CN103431111A - Preparation method for honeysuckle throat smoothing tea - Google Patents

Preparation method for honeysuckle throat smoothing tea Download PDF

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CN103431111A
CN103431111A CN2013103479691A CN201310347969A CN103431111A CN 103431111 A CN103431111 A CN 103431111A CN 2013103479691 A CN2013103479691 A CN 2013103479691A CN 201310347969 A CN201310347969 A CN 201310347969A CN 103431111 A CN103431111 A CN 103431111A
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preparation
tea
filtrate
honeysuckle
powder
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CN2013103479691A
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CN103431111B (en
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李翔宇
刘爱武
尹洁
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李翔宇
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Abstract

The invention discloses a preparation method for honeysuckle throat smoothing tea. The preparation method comprises the following four steps of extract extraction, concentrated solution preparation, powder preparation and mixing. The invention further discloses throat smoothing tea prepared by adopting the method. According to the invention, different processing manners are adopted for different raw materials according to the technology, the effective constituents in raw materials are released furthest, and the nutritional ingredient waste caused by an adopted single processing manner is avoided.

Description

A kind of preparation method of honeysuckle throat-moistening tea
Technical field
The invention belongs to the medicines and health protection technical field, relate to a kind of preparation method of honeysuckle throat-moistening tea.
Background technology
Pharyngitis is pharyngeal mucosa, and the inflammation of submucous tissue is often the part of the infection of the upper respiratory tract.According to the length of the course of disease and the difference of pathological change character, be divided into acpuei pharyngitis, the large class of chronic pharyngitis two.In daily life, chronic pharyngitis is because morbidity is uncertain and the cycle is long, as easy as rolling off a logly by people, ignored.Chronic pharyngitis (Chronic pharyngitis) is mainly pharynx mucous membrane chronic inflammation, and diffuse inflammation is often the part of chronic other property inflammation of the upper respiratory tract, and the limitation inflammation is many inflammation with the pharynx GALT.Chronic pharyngitis is a kind of common disease, frequently-occurring disease clinically, in conventional drug therapy, more obstinate, and outbreak repeatedly, and flu increases the weight of, common with a middle-aged person.Main manifestations is pharyngeal mucous membrane chronic congestion, and foreign body sensation is arranged.Pathology mainly concentrates on pharyngeal mucous layer, around its blood vessel, has more lymphoid tissue to infiltrate, also visible leucocyte and plasmocyte infiltrating.Connective tissue proliferation under mucous membrane and mucous membrane, can be with the mucous gland hypertrophy, glandular secretion hyperfunction, mucus secretion increasing and than thickness.Chronic pharyngitis is more common in the adult, and children also can occur.Constitutional symptom is all not obvious, take local symptom as main.Various chronic pharyngitis symptom is roughly similar and varied, as pharyngeal sense of discomfort, foreign body sensation, pharyngeal secretion are difficult for expectoration, pharyngeal gargalesthesia, burn feeling, dry sensation or excitement, also the hypodynia sense can be arranged.Because the pharynx rear wall adheres to because pharyngeal chronic inflammation causes than thick secretions usually, and, because nose, nasal sinus, nasopharynx pathological changes cause the mouth breathing at night, occur irritable cough the morning of being everlasting while rising and feel sick.Because can showing as frequently, the foreign body in pharynx sense swallows.Pharyngeal secretion is few and be difficult for expectoration person and often show as habitually dry cough and the action of coughing up phlegm of clearing one's throat, if firmly cough or clear one's throat, can cause pharyngeal mucosa hemorrhage, causes in secretion and is with blood.
At present, the method for the treatment of chronic pharyngitis has a lot.Doctor trained in Western medicine is dispelled the cause of disease to adopt of the treatment of chronic pharyngitis more, gives up tobacco and wine, avoids dust and pernicious gas etc., and the main idodine of using for oral administration, can promote secretion to increase, and improves dry symptom.Take vitamin A, B2, C, the medicines such as E, can promote the mucosal epithelium growth.Use in case of necessity the external therapys such as laser, radio frequency, by the transfer factor branch, be injected in pharyngeal treatment chronic pharyngitis.Transfer factor is as a kind of immunopotentiator, and the one, improve and eliminate local scorching card, the 2nd, regulate and strengthen the immunologic function of body.The uncertain therapeutic efficacy of Western medicine is cut, although use inustion, to foreign body in pharynx, sense makes moderate progress, and because of reasons such as the glandular secretion that destroyed mucous membrane and scar contractures, tends to bring dry throat, and pharyngalgia increases the weight of, and the Chinese traditional treatment chronic pharyngitis has its unique curative effect than doctor trained in Western medicine.The inventor has succeeded in developing a kind of honeysuckle throat-moistening tea (China Patent No. 2010102397703) in 2010, this tea has been obtained certain effect, but also there is more defect, for example, adopt simple raw material to mix, according to the difference of raw material, do not adopt different technologies, active ingredient in raw material does not discharge fully, the waste of the nutritional labeling that causes, and tealeaves is not easy to carry, and very easily becomes tide summer.
