CN103417433A - Whitening and freckle-removing cream with whitening and freckle-removing functions, production technology of cream, and nitrogen filling machine - Google Patents
Whitening and freckle-removing cream with whitening and freckle-removing functions, production technology of cream, and nitrogen filling machine Download PDFInfo
- Publication number
- CN103417433A CN103417433A CN201310338208XA CN201310338208A CN103417433A CN 103417433 A CN103417433 A CN 103417433A CN 201310338208X A CN201310338208X A CN 201310338208XA CN 201310338208 A CN201310338208 A CN 201310338208A CN 103417433 A CN103417433 A CN 103417433A
- Authority
- CN
- China
- Prior art keywords
- whitening
- nitrogen
- eliminating cream
- spot eliminating
- cream
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title claims abstract description 107
- 230000002087 whitening effect Effects 0.000 title claims abstract description 93
- 239000006071 cream Substances 0.000 title claims abstract description 60
- 229910052757 nitrogen Inorganic materials 0.000 title claims abstract description 53
- 238000011049 filling Methods 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- 238000005516 engineering process Methods 0.000 title claims abstract description 16
- 208000003351 Melanosis Diseases 0.000 title abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 53
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims abstract description 51
- VYGQUTWHTHXGQB-FFHKNEKCSA-N Retinol Palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C VYGQUTWHTHXGQB-FFHKNEKCSA-N 0.000 claims abstract description 44
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229960003471 retinol Drugs 0.000 claims abstract description 25
- 235000020944 retinol Nutrition 0.000 claims abstract description 25
- 239000011607 retinol Substances 0.000 claims abstract description 25
- 239000002502 liposome Substances 0.000 claims abstract description 24
- OEWBEINAQKIQLZ-CMRBMDBWSA-N [(2s)-2-[(2r)-3,4-bis(2-hexyldecanoyloxy)-5-oxo-2h-furan-2-yl]-2-(2-hexyldecanoyloxy)ethyl] 2-hexyldecanoate Chemical compound CCCCCCCCC(CCCCCC)C(=O)OC[C@H](OC(=O)C(CCCCCC)CCCCCCCC)[C@H]1OC(=O)C(OC(=O)C(CCCCCC)CCCCCCCC)=C1OC(=O)C(CCCCCC)CCCCCCCC OEWBEINAQKIQLZ-CMRBMDBWSA-N 0.000 claims abstract description 22
- 229940108325 retinyl palmitate Drugs 0.000 claims abstract description 22
- 239000011769 retinyl palmitate Substances 0.000 claims abstract description 22
- 235000019172 retinyl palmitate Nutrition 0.000 claims abstract description 22
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 90
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 45
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 45
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 30
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims description 30
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 30
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 claims description 30
- 150000001875 compounds Chemical class 0.000 claims description 26
- 239000000203 mixture Substances 0.000 claims description 24
- 238000007789 sealing Methods 0.000 claims description 20
- 241000208681 Hamamelis virginiana Species 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 239000000047 product Substances 0.000 claims description 16
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 15
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims description 15
- 239000004322 Butylated hydroxytoluene Substances 0.000 claims description 15
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims description 15
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims description 15
- 229960000458 allantoin Drugs 0.000 claims description 15
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 15
- 229940095259 butylated hydroxytoluene Drugs 0.000 claims description 15
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims description 15
- 229940086555 cyclomethicone Drugs 0.000 claims description 15
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 15
- PKPOVTYZGGYDIJ-UHFFFAOYSA-N dioctyl carbonate Chemical compound CCCCCCCCOC(=O)OCCCCCCCC PKPOVTYZGGYDIJ-UHFFFAOYSA-N 0.000 claims description 15
- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 claims description 15
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims description 15
- 229910052740 iodine Inorganic materials 0.000 claims description 15
- 239000011630 iodine Substances 0.000 claims description 15
- 238000011068 loading method Methods 0.000 claims description 15
- KRPAJLYSLFNDOA-UHFFFAOYSA-N mephenesin carbamate Chemical compound CC1=CC=CC=C1OCC(O)COC(N)=O KRPAJLYSLFNDOA-UHFFFAOYSA-N 0.000 claims description 15
- 229950006838 mephenesin carbamate Drugs 0.000 claims description 15
- FBUKVWPVBMHYJY-UHFFFAOYSA-M nonanoate Chemical compound CCCCCCCCC([O-])=O FBUKVWPVBMHYJY-UHFFFAOYSA-M 0.000 claims description 15
- 239000004006 olive oil Substances 0.000 claims description 15
- 235000008390 olive oil Nutrition 0.000 claims description 15
- 239000011265 semifinished product Substances 0.000 claims description 15
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims description 15
- 239000004408 titanium dioxide Substances 0.000 claims description 15
- 235000010384 tocopherol Nutrition 0.000 claims description 15
- 229960001295 tocopherol Drugs 0.000 claims description 15
- 229930003799 tocopherol Natural products 0.000 claims description 15
- 239000011732 tocopherol Substances 0.000 claims description 15
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 15
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 14
- 239000000787 lecithin Substances 0.000 claims description 14
- 229940067606 lecithin Drugs 0.000 claims description 14
- 235000010445 lecithin Nutrition 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 239000003921 oil Substances 0.000 claims description 9
- 235000019198 oils Nutrition 0.000 claims description 9
- 230000002045 lasting effect Effects 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 7
- 229940082431 hamamelis virginiana leaf extract Drugs 0.000 claims description 7
- -1 Parleam Chemical compound 0.000 claims description 6
- 229960004106 citric acid Drugs 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- FDDDEECHVMSUSB-UHFFFAOYSA-N sulfanilamide Chemical compound NC1=CC=C(S(N)(=O)=O)C=C1 FDDDEECHVMSUSB-UHFFFAOYSA-N 0.000 claims description 6
- 239000003643 water by type Substances 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 4
- 210000003437 trachea Anatomy 0.000 claims description 4
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 10
- 239000002537 cosmetic Substances 0.000 abstract description 9
- 238000002156 mixing Methods 0.000 abstract description 6
- 231100000331 toxic Toxicity 0.000 abstract description 3
- 230000002588 toxic effect Effects 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract 5
- 239000002131 composite material Substances 0.000 abstract 4
- 241000208680 Hamamelis mollis Species 0.000 abstract 1
- 239000002085 irritant Substances 0.000 abstract 1
- 231100000021 irritant Toxicity 0.000 abstract 1
- 229940118846 witch hazel Drugs 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 12
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 6
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 6
