CN103407215B - Electrostatic flocking fabric made of alginate fiber and preparation method of electrostatic flocking fabric - Google Patents
Electrostatic flocking fabric made of alginate fiber and preparation method of electrostatic flocking fabric Download PDFInfo
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- CN103407215B CN103407215B CN201310378355.XA CN201310378355A CN103407215B CN 103407215 B CN103407215 B CN 103407215B CN 201310378355 A CN201310378355 A CN 201310378355A CN 103407215 B CN103407215 B CN 103407215B
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Abstract
The invention discloses electrostatic flocking fabric made of alginate fiber. The electrostatic flocking fabric comprises a flock layer, an adhesive layer and a base cloth layer, and is characterized in that the flock layer is the alginate fiber; the base cloth layer is aramid plain woven cloth; the middle adhesive layer is an organic silicon modified epoxy resin adhesive. The invention also discloses a preparation method of the electrostatic flocking fabric made of the alginate fiber. The preparation method is characterized by comprising the following steps of cutting alginate fiber strands into alginate fiber flock, and performing electric conduction and coloring treatment; pre-coating and mainly coating adhesives on flocking base cloth, wherein the total thickness of the adhesives is 0.2 to 0.25mm; performing flocking in an electrostatic flocking room to obtain flocked cloth; and performing baking to firmly composite the flock with the base cloth so as to obtain the electrostatic flocking fabric. The electrostatic flocking fabric has good flame resistance and is applicable to army combat uniforms, warship and submarine combat uniforms, bedding equipment, airman training combat uniforms, second artillery training combat uniforms and the like.
Description
Technical field
The present invention relates to a kind of electrostatic flocking fabric and manufacture method thereof, particularly relate to a kind of extraordinary military alginate fibre electrostatic flocking fabric and manufacture method thereof.。
Background technology
Flocked fiber used is at present mostly fibers material, and with less as flocked material of natural fiber, environmental-protecting performance is poor, easily in manufacturing process and later stage use procedure, produces environmental pollution.Alginate fibre has far infrared, anion, antibacterial, deodorization, fire-retardant excellent specific property, and there is excellent high-hydroscopicity, ease of removal, plastic is obstructive, biocompatibility, degradable absorbability and environmental-protecting performance, it is tencel the most excellent in recent years, military natural fire-retardant for special type, radiation proof, far infrared, do extraordinary military excellent selection, therefore need to develop a kind of extraordinary military alginate fibre electrostatic flocking fabric, can be applicable to fight of army clothes, warship Submarine Combat clothes and bed necessaries equipment, air arm does to instruct fighting uniform, Second Artillery Force makes instruction fighting uniform etc.
Summary of the invention
The extraordinary military alginate fibre electrostatic flocking fabric of flame retardant type that the object of this invention is to provide a kind of natural environmental-protective with and preparation method thereof.
In order to solve the problem, the technical solution used in the present invention is:
A kind of alginate fibre electrostatic flocking fabric, comprise tapetum, adhesive phase and bottom cloth layer, described tapetum is alginate fibre, and base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, and intermediary adhesive layer is modifying epoxy resin by organosilicon glue.
Described tapetum is the blend fibre of one or more in alginate fibre and viscose glue, cotton, chemical fibre.
Described base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, base fabric fabric density 108 × 58, and fineness of yarn is 16tex.
The technical indicator of alginate fibre electrostatic flocking fabric: fire resistance reaches A level requirement in GB 8965 flame-resistant garment-flame protection; Environmental-protecting performance reaches I class and II class index request in HJ/T 307-2006; Critical radiant flux: NEPA 253; Electrostatic propensity is tested: AATCC 134; Antistatic property: ISO6356.