Summary of the invention
The preparation method who the purpose of this invention is to provide a kind of honeysuckle throat-moistening tea, its technique uniqueness, utilized raw material to greatest extent, and preparation method's simple possible, overcome the defect of the wastage of material of prior art existence.
In order to reach technical purpose of the present invention, the present invention is achieved by the following technical solution,
A kind of preparation method of honeysuckle throat-moistening tea, is characterized in that, described method comprises the steps:
1) take honeysuckle 1000g and the tuber of dwarf lilyturf 500g, mix, the decocting that adds 2 times of weight boils 2 hours, filter to collect filtrate, with the PH of the hydrochloric acid solution adjustment filtrate of 1mol/L, is 6, then filtrate is condensed into to the medicinal extract that density is 1.1g/ml;
2) get hawthorn 900g and mulberry leaf 100g and put in pulverizer and pulverize, take out and be laid into 1 square metre, ultraviolet ray is lower irradiates 5 minutes, and uitraviolet intensity is 1500uW/cm 2; Then use the deionized water of 2L as solvent, maintain under 0.2 atmospheric pressure state, 60 ℃ are hydrolyzed 1 day, filter and collect filtrate; Filtrate is placed in vacuum decker, is concentrated in vacuo to 1/5th of filtrate volume, obtain concentrate;
3) selecting fresh radix bardanae 800g, dries in the shade in the drying place that puts into cool place, ventilation, then is cut into the square fragment of 5-10mm, and the ethanol that to put into volume fraction be 70% soaks 30 minutes, and the decompression rotary evaporation is removed ethanol; Be placed in the lower irradiation of ultraviolet ray 10 minutes, uitraviolet intensity is 3000uW/cm 2, it is the above powder of 100 orders that the final powder breakdown mill becomes particle diameter;
4) by step 1) medicinal extract, the step 2 that prepare) concentrate and the step 3 that prepare) powder for preparing mixes, and obtains active ingredient, then with fructose, mixes, stirs, and then is prepared into the particle that particle diameter is less than 10 microns, the paper bag and get final product of sterilizing of packing into; The mass ratio of above-mentioned active ingredient and fructose is 5: 1; Every bag containing 1g.
The warm water of edible immersion way: 70-80 ℃ soaks, and the time is 5 minutes; Suggestion is soaked according to the ratio of the corresponding 500g water of 1g tea.
The invention also discloses honeysuckle throat-moistening tea prepared by said method and uses thereof.
The beneficial effect that the present invention obtains, mainly contain following some:
The present invention adopts unique technology, and the active ingredient in raw material is discharged to greatest extent;
The raw material that the present invention is different adopts different processing modes, the nutritional labeling waste of having avoided single processing mode to cause;
The present invention selects the UV treatment of suitable time and amount of radiation, makes the cell membrane of hawthorn and radix bardanae thoroughly be destroyed, the discharging to greatest extent of sterol flavone compound;
The present invention adopts the different solvents extraction to hawthorn or radix bardanae, has avoided unnecessary wastage of material;
Tea prepared by the present invention, more easily carry than traditional tealeaves, and can directly drink, without outwelling tealeaves;
Extraction step of the present invention is simple to operate, is applicable to suitability for industrialized production, possesses wide application prospect;
The selected selection of the present invention four flavor Chinese herbal medicines, reasonable compatibility, not only possess health care, and also possessing wets one's whistle promotes the production of body fluid, clearing heat and detoxicating function.
The specific embodiment
Below will adopt specific embodiment to make further explanation to the present invention, but it is not as the restriction to initiative spirit of the present invention.
Embodiment 1
A kind of preparation method of honeysuckle throat-moistening tea, comprise the steps:
1) take honeysuckle 1000g and the tuber of dwarf lilyturf 500g, mix, the decocting that adds 2 times of weight boils 2 hours, filter to collect filtrate, with the PH of the hydrochloric acid solution adjustment filtrate of 1mol/L, is 6, then filtrate is condensed into to the medicinal extract that density is 1.1g/ml;
2) get hawthorn 900g and mulberry leaf 100g and put in pulverizer and pulverize, take out and be laid into 1 square metre, ultraviolet ray is lower irradiates 5 minutes, and uitraviolet intensity is 1500uW/cm 2; Then use the deionized water of 2L as solvent, maintain under 0.2 atmospheric pressure state, 60 ℃ are hydrolyzed 1 day, filter and collect filtrate; Filtrate is placed in vacuum decker, is concentrated in vacuo to 1/5th of filtrate volume, obtain concentrate;