- 241000863032 Trieres Species 0.000 description 6
- 239000008187 granular material Substances 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 238000010612 desalination reaction Methods 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 3
- 229930003268 Vitamin C Natural products 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 238000003556 assay Methods 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 230000005484 gravity Effects 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 235000019154 vitamin C Nutrition 0.000 description 3
- 239000011718 vitamin C Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 208000037259 Amyloid Plaque Diseases 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- 101100117236 Drosophila melanogaster speck gene Proteins 0.000 description 1
- 206010020880 Hypertrophy Diseases 0.000 description 1
- 206010023126 Jaundice Diseases 0.000 description 1
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 description 1
- 241001597008 Nomeidae Species 0.000 description 1
- 206010042496 Sunburn Diseases 0.000 description 1
- 102000003425 Tyrosinase Human genes 0.000 description 1
- 108060008724 Tyrosinase Proteins 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229910052756 noble gas Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 210000002706 plastid Anatomy 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000036559 skin health Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 210000000438 stratum basale Anatomy 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
Images
Landscapes
- Cosmetics (AREA)
Abstract
The invention relates to a whitening and freckle-removing cream with whitening and freckle-removing functions, a production technology of the cream and a nitrogen filling machine, and aims to prepare a cosmetic with better whitening and freckle-removing efficacies and without any irritant and toxic side effects as well as provide equipment which can prolong the quality guarantee period of the cosmetic. The invention adopts the technical scheme as follows: the whitening and freckle-removing cream added with whitening and freckle-removing composite raw materials comprises a witch hazel extract, ascorbyl tetraisopalmitate, retinyl palmitate, liposome-coated retinol and other raw materials. The production technology comprises the following steps: 1) mixing a plurality of raw materials into an oil-phase composite solution; 2) mixing a plurality of raw materials into a water-phase composite solution; 3) mixing and homogenizing the two composite solutions; 4) adding a plurality of raw materials, and homogenizing; 5) filling nitrogen, and performing endcapping to obtain a product. A filling assembly of a nitrogen filling and endcapping machine comprises an injecting barrel, an inner material filling joint, a nitrogen filling joint and an exhausting joint, and is provided with an electromagnetic valve controlled by a PLC controller.
Description
Technical field
What the present invention relates to the production technology of a kind of whitening and spot eliminating cream, whitening and spot eliminating cream and production whitening and spot eliminating cream fills the nitrogen conduit loading tail sealing machine.
Background technology
When ultraviolet radiation skin, the chromoplast that is arranged in stratum basale can secrete a kind of Mai Laning pigment, thereby the activity that it can activate tryrosinase makes tyrosine in tryrosinase and blood react, generates melanin.Melanin can effectively absorb ultraviolet, and the protection human body is avoided ultraviolet injury.But, after if melanin fails to excrete by body metabolism, will remain in epidermal area and form pigmented spots (comprising freckle, sunburn, black speck etc.), affect very much the aesthetic feeling of face.
And, in the production process of whitening class cosmetics (being generally the emulsifiable paste shape with gluey), usually use flexible pipe loading equipment to carry out the fill sealing.But owing to being subject to device-restrictive, cosmetics entrained air very easily during fill, deposit a period of time after airborne oxygen can make cosmetics the jaundice denaturalization phenomenon occur, greatly affected product quality.
Summary of the invention
The objective of the invention is to overcome the deficiency in the above-mentioned background technology, what a kind of whitening and spot eliminating cream, production technology and production whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material was provided respectively fills the nitrogen conduit loading tail sealing machine; This product and production technology thereof should be able to be produced a kind ofly has better whitening effect and the cosmetics without any zest and toxic and side effects to skin; Thereby this equipment should be able to make cosmetics avoid contacting with air the quality guarantee period that extends cosmetics.
Technical scheme provided by the invention is: a kind of whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material is characterized in that this whitening and spot eliminating cream comprises following component and weight portion: propylene glycol 5.0～10.0%, ethylhexyl palmitate 5.0～8.0%, Cyclomethicone 4.0～6.0%, stearyl alcohol polyethers-23.0～4.0%, cetearyl alcohol 3.0～4.0%, Parleam 3.0～4.0%, stearyl alcohol polyethers-212.0～2.5%, the different pelargonate 2.0～2.5% of cetearyl alcohol, olive oil 1.0～1.5%, dicaprylyl carbonate 1.0～1.5%, titanium dioxide 1.0～1.5%, AVC 0.3～0.6%, Ascorbyl Tetraisopalmitate 0.3～0.5%, allantoin 0.1～0.2%, citric acid 0.1～0.2%, tocopherol acetas 0.1～0.2%, lecithin 0.1～0.2%, butylated hydroxytoluene 0.1～0.2%, retinyl palmitate 0.1～0.15%, EDETATE SODIUM 0.05～0.1%, Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract 0.05～0.10%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01～0.04%, essence 0.03～0.05%, liposomes coats retinol 0.02～0.05%, and all the other are deionized waters, whitening and speckle dispelling compound material wherein (Ascorbyl Tetraisopalmitate, retinyl palmitate and liposomes coat retinol) content is 0.42～0.7%.
A kind of whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material, is characterized in that this whitening and spot eliminating cream comprises following component and weight portion: propylene glycol 5.0～10.0%, ethylhexyl palmitate 5.0～8.0%, Cyclomethicone 4.0～6.0%, stearyl alcohol polyethers-23.0～4.0%, cetearyl alcohol 3.0～4.0%, Parleam 3.0～4.0%, stearyl alcohol polyethers-212.0～2.5%, the different pelargonate 2.0～2.5% of cetearyl alcohol, olive oil 1.0～1.5%, dicaprylyl carbonate 1.0～1.5%, titanium dioxide 1.0～1.5%, AVC 0.3～0.6%, Ascorbyl Tetraisopalmitate 0.25～0.45%, allantoin 0.1～0.2%, citric acid 0.1～0.2%, tocopherol acetas 0.1～0.2%, lecithin 0.1～0.2%, butylated hydroxytoluene 0.1～0.2%, retinyl palmitate 0.05～0.10%, EDETATE SODIUM 0.05～0.1%, Hamamelis virginiana leaf extract 0.05～0.10%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01～0.04%, essence 0.03～0.05%, liposomes coats retinol 0.01～0.03%, and all the other are deionized waters, whitening and speckle dispelling compound material wherein (Ascorbyl Tetraisopalmitate, retinyl palmitate and liposomes coat retinol) content is 0.31～0.58%.