The manufacture method of above-mentioned a kind of alginate fibre electrostatic flocking fabric, is characterized in that comprising the steps:
A, by alginate fibre tow through cutting, making length is 1.0-1.2 millimeter, and fineness is the alginate fibre fine hair at 1.5 dawn, carries out conductive processing to fine hair afterwards, and carries out coloring treatment as required, then fine hair is dry, screening;
B, coating adhesive that base fabric aramid fiber plain weaving machine weaved cotton cloth, adhesive divides two-layer, and first precoating carries out main painting again after preliminary drying, and adhesive gross thickness is 0.2-0.25 millimeter;
C, indoor at electrostatic spinning, adopt high-voltage alternating electrostatic to produce electric field flocking, the base fabric surface making fine hair neatly implant under the effect of electric field force in high-voltage alternating electrostatic field to scribble adhesive;
D, the base fabric that step c is obtained, the cylinder decorative pattern utilizing pressure-air to pass through to cover on air knife periphery at following fan parameter carries out air cotton ginning at matte, fan pressure 42-44Pa, cylinder rotating speed 12-14rpm, rotation speed of fan 35-38rpm, carry out when speed of a motor vehicle 10m/min, become the electrostatic flocking fabric of band special air cotton ginning decorative pattern;
E, fabric step c or steps d obtained, utilize the anti-processing method of foaming type three to carry out three anti-process.
Below the further improvement to technique scheme:
In step a, fine hair moisture control is at 8%-10%, and ratio resistance controls 3.6 × 10
8-3.6 × 10
9Ω ㎝.
Step c mesohigh electrode network is for exchanging electrostatic, and electrostatic high-pressure controls as 20-22kv, and the distance between one side high voltage electrode net and base fabric scribbling adhesive is 15-20 centimetre.
In step b, adhesive is modifying epoxy resin by organosilicon glue, and preliminary drying temperature is 80-90 DEG C and raises successively, and preliminary drying time is 1-1.5min; Main baking temperature is 110-140 DEG C and raises successively, and the main baking time is 3-4min.
Foaming machine is utilized three-proof finishing agent to be carried out foaming process in step e, blowing agent is fluorocarbon polymer finishing agent, web surface is coated onto by the mode of blade coating, then drying and processing is carried out, the equipment speed of service is 10m/min, bake out temperature is 130-150 DEG C and raises successively, and drying time is 4-5 minute.
The invention has the beneficial effects as follows: because alginate fibre price is higher, utilizing electrostatic flocking technology to make alginate fibre electrostatic flocking fabric is distributed in alginate fibre on fabric significant surface, not only give full play to the uniqueness of alginate fibre but also excellent quality heterosis, and can effectively reduce alginate fibre cost compared with the alginate fiber fabric of same grammes per square metre.
The combination of alginate fibre, modifying epoxy resin by organosilicon glue and aramid fiber base fabric, making fabric have the features such as outstanding fire-retardant, environmental protection, natural antibacterial, far infrared, radiation proof, high strength, acid and alkali-resistance, life cycle are long, is the excellent textile of extraordinary function.Alginate fibre has the excellent specific property of fire-retardant, far infrared, anion, antibacterial, deodorization, and have that excellent high-hydroscopicity, ease of removal, plastic are obstructive, biocompatibility, degradable absorbability and environmental-protecting performance, be tencel the most excellent in recent years; The premium properties such as aramid fiber has superhigh intensity, high-modulus and high temperature resistant, acid-fast alkali-proof, lightweight, insulation, anti-aging, life cycle is long; Modifying epoxy resin by organosilicon glue has good resistance to elevated temperatures, the flocked fabric using this adhesive obtained is formaldehydeless, good flame resistance, environmental protection, and fastness is high, and fabric wearability is good.Therefore this alginate fibre electrostatic flocking fabric is applicable to fight of army clothes, warship Submarine Combat clothes and bed necessaries equipment, air arm makes instruction fighting uniform, Second Artillery Force makes instruction fighting uniform etc., and DEVELOPMENT PROSPECT is wide, economic benefit and social benefit good.
detailed description of the invention:
embodiment 1
A kind of alginate fibre electrostatic flocking fabric, comprise tapetum, adhesive phase and bottom cloth layer, described tapetum is alginate fibre, and base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, and intermediary adhesive layer is modifying epoxy resin by organosilicon glue.Wherein:
Described tapetum is the blend fibre of one or more in alginate fibre and viscose glue, cotton, chemical fibre.