3) selecting fresh radix bardanae 800g, dries in the shade in the drying place that puts into cool place, ventilation, then is cut into the square fragment of 5-10mm, and the ethanol that to put into volume fraction be 70% soaks 30 minutes, and the decompression rotary evaporation is removed ethanol; Be placed in the lower irradiation of ultraviolet ray 10 minutes, uitraviolet intensity is 3000uW/cm 2, it is the above powder of 100 orders that the final powder breakdown mill becomes particle diameter;
4) by step 1) medicinal extract, the step 2 that prepare) concentrate and the step 3 that prepare) powder for preparing mixes, and obtains active ingredient, then with fructose, mixes, stirs, and then is prepared into the particle that particle diameter is less than 10 microns, the paper bag and get final product of sterilizing of packing into; The mass ratio of above-mentioned active ingredient and fructose is 5: 1; Every bag containing 1g.
The warm water of edible immersion way: 70-80 ℃ soaks, and the time is 5 minutes; Suggestion is soaked according to the ratio of the corresponding 500g water of 1g tea.
Embodiment 2
The clinical effectiveness of the tea for moistening of embodiment 1 preparation:
Adopting inventor's formula (referring to CN2010102397703) before this in contrast, select two control groups, is respectively control group 1: gram, balloonflower root 20 grams directly were mixed, packed, every bag 5g honeysuckle 50 grams, the tubers of dwarf lilyturf 30; Control group 2: honeysuckle 40 grams, the tubers of dwarf lilyturf 40 gram, balloonflower root 20 grams, hawthorn 20 grams, above-mentioned raw materials first is processed into respectively to coarse granule, then is mixed, packs, every bag 5g; The tea for moistening of experimental group: embodiment 1 preparation.
Drinking way:
Control group 1 and 2 is: the hot-water soak of 90 ℃, and the time is 5 minutes; Ratio according to the corresponding 500g water of 5g tea is soaked; Drink 1500g tea every day, minute morning, noon and afternoon drink for three times.
Experimental group is: the warm water of 70-80 ℃ soaks, and the time is 5 minutes; Ratio according to the corresponding 500g water of 1g tea is soaked; Drink 1500g tea every day, minute morning, noon and afternoon drink for three times.
One, drink the mouthfeel investigation
Drink the crowd: the general population; Drink the time: one week; Drink number: every group of 30 people;
Index: drink rear fresh and sweet sweet being designated as that have back of obviously feeling; Drink being designated as of the fresh and sweet micro-hardship of after sensation general; Drink after sensation heavy bitter taste mouthfeel poor be designated as poor.Specifically in Table 1.
Group " good " number " generally " number " poor " number
Control group 1 2 13 15
Control group 2 4 12 14
Experimental group 18 11 1
Two, to the result for the treatment of of chronic pharyngitis:
Patient's data: the patient is totally 60 examples, male 34 examples wherein, and female's 26 examples, age 20-60 is between year, average course of disease 1.5 years; Be equally divided at random three groups, i.e. experimental group (drinking tea product prepared by above-mentioned experimental group), control group 1 (drinking the tea product of above-mentioned control group 1 preparation), control group 2 (drinking the tea product of above-mentioned control group 2 preparations).Every group of 20 people.Diagnostic criteria: diagnostic criteria is planned the diagnostic criteria of teaching material, national medical school teaching material " otorhinolaryngology " third edition chronic pharyngitis with reference to the Ministry of Public Health.Cardinal symptom is: foreign body in pharynx sense, burn feeling, dryly itch or slight cough, pharyngalgia are arranged, function of deglutition is normal, during empty pharynx, sense of discomfort is obvious, pharyngeal symptom can be multi-lingual because overworking, suffer from cold, tobacco and wine excessively reach the aggravations such as direct stimulation, gets rid of that the early stage pharynx of the cancer of the esophagus is uncomfortable, the symptoms such as the swollen thing of epiglottis and supraglottic carcinoma patients, early stage bottleneck throat discomfort.Treatment time: drink continuously 1 month.
Efficacy assessment standard
Cure: subjective symptoms disappears or basic the disappearance, and pharyngeal mucous membrane is congested to disappear;
Effectively; Symptom obviously alleviates, and pharyngeal mucous membrane hyperemia is disappeared to some extent;
Invalid: symptom and sign is without improvement.
Concrete treatment situation is referring to table 2:
Table 2
Group Cure Effectively Invalid Efficient
Control group 1 4 11 5 75%
Control group 2 4 12 4 80%
Experimental group 7 12 1 95%
Three, the analysis of each active ingredient in tea: analyze discovery by detection, tea Content of Chlorogenic Acid 13.9mg/g prepared by experimental group of the present invention, its content surpasses more than 20 times of control group 2; Protocatechuic acid is 23.2mg/g, and content is about 15 times of left and right of control group 2; Quercetin is 8.7mg/g, and content surpasses 10 times of control group 2; Simultaneously, by detecting above-mentioned two groups of tea product, soak the tea discovery obtained, the content of experimental group edible burdock inulin is 236mg/L, and control group is only 21mg/L.
Although, above used general explanation, the specific embodiment and test, the present invention is described in detail, on basis of the present invention, can make some modifications or improvements it, and this will be apparent to those skilled in the art.Therefore, these modifications or improvements, all belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.