A kind of whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material, it is characterized in that this whitening and spot eliminating cream comprises following component and weight portion: propylene glycol 6.0%, ethylhexyl palmitate 5.5%, Cyclomethicone 4.0%, stearyl alcohol polyethers-23.0%, cetearyl alcohol 3.0%, Parleam 3.0%, stearyl alcohol polyethers-212.0%, the different pelargonate 2.0% of cetearyl alcohol, olive oil 1.0%, dicaprylyl carbonate 1.0%, titanium dioxide 1.0%, AVC 0.4%, Ascorbyl Tetraisopalmitate 0.4%, allantoin 0.2%, citric acid 0.1%, tocopherol acetas 0.1%, lecithin 0.1%, butylated hydroxytoluene 0.1%, retinyl palmitate 0.10%, EDETATE SODIUM 0.05%, Hamamelis virginiana leaf extract 0.05%, DMDM Hydantoin 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01%, essence 0.05%, liposomes coats retinol 0.02%, all the other are deionized waters, whitening and speckle dispelling compound material wherein (Ascorbyl Tetraisopalmitate, retinyl palmitate and liposomes coat retinol) content is 0.52%, is optimal proportion.
A kind of production technology of adding the whitening and spot eliminating cream of whitening and speckle dispelling compound material comprises the following steps:
1), by ethylhexyl palmitate, Cyclomethicone, stearyl alcohol polyethers-2, cetearyl alcohol, Parleam, stearyl alcohol polyethers-21, the different pelargonate of cetearyl alcohol, olive oil, dicaprylyl carbonate, titanium dioxide, Ascorbyl Tetraisopalmitate, tocopherol acetas, butylated hydroxytoluene, lecithin, retinyl palmitate mix and blend heating for dissolving, temperature control becomes oil phase combination liquid at 70-80 ℃;
2), by propylene glycol, AVC, allantoin, citric acid, EDETATE SODIUM, deionized water mix and blend heating for dissolving, temperature control becomes water combination liquid at 80-90 ℃;
3) oil phase is combined to liquid and pour in water combination liquid, after homogenizing, lasting stirring cools;
4) in the semi-finished product that make in previous step, add Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract, DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, essence, liposomes to coat retinol, evacuation being cooled to below 35 ℃ after homogenizing, obtain the semi-finished product of whitening and spot eliminating cream;
5) semi-finished product of whitening and spot eliminating cream are obtained to the whitening and spot eliminating cream finished product after filling nitrogen fill sealing.
Rev/min rotating speed in described step 3) during homogenizing is 2500-3500RPM(Revolutions Per Minute) and the time be 4-6 minute, cooling rear temperature is 42-48 ℃.
Homogenizing process in described step 4) is: first when rotating speed is 2500-3500RPM, stir 0.5-1.5 minute, then rotating speed is reduced to 800-1200RPM evacuation from 0 to-0.1Mpa, lasting stirring is cooled to below 35 degrees centigrade.
A kind of produce whitening and spot eliminating cream fill the nitrogen conduit loading tail sealing machine, the interior material filling adaptor that filling components wherein comprises the material feeding bucket, be arranged on material feeding bucket below and be connected with the material feeding bottom of the barrel is characterized in that: on described interior material filling adaptor, also be arranged side by side with store up that nitrogen equipment is connected fill the nitrogen joint and for derive air exhaust joint; Described interior material filling adaptor with fill the nitrogen joint on electromagnetic valve is housed and all electromagnetic valves all are connected with the PLC controller.
The described nitrogen joint that fills is connected with the storage nitrogen equipment by flexible pipe.
Described exhaust joint is by trachea and extraneous conducting.
Described nitrogen storage equipment is nitrogen cylinder.
The invention has the beneficial effects as follows:
1, be added with whitening and speckle dispelling compound material (comprising that Ascorbyl Tetraisopalmitate, retinyl palmitate, liposomes coat retinol) in the whitening and spot eliminating cream in the present invention; Ascorbyl Tetraisopalmitate and retinyl palmitate are fat soluble vitamin C derivant, can resolve into free vitamin C after being absorbed by the skin, free vitamin C can suppress the activity of Tyrosinase, thereby avoids melanic generation and stimulation collagen hypertrophy with the desalination microgroove; And liposomes coats liposomes carrier in retinol and can enter in horny layer and discharge retinol, reach and accelerate cutin metabolism and desalination pigmented spots effect;
Therefore, this whitening and spot eliminating cream product has whitening and speckle dispelling effect preferably, can effectively desalinate skin pigment spot and microgroove, make skin health bright, and this product, is suitable for any ages and uses (especially the senile plaque for older person has better effect) without any zest and toxic and side effects skin.
2, the production technology provided can be guaranteed the quality of whitening and spot eliminating cream, and production efficiency is higher.
3, filling in the nitrogen conduit loading tail sealing machine in the present invention has additional nitrogen charging device, by pouring in advance nitrogen when the fill to discharge the air in product, avoids product oxidation deterioration to occur, the activity of the QUBAN SHUANG of can effectively staying pale when long-time the preservation.
The accompanying drawing explanation
Fig. 1 is the main TV structure schematic diagram that fills the nitrogen conduit loading tail sealing machine in the present invention.
Fig. 2 is the structure for amplifying schematic diagram of A section in Fig. 1.
The specific embodiment
Liposomes of the present invention coats retinol (retinol is vitamin A), directly from German ROVI COSMETICS company, buys (referring to the said firm's product description).
Hamamelis virginiana leaf extract of the present invention, directly buy (referring to the said firm's product description from Taiwan Wei Heng Industry Co.,Ltd; The description name is called " Radix Hamamelidis Mollis extraction ").
Below in conjunction with non-limiting examples, the whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material is described further.
Embodiment 1
Get propylene glycol 5.0Kg, ethylhexyl palmitate 5.0Kg, Cyclomethicone 4.0Kg, stearyl alcohol polyethers-23.0Kg, cetearyl alcohol 3.0Kg, Parleam 3.0Kg, stearyl alcohol polyethers-212.0Kg, the different pelargonate 2.0Kg of cetearyl alcohol, olive oil 1.0Kg, dicaprylyl carbonate 1.0Kg, titanium dioxide 1.0Kg, AVC 0.3Kg, Ascorbyl Tetraisopalmitate 0.3Kg, allantoin 0.1Kg, citric acid 0.1Kg, tocopherol acetas 0.1Kg, lecithin 0.1Kg, butylated hydroxytoluene 0.1Kg, retinyl palmitate 0.1Kg, EDETATE SODIUM 0.05Kg, Hamamelis virginiana leaf extract 0.05Kg, DMDM Hydantoin 0.05Kg, iodine propilolic alcohol butyl mephenesin Carbamate 0.01Kg, essence 0.03Kg, liposomes coats retinol 0.02Kg, surplus is deionized water 68.59Kg.