Described base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, base fabric fabric density 108 × 58, and fineness of yarn is 16tex.
The fire resistance of described alginate fibre electrostatic flocking fabric reaches A level requirement in GB 8965 flame-resistant garment-flame protection.
The manufacture method of above-mentioned alginate fibre electrostatic flocking fabric, comprises the steps:
A, by alginate fibre tow through cutting, making length is 1.0 millimeters, and fineness is the alginate fibre fine hair at 1.5 dawn, afterwards conductive processing and coloring treatment are carried out to fine hair, then fine hair is dry, screening, control fine hair moisture content 8%, ratio resistance controls 3.6 × 10
8Ω ㎝.
B, by the base fabric first precoating layer adhesive of blade coating mode, blade surface is close to base fabric surface, then preliminary drying, temperature 80-90 DEG C raises successively, and drying time is 1min, through the not only surfacing of the pre-baked base fabric of precoating, seamless, be beneficial to the attractive in appearance of final flocked fabric cloth cover, and after precoating preliminary drying, be more conducive to the combination between adhesive and base fabric, make adhesives fastness higher; After main painting layer of adhesive again, main baking temperature is 110-140 DEG C and raises successively, and the main baking time is 3min, and adhesive gross thickness is 0.2 millimeter.
C, indoor at electrostatic spinning, adopt high-voltage alternating electrostatic to produce electric field flocking, the base fabric surface making fine hair neatly implant under the effect of electric field force in high-voltage alternating electrostatic field to scribble adhesive.High voltage electrode net is for exchanging electrostatic, and electrostatic high-pressure controls as 20kv, and the distance between one side high voltage electrode net and base fabric scribbling adhesive is 15 centimetres.
D, the flocked fabric obtained by step c, through baking, make fine hair and the firm compound of base fabric.
E, utilize foaming machine that flocked fabric obtained to steps d for three-proof finishing agent is carried out foaming to process, blowing agent is the fluorocarbon polymer finishing agent that Shandong Ling Chao new material Co., Ltd produces, web surface is coated onto by the mode of blade coating, then drying and processing is carried out, the equipment speed of service is 10m/min, bake out temperature is 130-150 DEG C and raises successively, and drying time is 4 minutes, becomes the static flocking cloth without decorative pattern.
Embodiment 2:
A kind of alginate fibre electrostatic flocking fabric, comprise tapetum, adhesive phase and bottom cloth layer, described tapetum is alginate fibre, and base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, and intermediary adhesive layer is modifying epoxy resin by organosilicon glue.Wherein:
Described tapetum is the blend fibre of one or more in alginate fibre and viscose glue, cotton, chemical fibre.
Described base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, base fabric fabric density 108 × 58, and fineness of yarn is 16tex.
The fire resistance of described alginate fibre electrostatic flocking fabric reaches A level requirement in GB 8965 flame-resistant garment-flame protection.
The manufacture method of above-mentioned alginate fibre electrostatic flocking fabric, comprises the steps:
A, by alginate fibre tow through cutting, making length is 1.2 millimeters, and fineness is the alginate fibre fine hair at 1.5 dawn, afterwards conductive processing and coloring treatment are carried out to fine hair, then fine hair is dry, screening, control fine hair moisture content 10%, ratio resistance controls 3.6 × 10
9Ω ㎝.
B, flocking base fabric adopt aramid fiber plain weaving machine to weave cotton cloth, the modifying epoxy resin by organosilicon glue that adhesive adopts Shandong Ling Chao new material Co., Ltd to produce, modifying epoxy resin by organosilicon glue has good resistance to elevated temperatures, the flocked fabric using this adhesive obtained is formaldehydeless, good flame resistance, environmental protection, and fastness is high, fabric wearability is good.