Claims (4)

1. the preparation method of a honeysuckle throat-moistening tea, is characterized in that, described method comprises the steps: that medicinal extract extracts, concentrate preparation, powder preparation and mixing.
2. preparation method as claimed in claim 1, is characterized in that, described method specifically comprises the steps:
1) medicinal extract extracts: take honeysuckle 1000g and the tuber of dwarf lilyturf 500g, mix, the decocting that adds 2 times of weight boils 2 hours, filter and collect filtrate, with the pH of the hydrochloric acid solution adjustment filtrate of 1mol/L, be 6, then filtrate is condensed into to the medicinal extract that density is 1.1g/m1;
2) concentrate preparation: get hawthorn 900g and mulberry leaf 100g, put in pulverizer and pulverize, take out and be laid into 1 square metre, ultraviolet ray is lower irradiates 5 minutes, and uitraviolet intensity is 1500uW/cm 2; Then use the deionized water of 2L as solvent, maintain under 0.2 atmospheric pressure state, 60 ℃ are hydrolyzed 1 day, filter and collect filtrate; Filtrate is placed in vacuum decker, is concentrated in vacuo to 1/5th of filtrate volume, obtain concentrate;
3) powder preparation: selecting fresh radix bardanae 800g, dries in the shade in the drying place that puts into cool place, ventilation, then is cut into the square fragment of 5-10mm, and the ethanol that to put into volume fraction be 70% soaks 30 minutes, and the decompression rotary evaporation is removed ethanol; Be placed in the lower irradiation of ultraviolet ray 10 minutes, uitraviolet intensity is 3000uW/cm 2, it is the above powder of 100 orders that the final powder breakdown mill becomes particle diameter;
4) mix: by step 1) medicinal extract, the step 2 that prepare) concentrate and the step 3 that prepare) powder for preparing mixes, obtain active ingredient, then mix with fructose, stir, finally be prepared into the particle that particle diameter is less than 10 microns, the sterilization paper bag and get final product of packing into; The mass ratio of described active ingredient and described fructose is 5: 1.
3. the tea for moistening prepared in accordance with the method for claim 2.
4. the health therapy function of tea for moistening claimed in claim 3.
CN201310347969.1A 2013-08-09 2013-08-09 Preparation method for honeysuckle throat smoothing tea Expired - Fee Related CN103431111B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106689586A (en) * 2016-12-12 2017-05-24 哈尔滨灵丹鸿运茶品有限公司 Arctium lappa and Japanese honeysuckle tea and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1511568A (en) * 2002-12-30 2004-07-14 郭浩山 Method for producing bagged tea for removing intense heat from throat
CN101874533A (en) * 2010-06-15 2010-11-03 吴振耀 Golden bamboo tea
CN101940246A (en) * 2010-07-24 2011-01-12 刘爱武 Honeysuckle throat-moistening tea
CN102429056A (en) * 2010-09-29 2012-05-02 南通玺运贸易有限公司 Honeysuckle flower tea containing soluble burdock dreg dietary fibers
CN102475175A (en) * 2010-11-29 2012-05-30 潘亚琴 Anemopyretic cold alleviating tea

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1511568A (en) * 2002-12-30 2004-07-14 郭浩山 Method for producing bagged tea for removing intense heat from throat
CN101874533A (en) * 2010-06-15 2010-11-03 吴振耀 Golden bamboo tea
CN101940246A (en) * 2010-07-24 2011-01-12 刘爱武 Honeysuckle throat-moistening tea
CN102429056A (en) * 2010-09-29 2012-05-02 南通玺运贸易有限公司 Honeysuckle flower tea containing soluble burdock dreg dietary fibers
CN102475175A (en) * 2010-11-29 2012-05-30 潘亚琴 Anemopyretic cold alleviating tea

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106689586A (en) * 2016-12-12 2017-05-24 哈尔滨灵丹鸿运茶品有限公司 Arctium lappa and Japanese honeysuckle tea and preparation method thereof

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