1) by formula ratio, oil phase component ethylhexyl palmitate, Cyclomethicone, stearyl alcohol polyethers-2, cetearyl alcohol, Parleam, stearyl alcohol polyethers-21, the different pelargonate of cetearyl alcohol, olive oil, dicaprylyl carbonate, titanium dioxide, Ascorbyl Tetraisopalmitate, tocopherol acetas, butylated hydroxytoluene, lecithin, retinyl palmitate mix and blend are heated to all dissolve without after granule, temperature control to 75 is ℃ standby:
2) water component propylene glycol, AVC, allantoin, citric acid, EDETATE SODIUM, deionized water mix and blend are heated to all dissolve without after granule, temperature control to 85 is ℃ standby:
3) until A with after B completes mutually, pour mutually A into the B phase, homogenizing adjustment of rotational speed to 3,000RPM, homogenizing 5 minutes continues to stir the cooling C phase that obtains:
4) when C phase temperature is down to 45 ℃, active adding ingredient Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract, DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, essence, liposomes are coated to retinol to add, by homogenizing adjustment of rotational speed to 3,000RPM, time 1Mins, after completing this step, adjust mixing speed to 1,000RPM, evacuation is from 0 to-0.1Mpa, and lasting stirring is cooled to below 35 ℃, by the negative pressure transportation discharging, get final product to obtain a kind of whitening and spot eliminating cream semi-finished product for standby of adding the whitening and speckle dispelling compound material again:
5) treat a kind of whitening and spot eliminating cream semi-finished product physical and chemical index that adds the whitening and speckle dispelling compound material after the assay was approved, see through the Full automatic soft pipe conduit loading tail sealing machine, control electromagnetic valve by PLC, realize that every plastic-aluminum flexible pipe is filled with inert nitrogen gas before fill, inflated with nitrogen interface 8MM diameter, the interface 2MM diameter of giving vent to anger, inflated with nitrogen pressure is more than 0.4MP, utilize the specific gravity of gas difference, oxygen is discharged, fill obtains the whitening and spot eliminating cream finished product.
Embodiment 2
Get propylene glycol 10.0Kg, ethylhexyl palmitate 8.0Kg, Cyclomethicone 6.0Kg, stearyl alcohol polyethers-24.0Kg, cetearyl alcohol 4.0Kg, Parleam 4.0Kg, stearyl alcohol polyethers-212.5Kg, the different pelargonate 2.5Kg of cetearyl alcohol, olive oil 1.5Kg, dicaprylyl carbonate 1.5Kg, titanium dioxide 1.5Kg, AVC 0.6Kg, Ascorbyl Tetraisopalmitate 0.5Kg, allantoin 0.2Kg, citric acid 0.2Kg, tocopherol acetas 0.2Kg, lecithin 0.2Kg, butylated hydroxytoluene 0.2Kg, retinyl palmitate 0.15Kg, EDETATE SODIUM 0.1Kg, Hamamelis virginiana leaf extract 0.10Kg, DMDM Hydantoin 0.10Kg, iodine propilolic alcohol butyl mephenesin Carbamate 0.04Kg, essence 0.05Kg, liposomes coats retinol 0.05Kg, deionized water 51.81Kg.
1) by formula ratio, oil phase component ethylhexyl palmitate, Cyclomethicone, stearyl alcohol polyethers-2, cetearyl alcohol, Parleam, stearyl alcohol polyethers-21, the different pelargonate of cetearyl alcohol, olive oil, dicaprylyl carbonate, titanium dioxide, Ascorbyl Tetraisopalmitate, tocopherol acetas, butylated hydroxytoluene, lecithin, retinyl palmitate mix and blend are heated to all dissolve without after granule, temperature control to 75 is ℃ standby:
2) water component propylene glycol, AVC, allantoin, citric acid, EDETATE SODIUM, deionized water mix and blend are heated to all dissolve without after granule, temperature control to 85 is ℃ standby:
3) until A with after B completes mutually, pour mutually A into the B phase, homogenizing adjustment of rotational speed to 3,000RPM, homogenizing 5 minutes continues to stir the cooling C phase that obtains:
4) when C phase temperature is down to 45 ℃, active adding ingredient Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract, DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, essence, liposomes are coated to retinol to add, by homogenizing adjustment of rotational speed to 3,000RPM, time 1Mins, after completing this step, adjust mixing speed to 1,000RPM, evacuation is from 0 to-0.1Mpa, and lasting stirring is cooled to below 35 ℃, by the negative pressure transportation discharging, get final product to obtain a kind of whitening and spot eliminating cream semi-finished product for standby of adding the whitening and speckle dispelling compound material again:
5) treat a kind of whitening and spot eliminating cream semi-finished product physical and chemical index that adds the whitening and speckle dispelling compound material after the assay was approved, see through the Full automatic soft pipe conduit loading tail sealing machine, control electromagnetic valve by PLC, realize that every plastic-aluminum flexible pipe is filled with inert nitrogen gas before fill, inflated with nitrogen interface 8MM diameter, the interface 2MM diameter of giving vent to anger, inflated with nitrogen pressure is more than 0.4MP, utilize the specific gravity of gas difference, oxygen is discharged, fill obtains the whitening and spot eliminating cream finished product.
Embodiment 3
Get propylene glycol 6.0Kg, ethylhexyl palmitate 5.5Kg, Cyclomethicone 4.0Kg, stearyl alcohol polyethers-23.0Kg, cetearyl alcohol 3.0Kg, Parleam 3.0Kg, stearyl alcohol polyethers-212.0Kg, the different pelargonate 2.0Kg of cetearyl alcohol, olive oil 1.0Kg, dicaprylyl carbonate 1.0Kg, titanium dioxide 1.0Kg, AVC 0.4Kg, allantoin 0.2Kg, citric acid 0.1Kg, tocopherol acetas 0.1Kg, lecithin 0.1Kg, butylated hydroxytoluene 0.1Kg, EDETATE SODIUM 0.05Kg, Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract 0.05Kg, DMDM Hydantoin 0.05Kg, iodine propilolic alcohol butyl mephenesin Carbamate 0.03Kg, essence 0.05Kg, Ascorbyl Tetraisopalmitate 0.4Kg, retinyl palmitate 0.10Kg, liposomes coats retinol 0.02Kg, deionized water 66.73Kg.