By the base fabric first precoating layer adhesive of blade coating mode, blade surface is close to base fabric surface, then preliminary drying, temperature 80-90 DEG C raises successively, and drying time is 1.5min, through the not only surfacing of the pre-baked base fabric of precoating, seamless, be beneficial to the attractive in appearance of final flocked fabric cloth cover, and after precoating preliminary drying, be more conducive to the combination between adhesive and base fabric, make adhesives fastness higher; After main painting layer of adhesive again, main baking temperature is 110-140 DEG C and raises successively, and the main baking time is 4min, and adhesive gross thickness is 0.25 millimeter;
C, indoor at electrostatic spinning, adopt high-voltage alternating electrostatic to produce electric field flocking, the base fabric surface making fine hair neatly implant under the effect of electric field force in high-voltage alternating electrostatic field to scribble adhesive.High voltage electrode net is for exchanging electrostatic, and electrostatic high-pressure controls as 22kv, and the distance between one side high voltage electrode net and base fabric scribbling adhesive is 20 centimetres.
D, the flocked fabric obtained by step c, through baking, make fine hair and the firm compound of base fabric.
E, utilize foaming machine that flocked fabric obtained to steps d for three-proof finishing agent is carried out foaming to process, blowing agent is the fluorocarbon polymer finishing agent that Shandong Ling Chao new material Co., Ltd produces, web surface is coated onto by the mode of blade coating, then drying and processing is carried out, the equipment speed of service is 10m/min, bake out temperature is 130-150 DEG C and raises successively, and drying time is 5 minutes, becomes the static flocking cloth without decorative pattern.
Embodiment 3:
A kind of alginate fibre electrostatic flocking fabric, comprise tapetum, adhesive phase and bottom cloth layer, described tapetum is alginate fibre, and base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, and intermediary adhesive layer is modifying epoxy resin by organosilicon glue.Wherein:
Described tapetum is the blend fibre of one or more in alginate fibre and viscose glue, cotton, chemical fibre.
Described base fabric is that aramid fiber plain weaving machine is weaved cotton cloth, base fabric fabric density 108 × 58, and fineness of yarn is 16tex.
The fire resistance of described alginate fibre electrostatic flocking fabric reaches A level requirement in GB 8965 flame-resistant garment-flame protection.
The manufacture method of above-mentioned alginate fibre electrostatic flocking fabric, comprises the steps:
A, by alginate fibre tow through cutting, making length is 1.0 millimeters, and fineness is the alginate fibre fine hair at 1.5 dawn, carries out conductive processing and coloring treatment to fine hair afterwards, then fine hair is dry, screening.Control fine hair moisture content 8%, ratio resistance controls 3.6 × 10
8Ω ㎝.
B, by the base fabric first precoating layer adhesive of blade coating mode, blade surface is close to base fabric surface, then preliminary drying, temperature 80-90 DEG C raises successively, and drying time is 1min, through the not only surfacing of the pre-baked base fabric of precoating, seamless, be beneficial to the attractive in appearance of final flocked fabric cloth cover, and after precoating preliminary drying, be more conducive to the combination between adhesive and base fabric, make adhesives fastness higher; After main painting layer of adhesive again, main baking temperature is 110-140 DEG C and raises successively, and the main baking time is 3min, and adhesive gross thickness is 0.2 millimeter.
C, indoor at electrostatic spinning, adopt high-voltage alternating electrostatic to produce electric field flocking, the base fabric surface making fine hair neatly implant under the effect of electric field force in high-voltage alternating electrostatic field to scribble adhesive.High voltage electrode net is for exchanging electrostatic, and electrostatic high-pressure controls as 20kv, and the distance between one side high voltage electrode net and base fabric scribbling adhesive is 15 centimetres.
D, the flocked fabric that step c is obtained, the cylinder decorative pattern utilizing pressure-air to pass through to cover on air knife periphery at following fan parameter carries out air cotton ginning at matte, fan pressure 42-44Pa, cylinder rotating speed 12-14rpm, rotation speed of fan 35-38rpm, carry out when speed of a motor vehicle 10m/min, become the electrostatic flocking fabric of band special air cotton ginning decorative pattern.
