02-23 | 湖北一致魔芋生物科技股份有限公司 | Konjak mask base cloth preparation method and konjak mask |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104523443A (en) * | 2014-12-17 | 2015-04-22 | 湖北一致魔芋生物科技有限公司 | Preparation method of lycopene and konjak cleansing cotton |
| CN104523443B (en) * | 2014-12-17 | 2017-06-23 | 湖北一致魔芋生物科技有限公司 | A kind of preparation method of lycopene konjaku clean skin cotton |
| CN104546540A (en) * | 2015-01-12 | 2015-04-29 | 武汉芘芘薇莎生物科技有限公司 | Preparation method of compound polysaccharide biological masks |
| CN105054565A (en) * | 2015-07-03 | 2015-11-18 | 福建农林大学 | Konjac glucomannan double eyelid sticker and preparation method thereof |
| CN105213248A (en) * | 2015-08-07 | 2016-01-06 | 袁朝宁 | A kind of ecosystem fruit-vegetable facial mask pastes |
| CN107184456A (en) * | 2017-05-22 | 2017-09-22 | 福建农林大学 | A kind of konjaku glucomannan eye mask and preparation method thereof |
| CN110151579A (en) * | 2019-06-12 | 2019-08-23 | 陈敏 | A kind of application of plant component in terms of the cosmetics that preparation promotes skin repair, anti-aging |
| CN110200885A (en) * | 2019-06-26 | 2019-09-06 | 武汉芘芘薇莎生物科技有限公司 | A kind of konjac facial mask base fabric and preparation method thereof and konjac facial mask |
| WO2020258740A1 (en) * | 2019-06-26 | 2020-12-30 | 武汉芘芘薇莎生物科技有限公司 | Konjac face mask base cloth and preparation method therefor, and konjac face mask |
| CN110693727A (en) * | 2019-10-15 | 2020-01-17 | 武汉芘芘薇莎生物科技有限公司 | Preparation method of konjak hydrogel eye mask |
| CN111686058A (en) * | 2020-07-13 | 2020-09-22 | 富源县金地魔芋种业有限公司 | Formed konjak mask and preparation method thereof |
| CN112391837A (en) * | 2020-11-30 | 2021-02-23 | 湖北一致魔芋生物科技股份有限公司 | Konjak mask base cloth preparation method and konjak mask |
| CN112391837B (en) * | 2020-11-30 | 2022-11-15 | 湖北一致魔芋生物科技股份有限公司 | Konjak mask base cloth preparation method and konjak mask |
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Address after: 443500, No. 438, Changyang Avenue, Yichang Economic Development Zone, Changyang Tujia Autonomous County, Hubei, China Patentee after: Hubei Polytron Technologies Inc Address before: 443500 No. 438 Changyang Road, economic development zone, Changyang Tujia Autonomous County, Hubei Province Patentee before: Hubei Yizhi Konjac Biotechnology Co., Ltd. |