1) by formula ratio, oil phase component ethylhexyl palmitate, Cyclomethicone, stearyl alcohol polyethers-2, cetearyl alcohol, Parleam, stearyl alcohol polyethers-21, the different pelargonate of cetearyl alcohol, olive oil, dicaprylyl carbonate, titanium dioxide, Ascorbyl Tetraisopalmitate, tocopherol acetas, butylated hydroxytoluene, lecithin, retinyl palmitate mix and blend are heated to all dissolve without after granule, temperature control to 70 is ℃ standby:
2) water component propylene glycol, AVC, allantoin, citric acid, EDETATE SODIUM, deionized water mix and blend are heated to all dissolve without after granule, temperature control to 80 is ℃ standby:
3) until A with after B completes mutually, pour mutually A into the B phase, homogenizing adjustment of rotational speed to 3,000RPM, homogenizing 5 minutes continues to stir the cooling C phase that obtains:
4) when C phase temperature is down to 45 ℃, active adding ingredient Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract, DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, essence, liposomes are coated to retinol to add, by homogenizing adjustment of rotational speed to 3,000RPM, time 1Mins, after completing this step, adjust mixing speed to 1,000RPM, evacuation is from 0 to-0.1Mpa, and lasting stirring is cooled to 33 ℃, by the negative pressure transportation discharging, get final product to obtain a kind of whitening and spot eliminating cream semi-finished product for standby of adding the whitening and speckle dispelling compound material again:
5) treat this whitening and spot eliminating cream semi-finished product physical and chemical index after the assay was approved, see through the Full automatic soft pipe conduit loading tail sealing machine, control electromagnetic valve by PLC, realize that every plastic-aluminum flexible pipe is filled with inert nitrogen gas before fill, inflated with nitrogen interface 8MM diameter, the interface 2MM diameter of giving vent to anger, inflated with nitrogen pressure is more than 0.4MP, utilize the specific gravity of gas difference, oxygen is discharged, fill obtains the whitening and spot eliminating cream finished product.
For understanding result of use of the present invention, form with questionnaire survey has been carried out investigation on probation widely to this product, men and women trier 250 people in all parts of the country are included in this investigation altogether in, male 110 people wherein, women 140 people, the oldest 58 years old, minimum 30 years old, the mean age one's mid-40s, regain 190 parts of effective questionnaires altogether.
190 triers use a kind of whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material, and after 3 months, to whitening and speckle dispelling, the result of relevant indices degree self evaluation is as follows:
Dwindle the pore fineness: have respectively 30% and 55% trier to have moderate to improve and obviously improve;
Promote the skin lightness: have respectively 40% and 70% trier to have moderate to improve and obviously improve;
Desalination skin speckle amount: have respectively 50% and 75% trier to have moderate to improve and obviously improve;
Reduce skin microgroove amount: have respectively 45% and 50% trier to have moderate to improve and obviously improve;
From the result of trier's self assessment, can find out, this product to dwindle pore careful, promote that skin is bright, the desalination skin speckle, reduce the skin microgroove improvement is in various degree arranged.According to survey result, show: the whitening and spot eliminating cream of this interpolation whitening and speckle dispelling compound material has desalinates skin speckle and microgroove effect preferably.
Below in conjunction with non-limiting examples, a kind of production technology of adding the whitening and spot eliminating cream of whitening and speckle dispelling compound material is described further.
A kind of production technology of adding the whitening and spot eliminating cream of whitening and speckle dispelling compound material comprises the following steps:
1), by after ethylhexyl palmitate, Cyclomethicone, stearyl alcohol polyethers-2, cetearyl alcohol, Parleam, stearyl alcohol polyethers-21, the different pelargonate of cetearyl alcohol, olive oil, dicaprylyl carbonate, titanium dioxide, Ascorbyl Tetraisopalmitate, tocopherol acetas, butylated hydroxytoluene, retinyl palmitate mix and blend heating for dissolving, temperature control becomes oil phase combination liquid at 70-80 ℃.
2), by after propylene glycol, AVC, allantoin, citric acid, EDETATE SODIUM, deionized water mix and blend heating for dissolving, temperature control becomes water combination liquid at 80-90 ℃.
3) oil phase is combined to liquid and pour in water combination liquid, cooling after homogenizing; Wherein, rotating speed during homogenizing is that 2500-3500RPM and time are 4-6 minute, and cooling rear temperature is 42-48 ℃;
4) in the semi-finished product that make in previous step, add Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract, DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, essence, liposomes to coat retinol, obtain the semi-finished product of whitening and spot eliminating cream after homogenizing; Its homogenizing process is,
1. the homogenizing rotating speed is 2500-3500RPM, stirs 0.5-1.5 minute;
2. speed of agitator is reduced to 800-1200RPM evacuation from 0 to-0.1Mpa, lasting stirring is cooled to below 35 degrees centigrade.
5) semi-finished product of whitening and spot eliminating cream are obtained to the whitening and spot eliminating cream finished product after filling nitrogen fill sealing.
Below in conjunction with Figure of description, the nitrogen conduit loading tail sealing machine that fills in the present invention is described further, but the present invention is not limited to following examples.
As shown in Figure 1, a kind of produce whitening and spot eliminating cream fill the nitrogen conduit loading tail sealing machine, filling components wherein comprises material feeding bucket 1, interior material filling adaptor 2, fills nitrogen joint 3, exhaust joint 4, storage nitrogen equipment 6, electromagnetic valve 5, PLC controller 7; Folding sealing operation is completed by folding sealing assembly (conventional equipment).
Wherein: the container that the material feeding bucket is the housing shape, its top be shaped with for feed openings, its bottom is for taper; Interior material filling adaptor, fill nitrogen joint, exhaust joint and all be arranged in the adapter 7 of material feeding bucket below and be arranged side by side together; Interior material filling adaptor is communicated with the material feeding bottom of the barrel by material receiving tube; Fill the nitrogen joint and be communicated with (the storage nitrogen equipment is generally nitrogen cylinder, and internal pressure is more than 0.4MP) by flexible pipe 6-1 with the storage nitrogen equipment; Exhaust joint also is communicated with atmosphere by trachea 4-1; The trachea of the material receiving tube of interior material filling adaptor, the flexible pipe that fills the nitrogen joint and exhaust joint all interts and is arranged in adapter, and material receiving tube and flexible pipe have been installed respectively electromagnetic valve; All electromagnetic valves all are connected (the PLC controller is for controlling all electromagnetic valves) with the PLC controller; In addition, the diameter that fills the nitrogen joint is generally 6-10MM, and the diameter of exhaust joint is general 1-3MM.