E, utilize foaming machine that flocked fabric obtained to steps d for three-proof finishing agent is carried out foaming to process, blowing agent is the fluorocarbon polymer finishing agent that Shandong Ling Chao new material Co., Ltd produces, web surface is coated onto by the mode of blade coating, then drying and processing is carried out, the equipment speed of service is 10m/min, bake out temperature is 130-150 DEG C and raises successively, and drying time is 4-5 minute, the electrostatic flocking fabric of obtained band special air cotton ginning decorative pattern.
The alginate fibre electrostatic flocking fabric that Example 1,2,3 is obtained is respectively tested, and technical indicator is as follows:
Flame-retarding characteristic: reach A level requirement in GB 8965 flame-resistant garment-flame protection
Environmental protection test: reach I class and II class index request in HJ/T 307-2006
Color fastness to light: AATCC 4 grades
Fastness to rubbing: AATCC 165 dry grinds 4-5 level; Wet-milling 4-5 level
Flocking fastness: GB/21196.1 >=75000
Change in size and appearance after laundering: get three pieces of samples with entering test, perform by GB/8628, GB/T8629, GB/T8630 standard, select 5A program, always feed 2Kg, drying means F, and baking temperature is no more than 40 DEG C, averages.Rank reaches Pyatyi.
Critical radiant flux: NEPA 253
Electrostatic propensity is tested: AATCC 134
Antistatic property: ISO6356
Antibiotic property: AATCC 100
As can be seen from above technical indicator, obtained its key technical indexes of alginate fibre electrostatic flocking fabric reaches I class and II class index request in People's Republic of China (PRC) environmental protection professional standard HJ/T 307-2006, and flame-retarding characteristic reaches GB 8965 flame-resistant garment
-a level requirement in flame protection, as the military electrostatic spinning product of special type, can make instruction fighting uniform, Second Artillery Force's work instruction fighting uniform etc. for fight of army clothes, warship Submarine Combat clothes and bed necessaries equipment, air arm.
The present invention is not limited to above-mentioned embodiment; every pure alginate fibre or blending alginate fibre; as alginate fibre and viscose glue, alginate fibre and cotton, alginate fibre and chemical fibre etc., to be adjusted accordingly in electric treatment, the selection of fine hair pigment, backing material selection, adhesive allotment, electric-field intensity control etc. and obtained electrostatic spinning product all falls within protection scope of the present invention as long as at fine hair.
Claims (8)
1. an alginate fibre electrostatic flocking fabric, comprises tapetum, adhesive phase and bottom cloth layer, it is characterized in that: described tapetum is alginate fibre, and bottom cloth layer is that aramid fiber plain weaving machine is weaved cotton cloth, and adhesive phase is modifying epoxy resin by organosilicon glue;
The manufacture method of described alginate fibre electrostatic flocking fabric, comprises the steps:
A, by alginate fibre tow through cutting, making length is 1.0-1.2 millimeter, and fineness is the alginate fibre fine hair at 1.5 dawn, carries out conductive processing to fine hair and carries out coloring treatment as required afterwards, then fine hair is dry, screening;
B, coating adhesive that bottom cloth layer aramid fiber plain weaving machine weaved cotton cloth, adhesive divides two-layer, first precoating, after preliminary drying, carry out main painting again, and adhesive gross thickness is 0.2-0.25 millimeter;
C, indoor at electrostatic spinning, adopt high-voltage alternating electrostatic to produce electric field flocking, the bottom cloth layer surface making fine hair neatly implant under the effect of electric field force in high-voltage alternating electrostatic field to scribble adhesive;
D, the bottom cloth layer that step c is obtained, the cylinder decorative pattern utilizing pressure-air to pass through to cover on air knife periphery carries out air cotton ginning at matte, fan pressure 42-44Pa, at cylinder rotating speed 12-14rpm, rotation speed of fan 35-38rpm, carry out when speed of a motor vehicle 10m/min, the electrostatic flocking fabric of obtained band special air cotton ginning decorative pattern;
E, electrostatic flocking fabric steps d obtained, utilize the anti-processing method of foaming type three to carry out three anti-process.
2. a kind of alginate fibre electrostatic flocking fabric according to claim 1, is characterized in that: described tapetum is the blend fibre of alginate fibre and cotton fiber or chemical fibre.
3. a kind of alginate fibre electrostatic flocking fabric according to claim 1, is characterized in that: described bottom cloth layer is that aramid fiber plain weaving machine is weaved cotton cloth, bottom cloth layer fabric density 108 × 58, and fineness of yarn is 16tex.
4. a kind of alginate fibre electrostatic flocking fabric according to claim 1, is characterized in that: the technical indicator of alginate fibre electrostatic flocking fabric: fire resistance reaches A level requirement in GB 8965 flame-resistant garment-flame protection; Environmental-protecting performance reaches I class and II class index request in HJ/T 307-2006; Critical radiant flux: NEPA 253; Electrostatic propensity is tested: AATCC 134; Antistatic property: ISO6356.
5. a kind of alginate fibre electrostatic flocking fabric according to claim 1, is characterized in that: in step a, fine hair moisture control is at 8%-10%, and ratio resistance controls 3.6 × 10
8-3.6 × 10
9Ω ㎝.
6. a kind of alginate fibre electrostatic flocking fabric according to claim 1, it is characterized in that: it is high voltage electrode net that step c mesohigh exchanges electrostatic field, high-voltage alternating Electrostatic Control is 20-22kv, and the distance between the one side described high voltage electrode net and bottom cloth layer scribbling adhesive is 15-20 centimetre.
7. a kind of alginate fibre electrostatic flocking fabric according to claim 1, it is characterized in that: in step b, adhesive is modifying epoxy resin by organosilicon glue, preliminary drying temperature is 80-90 DEG C, and preliminary drying time is 1-1.5min.
8. a kind of alginate fibre electrostatic flocking fabric according to claim 1, it is characterized in that: in step e, utilize foaming machine three-proof finishing agent to be carried out foaming process, blowing agent is fluorocarbon polymer finishing agent, web surface is coated onto by the mode of blade coating, then drying and processing is carried out, the equipment speed of service is 10m/min, and bake out temperature is 130-150 DEG C, and drying time is 4-5 minute.
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| CN103660406B (en) * | 2014-01-15 | 2014-09-10 | 绍兴县恒兆纺织有限公司 | Colorful flocked fabric and preparation method thereof |
| CN107415359B (en) * | 2017-06-09 | 2019-10-11 | 山东领潮新材料有限公司 | Nanoscale heat-insulating noise-reducing tank interior composite material and preparation method thereof |
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| CN109281191A (en) * | 2018-09-06 | 2019-01-29 | 山东领潮新材料有限公司 | A kind of heat-resistant fireproof electrostatic flocking fabric and preparation method thereof |
| CN109225769B (en) * | 2018-09-06 | 2021-07-06 | 山东领潮新材料有限公司 | Multi-electric-field electrostatic flocking method and equipment |
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| CN110331518A (en) * | 2019-07-31 | 2019-10-15 | 太仓市梓怡纺织有限公司 | The production technology of seaweed aryl fiber cloth |
| CN111118917B (en) * | 2019-12-30 | 2022-04-01 | 苏州大学 | Real silk flocking material and preparation method and application thereof |
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| JP3197943B2 (en) * | 1992-04-30 | 2001-08-13 | エステー化学株式会社 | Brushed product made of natural rubber and method for producing the same |
| US5320890A (en) * | 1993-06-23 | 1994-06-14 | E. I. Du Pont De Nemours And Company | Fire resistant fabrics with a flocked nylon surface |
| CN201541787U (en) * | 2009-10-29 | 2010-08-11 | 公安部上海消防研究所 | Heat insulation protective clothing fabric for firemen |
| CN102505270A (en) * | 2011-10-31 | 2012-06-20 | 淄博奈琦尔纺织科技发展有限公司 | Seaweed fiber blending flame-retardant garment plus material and production method |
| CN202428739U (en) * | 2012-01-09 | 2012-09-12 | 上海伊贝纳纺织品有限公司 | Composite fabric formed by aramid fiber, modacrylic fiber and thermoplastic polyurethane |
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