Work process of the present invention is as follows:
1, all electromagnetic valves, all in closed condition, are put into container to be filled on the rotary-tray of filling machine;
2, the electromagnetic valve filled on the nitrogen joint is opened, and the container that is positioned at current station is charged noble gas, and the air in container is discharged from exhaust joint;
3, fill the closed electromagnetic valve on the nitrogen joint, the electromagnetic valve on interior material filling adaptor is opened, and interior material filling adaptor pours into whitening and spot eliminating cream in container;
Electromagnetic valve and the rotary-tray of 4, closing on interior material filling adaptor start, and carry out the fill of next station.
Claims (10)
1. a whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material, is characterized in that this whitening and spot eliminating cream comprises following component and weight portion: propylene glycol 5.0～10.0%, ethylhexyl palmitate 5.0～8.0%, Cyclomethicone 4.0～6.0%, stearyl alcohol polyethers-23.0～4.0%, cetearyl alcohol 3.0～4.0%, Parleam 3.0～4.0%, stearyl alcohol polyethers-212.0～2.5%, the different pelargonate 2.0～2.5% of cetearyl alcohol, olive oil 1.0～1.5%, dicaprylyl carbonate 1.0～1.5%, titanium dioxide 1.0～1.5%, AVC 0.3～0.6%, Ascorbyl Tetraisopalmitate 0.3～0.5%, allantoin 0.1～0.2%, citric acid 0.1～0.2%, tocopherol acetas 0.1～0.2%, lecithin 0.1～0.2%, butylated hydroxytoluene 0.1～0.2%, retinyl palmitate 0.1～0.15%, EDETATE SODIUM 0.05～0.1%, Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract 0.05～0.10%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01～0.04%, essence 0.03～0.05%, liposomes coats retinol 0.02～0.05%, and all the other are deionized waters.
2. a whitening and spot eliminating cream of adding the whitening and speckle dispelling compound material, is characterized in that this whitening and spot eliminating cream comprises following component and weight portion: propylene glycol 5.0～10.0%, ethylhexyl palmitate 5.0～8.0%, Cyclomethicone 4.0～6.0%, stearyl alcohol polyethers-23.0～4.0%, cetearyl alcohol 3.0～4.0%, Parleam 3.0～4.0%, stearyl alcohol polyethers-212.0～2.5%, the different pelargonate 2.0～2.5% of cetearyl alcohol, olive oil 1.0～1.5%, dicaprylyl carbonate 1.0～1.5%, titanium dioxide 1.0～1.5%, AVC 0.3～0.6%, Ascorbyl Tetraisopalmitate 0.25～0.45%, allantoin 0.1～0.2%, citric acid 0.1～0.2%, tocopherol acetas 0.1～0.2%, lecithin 0.1～0.2%, butylated hydroxytoluene 0.1～0.2%, retinyl palmitate 0.05～0.10%, EDETATE SODIUM 0.05～0.1%, Hamamelis virginiana leaf extract 0.05～0.10%, DMDM Hydantoin 0.05～0.10%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01～0.04%, essence 0.03～0.05%, liposomes coats retinol 0.01～0.03%, and all the other are deionized waters.
3. the whitening and spot eliminating cream of interpolation whitening and speckle dispelling compound material according to claim 1 and 2, it is characterized in that this whitening and spot eliminating cream comprises following component and weight portion: propylene glycol 6.0%, ethylhexyl palmitate 5.5%, Cyclomethicone 4.0%, stearyl alcohol polyethers-23.0%, cetearyl alcohol 3.0%, Parleam 3.0%, stearyl alcohol polyethers-212.0%, the different pelargonate 2.0% of cetearyl alcohol, olive oil 1.0%, dicaprylyl carbonate 1.0%, titanium dioxide 1.0%, AVC 0.4%, Ascorbyl Tetraisopalmitate 0.4%, allantoin 0.2%, citric acid 0.1%, tocopherol acetas 0.1%, lecithin 0.1%, butylated hydroxytoluene 0.1%, retinyl palmitate 0.10%, EDETATE SODIUM 0.05%, Hamamelis virginiana leaf extract 0.05%, DMDM Hydantoin 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.01%, essence 0.05%, liposomes coats retinol 0.02%, all the other are deionized waters, whitening and speckle dispelling compound material wherein (Ascorbyl Tetraisopalmitate, retinyl palmitate and liposomes coat retinol) content is 0.52%.
4. a production technology of adding the whitening and spot eliminating cream of whitening and speckle dispelling compound material comprises the following steps:
1), by ethylhexyl palmitate, Cyclomethicone, stearyl alcohol polyethers-2, cetearyl alcohol, Parleam, stearyl alcohol polyethers-21, the different pelargonate of cetearyl alcohol, olive oil, dicaprylyl carbonate, titanium dioxide, Ascorbyl Tetraisopalmitate, tocopherol acetas, butylated hydroxytoluene, lecithin, retinyl palmitate mix and blend heating for dissolving, temperature control becomes oil phase combination liquid at 70-80 ℃;
2), by propylene glycol, AVC, allantoin, citric acid, EDETATE SODIUM, deionized water mix and blend heating for dissolving, temperature control becomes water combination liquid at 80-90 ℃;
3) oil phase is combined to liquid and pour in water combination liquid, after homogenizing, lasting stirring cools;
4) in the semi-finished product that make in previous step, add Hamamelis virginiana (HAMAMELIS VIRGINIANA) leaf extract, DMDM Hydantoin, iodine propilolic alcohol butyl mephenesin Carbamate, essence, liposomes to coat retinol, evacuation being cooled to below 35 ℃ after homogenizing, obtain the semi-finished product of whitening and spot eliminating cream;
5) semi-finished product of whitening and spot eliminating cream are obtained to the whitening and spot eliminating cream finished product after filling nitrogen fill sealing.
5. the production technology of the whitening and spot eliminating cream of interpolation whitening and speckle dispelling compound material according to claim 4, rotating speed while it is characterized in that homogenizing in described step 3) is 2500-3500RPM{Revolutions Per Minute(rev/min) } and the time be 4-6 minute, cooling rear temperature is 42-48 ℃.
6. the production technology of the whitening and spot eliminating cream of interpolation whitening and speckle dispelling compound material according to claim 5, it is characterized in that the homogenizing process in described step 4) is: first when rotating speed is 2500-3500RPM, stir 0.5-1.5 minute, then rotating speed is reduced to 800-1200RPM evacuation from 0 to-0.1pa, lasting stirring is cooled to below 35 degrees centigrade.
One kind produce whitening and spot eliminating cream fill the nitrogen conduit loading tail sealing machine, the interior material filling adaptor (2) that filling components wherein comprises material feeding bucket (1), be arranged on material feeding bucket below and be connected with the material feeding bottom of the barrel is characterized in that: on described interior material filling adaptor, also be arranged side by side with store up that nitrogen equipment is connected fill nitrogen joint (3) and for derive air exhaust joint (4); Described interior material filling adaptor with fill the nitrogen joint on electromagnetic valve is housed and all electromagnetic valves all are connected with PLC controller (7).
According to claim 7 a kind of produce whitening and spot eliminating cream fill the nitrogen conduit loading tail sealing machine, it is characterized in that described fill the nitrogen joint by flexible pipe (6-1) with store up nitrogen equipment (6) and be connected.
According to claim 8 a kind of produce whitening and spot eliminating cream fill the nitrogen conduit loading tail sealing machine, it is characterized in that described exhaust joint is by trachea (4-1) and extraneous conducting.
According to claim 9 a kind of produce whitening and spot eliminating cream fill the nitrogen conduit loading tail sealing machine, it is characterized in that described nitrogen storage equipment is nitrogen cylinder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310338208.XA CN103417433B (en) | 2013-08-05 | 2013-08-05 | Whitening and freckle-removing cream with whitening and freckle-removing functions, production technology of cream, and nitrogen filling machine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310338208.XA CN103417433B (en) | 2013-08-05 | 2013-08-05 | Whitening and freckle-removing cream with whitening and freckle-removing functions, production technology of cream, and nitrogen filling machine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103417433A true CN103417433A (en) | 2013-12-04 |
| CN103417433B CN103417433B (en) | 2015-04-22 |
Family
ID=49643180
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310338208.XA Expired - Fee Related CN103417433B (en) | 2013-08-05 | 2013-08-05 | Whitening and freckle-removing cream with whitening and freckle-removing functions, production technology of cream, and nitrogen filling machine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103417433B (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105947953A (en) * | 2016-06-30 | 2016-09-21 | 东莞轩朗实业有限公司 | Production device for quantum dot light bar |
| CN106265338A (en) * | 2016-09-14 | 2017-01-04 | 广东丸美生物技术股份有限公司 | A kind of skin care oil and preparation method that there is Whitening, spot and purify smooth skin |
| CN106821794A (en) * | 2017-01-11 | 2017-06-13 | 杭州菲丝凯化妆品有限公司 | Eye bottoming cream and preparation method thereof |
| CN108210362A (en) * | 2016-12-14 | 2018-06-29 | 天津强微特生物科技有限公司 | A kind of VACE Essences of freckle removing and whitening |
| CN108888522A (en) * | 2018-07-24 | 2018-11-27 | 上海东晟源日化有限公司 | A kind of skin care liposomes inclusion enclave |
| CN109700696A (en) * | 2019-01-29 | 2019-05-03 | 江苏格创生物科技有限公司 | A kind of freckle removing and whitening anti-ageing cream and preparation method thereof |
| CN114709031A (en) * | 2022-04-25 | 2022-07-05 | 重庆科宝电缆股份有限公司 | Magnesium oxide powder feeding hopper and copper pipe copper sheath magnesium oxide insulated cable filling method |
| CN114709032A (en) * | 2022-04-25 | 2022-07-05 | 重庆科宝电缆股份有限公司 | Filling method of magnesium oxide drainage tube and magnesium oxide insulation fireproof cable |
| CN115364004A (en) * | 2021-10-19 | 2022-11-22 | 广州一一生物技术有限公司 | Vitamin composition for whitening, moisturizing and controlling oil and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1620446A (en) * | 2002-12-18 | 2005-05-25 | 高丽雅娜化妆品股份有限公司 | Retinol derivatives and cosmestics composition containing the same |
| CN1671353A (en) * | 2002-07-24 | 2005-09-21 | 巴斯福股份公司 | Retinoid-containing preparations |
| CN1762324A (en) * | 2004-10-22 | 2006-04-26 | 卢藏田 | Composite whitening speckle-removing rehabilitation cosmetic |
| CN101181198A (en) * | 2007-12-06 | 2008-05-21 | 曹月秀 | Nourishing type spot-eliminating and beautifying cream |
| CN101317815A (en) * | 2008-05-23 | 2008-12-10 | 海南京润珍珠生物技术股份有限公司 | Spot-removing cream containing pearl hydrolysate liposome |
| CN102008729A (en) * | 2005-01-07 | 2011-04-13 | 日本乐敦制药株式会社 | Composition for external use |
| CN102440943A (en) * | 2011-08-25 | 2012-05-09 | 唯美度科技（北京）有限公司 | Composition for caring and improving aged or damaged skin |
-
2013
- 2013-08-05 CN CN201310338208.XA patent/CN103417433B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1671353A (en) * | 2002-07-24 | 2005-09-21 | 巴斯福股份公司 | Retinoid-containing preparations |
| CN1620446A (en) * | 2002-12-18 | 2005-05-25 | 高丽雅娜化妆品股份有限公司 | Retinol derivatives and cosmestics composition containing the same |
| CN1762324A (en) * | 2004-10-22 | 2006-04-26 | 卢藏田 | Composite whitening speckle-removing rehabilitation cosmetic |
| CN102008729A (en) * | 2005-01-07 | 2011-04-13 | 日本乐敦制药株式会社 | Composition for external use |
| CN101181198A (en) * | 2007-12-06 | 2008-05-21 | 曹月秀 | Nourishing type spot-eliminating and beautifying cream |
| CN101317815A (en) * | 2008-05-23 | 2008-12-10 | 海南京润珍珠生物技术股份有限公司 | Spot-removing cream containing pearl hydrolysate liposome |
| CN102440943A (en) * | 2011-08-25 | 2012-05-09 | 唯美度科技（北京）有限公司 | Composition for caring and improving aged or damaged skin |
Non-Patent Citations (6)
| Title |
|---|
| 佚名: "美白祛斑霜", 《日用化学品科学》 * |
| 杨艳伟，等: "化妆品中常用的美白祛斑成分及其检测方法研究进展", 《环境与健康杂志》 * |
| 林春梅，等: "美白化妆品原料的开发及其祛斑美白机制", 《职业与健康》 * |
| 武玉峰，等: "美白配方", 《日用化学品科学》 * |
| 蒋旭红: "化妆品中的超微载体", 《日用化学工业》 * |
| 谢惠英，等: "几种植物提取物在化妆品中的应用现状", 《香料香精化妆品》 * |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105947953A (en) * | 2016-06-30 | 2016-09-21 | 东莞轩朗实业有限公司 | Production device for quantum dot light bar |
| CN106265338A (en) * | 2016-09-14 | 2017-01-04 | 广东丸美生物技术股份有限公司 | A kind of skin care oil and preparation method that there is Whitening, spot and purify smooth skin |
| CN106265338B (en) * | 2016-09-14 | 2020-02-14 | 广东丸美生物技术股份有限公司 | Skin care oil with whitening, spot-fading and skin-smoothing functions and preparation method thereof |
| CN108210362A (en) * | 2016-12-14 | 2018-06-29 | 天津强微特生物科技有限公司 | A kind of VACE Essences of freckle removing and whitening |
| CN106821794A (en) * | 2017-01-11 | 2017-06-13 | 杭州菲丝凯化妆品有限公司 | Eye bottoming cream and preparation method thereof |
| CN108888522A (en) * | 2018-07-24 | 2018-11-27 | 上海东晟源日化有限公司 | A kind of skin care liposomes inclusion enclave |
| CN109700696A (en) * | 2019-01-29 | 2019-05-03 | 江苏格创生物科技有限公司 | A kind of freckle removing and whitening anti-ageing cream and preparation method thereof |
| CN115364004A (en) * | 2021-10-19 | 2022-11-22 | 广州一一生物技术有限公司 | Vitamin composition for whitening, moisturizing and controlling oil and preparation method thereof |
| CN114709031A (en) * | 2022-04-25 | 2022-07-05 | 重庆科宝电缆股份有限公司 | Magnesium oxide powder feeding hopper and copper pipe copper sheath magnesium oxide insulated cable filling method |
| CN114709032A (en) * | 2022-04-25 | 2022-07-05 | 重庆科宝电缆股份有限公司 | Filling method of magnesium oxide drainage tube and magnesium oxide insulation fireproof cable |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103417433B (en) | 2015-04-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103417433B (en) | Whitening and freckle-removing cream with whitening and freckle-removing functions, production technology of cream, and nitrogen filling machine | |
| CN101849894B (en) | CO2 sustained release foam mask and preparation method thereof | |
| JP3186879U (en) | Carbonated pack | |
| CN107920962A (en) | The Clean- fater disintegration type graininess ball composition of hair | |
| CN104254312A (en) | Kit containing two separate compositions, in particular for cosmetic application | |
| CN102300542A (en) | Container For Pharmaceutical Use For The Quantitative Release Of A Single Dose For Oral Administration Of T3 And T4 Thyroid Hormones In Solution | |
| CN103655394A (en) | Radix lithospermi mask | |
| CN108289838A (en) | Flushing-free chemical foam containing bent Fa Luoting and their purposes in treating ichthyosis | |
| CN109843271A (en) | Low cross-linking gelatin | |
| CN106675855A (en) | Enzyme fancy soap and preparation method thereof | |
| JP6142343B2 (en) | One-part skin external preparation | |
| CN107702469A (en) | A kind of drying milling device for being used to prepare Phallus impudicus extract solution | |
| JP2013227270A (en) | Foamable skin care preparation | |
| JP4561952B2 (en) | Water discharge device | |
| JP6987374B2 (en) | Effervescent skin external application | |
| KR20140120648A (en) | Cosmetics composition comprising donkey milk and method of fabricating thereof | |
| JP2004267627A (en) | Spouting cylinder | |
| JP6851646B2 (en) | Kit for external preparations for skin | |
| CN104855636A (en) | Black tea extract and oral solid instant preparation thereof | |
| DK3119478T3 (en) | Anhydride consumable device for improvised preparation of a single dose cosmetic composition | |
| CN103845448A (en) | Spot-removing and beautifying granule | |
| CN107472710A (en) | A kind of combined type medicinal liquor bottle | |
| CN101612150A (en) | Isoconeazole nitrate vagina soft capsule and preparation method thereof | |
| JP6628197B2 (en) | Skin preparation kit | |
| CN207390026U (en) | A kind of combined type medicinal liquor bottle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171121 Address after: Hangzhou City, Zhejiang Province, 311231 block of South Xiaoshan economic and Technological Development Zone Chunchao Road No. 93 Patentee after: Yu Xingjun Address before: Hangzhou City, Zhejiang Province, the 311231 Xiaoshan economic and Technological Development Zone, Road No. 93 Patentee before: ARROW-BIO BIOTECHNOLOGY (HANGZHOU) Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171205 Address after: 310000 Sunshine Road No. 688, Chunan County, Chunan County, Hangzhou, 103-4 Patentee after: Only treasure Ltd. Address before: Hangzhou City, Zhejiang Province, 311231 block of South Xiaoshan economic and Technological Development Zone Chunchao Road No. 93 Patentee before: Yu Xingjun |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180521 Address after: 311215 spring tide road 93, Qiao Nan block, Xiaoshan economic and Technological Development Zone, Hangzhou, Zhejiang Patentee after: ARROW-BIO BIOTECHNOLOGY (HANGZHOU) Co.,Ltd. Address before: 310000 No. 688 Sunshine Road, Thousand Island Lake Town, Chunan County, Hangzhou, Zhejiang, 103-4 Patentee before: Only treasure Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190814 Address after: 313000 First Floor, Building 6, Meichang Kechuang Center, 1616 Pioneer Road, Dixi Town, Wuxing District, Huzhou City, Zhejiang Province Patentee after: Zhejiang Yalu Biotechnology Co.,Ltd. Address before: 311215 No. 93 Chunchao Road, Qiaonan District, Xiaoshan Economic and Technological Development Zone, Hangzhou City, Zhejiang Province Patentee before: ARROW-BIO BIOTECHNOLOGY (HANGZHOU) Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200529 Address after: 311200 floor 5, building 2, ChuanHua Kechuang building, ningwei street, Xiaoshan District, Hangzhou City, Zhejiang Province Patentee after: Zhejiang Laizhen Biotechnology Co.,Ltd. Address before: 313000 First Floor, Building 6, Meichang Kechuang Center, 1616 Pioneer Road, Dixi Town, Wuxing District, Huzhou City, Zhejiang Province Patentee before: Zhejiang Yalu Biotechnology Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20210910 Address after: 361001 unit 1229, Robinson summit, No. 885, Xiahe Road, Siming District, Xiamen City, Fujian Province Patentee after: Yiqilai (Xiamen) Cosmetics Co.,Ltd. Address before: 5 / F, building 2, ChuanHua science and technology building, ningwei street, Xiaoshan District, Hangzhou City, Zhejiang Province, 311200 Patentee before: Zhejiang Laizhen Biotechnology Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150422 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |