CN103404542A - Method for preparing field snake-expelling special-effect spray - Google Patents
Method for preparing field snake-expelling special-effect spray Download PDFInfo
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- CN103404542A CN103404542A CN2013103921901A CN201310392190A CN103404542A CN 103404542 A CN103404542 A CN 103404542A CN 2013103921901 A CN2013103921901 A CN 2013103921901A CN 201310392190 A CN201310392190 A CN 201310392190A CN 103404542 A CN103404542 A CN 103404542A
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Abstract
The invention discloses a method for preparing a field snake-expelling special-effect spray. The method comprises the following steps of: drying and smashing dried milkweed, dried celery seed, dried garlic, dried tobacco, dried bean thermopsis, dried rhizoma atractylodis, dried Chinese lobelia, dried dutchmanspipe root, dried paris polyphylla and dried angelica root until the granularity is 100 meshes, mixing, putting the mixture into extraction equipment, extracting composite snake-expelling volatile oil by adopting a supercritical CO2 fluid extraction technology, adding auxiliary materials such as ethyl alcohol into the extracted composite snake-expelling volatile oil to obtain a snake-expelling liquid spray, putting the snake-expelling liquid spray into a full-automatic liquid spray filling production line, and filling to obtain the bottled field snake-expelling special-effect spray. According to the invention, various plants which can be used for insect killing are adopted as the raw materials; different snakes are especially sensitive to different types of flavor components, and therefore, the composite snake-expelling volatile oil prepared by adopting the method disclosed by the invention has good expelling effect on different snakes. According to the method, the snake-expelling liquid spray is prepared into bottled spray and is convenient to carry in the field. The method disclosed by the invention is suitable for preparing environmentally-friendly snake-expelling medicaments.
Description
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Technical field
The present invention relates to a kind of field and drive the preparation method of snake special efficacy spray, belong to and drive antidote for snakebite thing technical field.
Background technology
The most basic purpose of " outdoor exercises " is exactly: back to nature, take exercises, purify one's soul, discharge the oneself, as long as you walk out door, just cry outdoor, outdoor motion is namely gone in outdoor exercises, be a motion of walking at any time, and a such fitness campaign is very family-friendly naturally!
The anti-snake of outdoor exercises is essential, and the most serious area of venomous snake bite is South America, South Asia and Southeast Asian countries.It is reported the hundreds of thousands of them is approximately arranged in the world by venomous snake bite every year.India is at the snakebite total number of persons of nineteen sixty-eight up to 300,000～400,000 people, and dead just have a people more than 30,000.Equally, in the South Asian Subcontinent and China, a considerable amount of snakebite patients are also arranged, the visible harm of venomous snake bite in these areas is very serious.In addition, the poisonous snake in pasture, grassland (particularly early spring) often damages drove, such as the pallas pit viper of Xinjiang of China Ili Prefecture, the poisonous snakes such as extremely northern viper of Kui He Altay Prefecture, grassland, all endangers the person poultry safety.Past, because of the lethal horses of snake evil, accounts for 20% of total death toll.
Field exploration, field survivorship, just more and more become the outdoor activity project that liked by the modern.The mankind also come out of from natural world although it should be noted that, the modern is too of a specified duration away from wild environment, more and more rely on artificial environment existence.While in entering natural environment, carrying out exploring, the problem how can survive safely in this environment just displays.
Outdoor exercises, field work, prevent snake to sting, and the area that vegetation is flouring at first in the wild, the visual field is not good, easily conceal animal, had better not go to pass through or trample, and keeps someone at a respectful distance; In addition, go back the mechanics of GPRS poisonous snake, snake reaches more than 18 ℃ just out movable at temperature usually, particularly when sultry wish rain or Harbeth, so before summer rain, after rain, flood will pay special attention to anti-snake in the time later.
China's effective way that the anti-snake of many methods is arranged among the people, prevent snake etc. if with realgar and sulphur, made various formulas.Certain methods among the people is often effective for a certain snake, but may be invalid to the snake of other kind.
Summary of the invention
Purpose of the present invention, in order to seek a kind ofly to various snakes, can to play and effectively drive and prevention effect, a kind of antidote for snakebite agent of driving easy to use again simultaneously, the present invention discloses the preparation method that snake special efficacy spray is driven in a kind of field.
Realize that technical scheme of the present invention is, the present invention, by various plants insecticide raw material drying and crushing after formula, makes combination flooding snake volatile oil, then itself and other auxiliary material formula is made and is driven snake liquid spray, then undertaken filling by filling production lines.
Preparation method's step that the present invention drives in a kind of field snake special efficacy spray is as follows:
(1) following composition raw material is got all the ready by formula, and crushed after being dried to 100 order: 1 part of dry milkweed, 1 part of dry celery seed, 1 part of dry Garlic Seeds, 1 part of dry tobacco, dry snake exterminate a family 1 part of 1 part, 1 part of dry rhizoma atractylodis, 1 part of dry Chinese lobelia, 1 part of dry dutchmanspipe root, 1 part of dry paris polyphylla and the extra dry white wine root of Dahurian angelica;
(2) the plant insecticide raw material after above-mentioned pulverizing is dropped into to extraction equipment, adopt supercritical CO
2Fluid extraction technology extracts into combination flooding snake volatile oil;
By experiment of single factor and orthogonal experiment, obtain the relevant technical parameter of overcritical each extraction: extracting pressure 27 MPas, extraction CO
2Flow is 53～58 kg/hours, extraction time 5 hours, and 52 ℃ of extraction temperature, 70% ethanol is made entrainer;
(3) in mass ratio 15.3%～15.5%, get the combination flooding snake volatile oil of extraction; The ethanol that adds mass ratio 80%; The citric acid that adds mass ratio 0.1%～0.3%, regulate pH value to 6.5 consumption; And to add mass ratio be that 3% organic silicon adhesive, mass ratio are that 0.1% isoamyl acetate, mass ratio are that 0.3% ethyl hexylate, mass ratio are 1% Tween 80; After mixing, fully stir and make it even; Adjust liquid to ormal weight: 1 milliliter contains 0.153～0.157 gram combination flooding snake volatile oil; Must drive snake liquid spray.
(4) will drive snake liquid spray sends into fully automatic liquid spray filling production lines and carries out filling.
Fully automatic liquid spray filling production lines workflow is as follows:
Empty bottle arranges (the reasonable bottle of equipment belt platform) → wash bottle → bakings bottle → empty bottle and advances filling station → detection and location → filling head decline → filling valve and open → start filling → mass metrology → arrival setting numerical value → filling valve and close → expire and bottle go out filling station → turn to → hang lid → spiral cover → labeling → coding.
Bulking system is comprised of filling valve, control valve, filling head, support, guide rail, pneumatic actuator, control system etc.The bulking system pouring process should be noted:
(1) bulking system precision: the bulking system precision depends primarily on the degree of stability of precision, filling speed and the system of measuring pump.
(2) antidrip filling after, the material that remains in filling head surface wants the regular hour just can flow to end, material will drip to the container appearance and pollutes like this, during this bulking system design, adopt pneumatic stop valve, simple in structure, folding rapidly, easy cleaning, good seal, effectively prevent the water clock problem of filling head in filling batch process.
(3) the filling machine part can realize fine setting.Under different temperatures, the material of different batches, issuable error in dipping, can solve by fine setting.
Principle of the present invention is, the raw material that the present invention selects is the plant insecticide raw material, after their drying and crushing are mixed, obtain combination flooding snake volatile oil through extraction, then driving on the clothing that snake liquid spray is sprayed on the people of adding that auxiliary material make just has and can play the effect of driving.
During use, only need just can be bonded on clothing, shoes and hats, gloves and drive snake, prevent that snake stings toward spraying a little with it; People's audible, the snake dislike; The people does not hinder, and snake is not dead; The insects such as all right anti-mosquito, wasp, have good dispersion effect, accomplishes getting along amiably and peacefully of man and nature.
The invention has the beneficial effects as follows, because adopting the multiple plant that can be used for desinsection, the present invention makes raw material, and different snakes is responsive especially to certain different fragrance matters, combination flooding snake volatile oil prepared by the inventive method all has the good effect of driveing for different snakes, be that it can drive multiple snake, particularly poisonous snake.The inventive method will be driven snake liquid spray and be made spray filling, more convenient go out field outing or the field work of carrying.The material adopted due to the inventive method is all to people's avirulence, and environmentally safe, be a kind of environmentally friendly antidote for snakebite agent of driving.
The inventive method is applicable to make environment-friendly type and drives the antidote for snakebite thing.
The accompanying drawing explanation
Fig. 1 is preparation method's flow chart that snake special efficacy spray is driven in field of the present invention.
Embodiment
Below by specific embodiment, further illustrate the present invention.
Preparation example: the technique of the special efficacy spray production of snake is driven in a kind of field:
The extraction of the special efficacy spray effective ingredient of snake, the best proportioning of special efficacy spray and the filling technological process of spray that snake is driven in field are driven in field, are undertaken by following program:
1, will drive snake special efficacy spray plant insecticide raw material used: exterminate a family 1 part of 1 part, 1 part of dry rhizoma atractylodis, 1 part of dry Chinese lobelia, 1 part of dry dutchmanspipe root, 1 part of dry paris polyphylla and the extra dry white wine root of Dahurian angelica of 1 part of dry milkweed, 1 part of dry celery seed, 1 part of dry Garlic Seeds, 1 part of dry tobacco, dry snake is crushed to 100 orders and mixes.
2, plant insecticide raw material pulvis previous step obtained drops into extraction equipment and carries out CO
2Extraction, the extraction entrainer is ethanol; Extracting pressure 27 MPas are set, 52 ℃ of extraction temperature, CO
2Flow is 53～58 kg/hours, and 70% ethanol is made entrainer, and extraction time is controlled at 5 hours.
3, combination flooding snake volatile oil extraction obtained in mass ratio 15.3% ~ 15.5%, add the ethanol of mass ratio 80%.
4, adding mass ratio is 0.1%～0.3% citric acid again, be used to regulating pH value=6.5.
5, add again the organic silicon adhesive of mass ratio 3%, the isoamyl acetate of mass ratio 0.1%, the ethyl hexylate of mass ratio 0.3%, the Tween 80 of mass ratio 1%, fully stir and make it evenly after mixing, get the filling use of step ready.
6, fully automatic liquid filling production lines workflow:
Empty bottle arranges (the reasonable bottle of equipment belt platform) → wash bottle → bakings bottle → empty bottle and advances filling station → detection and location → filling head decline → filling valve and open → start filling → mass metrology → arrival setting numerical value → filling valve and close → expire and bottle go out filling station → turn to → hang lid → spiral cover → labeling → coding
At first empty bottle is put on conveyer belt, by conveyer belt, is sent to bottle washing machine and carries out wash bottle, bottle washing machine is mainly to decide according to filling number of liquid filling machine, and for example filling number of liquid filling machine is 8, and the wash bottle position of bottle washing machine is 8 so.Next after wash bottle, be sent to warm air drier by bottle sterilization, oven dry by conveyer, then bottle is sent to liquid filling machine, filling after bottle orientation, be sent to afterwards spiral cover, capping machine seals the bottle of filling content, final step is to label and coding.This is the whole workflow of automatic Liquid filler.
The Canning Technique parameter
:
Type specification: 25-250 milliliter;
Applicable valve: 1 inch (25.4 millimeters);
The filling capacity of content: 25-250 milliliter;
Content input adapter: 20 millimeters stainless steel pagoda joints of external diameter;
The filling capacity of propellant: 25-250 milliliter propellant input adapter: the anti-tooth of M22*1.5 (for example can dock with standard 15KG, 50KG oil liquefied gas steel cylinder);
Filling accuracy: ± 1%;
Applicable inhalator jar height: 70-330 millimeter;
Applicable inhalator jar diameter: φ 35 arrives 65 millimeters of φ;
Operating pressure: 0.5-1.0 MPa;
Maximum air consumption: 1 cube/minute;
Production capacity: by the filling 100 milliliters of liquid propellants of every tank, calculate, 1200 tanks/hour.
Claims (3)
1. the preparation method that snake special efficacy spray is driven in field, is characterized in that, the step of described method is:
(1) following composition raw material is got all the ready by formula, mixed after crushed after being dried to 100 order: 1 part of dry milkweed, 1 part of dry celery seed, 1 part of dry Garlic Seeds, 1 part of dry tobacco, dry snake exterminate a family 1 part of 1 part, 1 part of dry rhizoma atractylodis, 1 part of dry Chinese lobelia, 1 part of dry dutchmanspipe root, 1 part of dry paris polyphylla and the extra dry white wine root of Dahurian angelica;
(2) the plant insecticide raw material after above-mentioned pulverizing is dropped into to extraction equipment, adopt supercritical CO
2Fluid extraction technology extracts into combination flooding snake volatile oil;
The combination flooding snake volatile oil that (3) will extract, mass ratio by 15.3%～15.5%, adding mass ratio is 80% ethanol, adding mass ratio is 0.1%～0.3% citric acid again, and to add mass ratio be 3% organic silicon adhesive, and mass ratio is 0.1% isoamyl acetate, mass ratio is 0.3% ethyl hexylate, mass ratio is 1% Tween 80, fully stirs and makes it evenly after mixing, and adjust liquid to ormal weight: 1 milliliter contains 0.153～0.157 gram combination flooding snake volatile oil; Must drive snake liquid spray;
(4) will drive snake liquid spray sends into fully automatic liquid spray filling production lines and carries out filling.
2. a kind of field according to claim 1 preparation method of driving snake special efficacy spray, is characterized in that described CO
2Fluid extraction pressure 27 MPas, extraction CO
2Flow is 53～58 kg/hours, extraction time 5 hours, and 52 ℃ of extraction temperature, 70% ethanol is made entrainer.
3. a kind of field according to claim 1 preparation method of driving snake special efficacy spray, is characterized in that, described citric acid is for adjusting pH value, and regulating pH value is 6.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310392190.1A CN103404542B (en) | 2013-09-03 | 2013-09-03 | Method for preparing field snake-expelling special-effect spray |
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| CN201310392190.1A CN103404542B (en) | 2013-09-03 | 2013-09-03 | Method for preparing field snake-expelling special-effect spray |
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| CN103404542A true CN103404542A (en) | 2013-11-27 |
| CN103404542B CN103404542B (en) | 2015-04-08 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106724286A (en) * | 2016-11-18 | 2017-05-31 | 广西大学 | A kind of chair for fishing |
| CN110115273A (en) * | 2019-05-13 | 2019-08-13 | 深圳市积臣氏户外用品有限公司 | A kind of drive snake concentrate and preparation method thereof |
| CN110742094A (en) * | 2019-11-14 | 2020-02-04 | 横县丰创农业科技有限公司 | Snake-prevention agent for frog culture and preparation method thereof |
| CN110839653A (en) * | 2019-11-14 | 2020-02-28 | 横县丰创农业科技有限公司 | Snake-proof agent for breeding rats and preparation method thereof |
| CN115735914A (en) * | 2022-11-09 | 2023-03-07 | 福建木盾生物化工有限公司 | Snake expelling foam liquid capable of being solidified at normal temperature and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106724286A (en) * | 2016-11-18 | 2017-05-31 | 广西大学 | A kind of chair for fishing |
| CN110115273A (en) * | 2019-05-13 | 2019-08-13 | 深圳市积臣氏户外用品有限公司 | A kind of drive snake concentrate and preparation method thereof |
| CN110742094A (en) * | 2019-11-14 | 2020-02-04 | 横县丰创农业科技有限公司 | Snake-prevention agent for frog culture and preparation method thereof |
| CN110839653A (en) * | 2019-11-14 | 2020-02-28 | 横县丰创农业科技有限公司 | Snake-proof agent for breeding rats and preparation method thereof |
| CN115735914A (en) * | 2022-11-09 | 2023-03-07 | 福建木盾生物化工有限公司 | Snake expelling foam liquid capable of being solidified at normal temperature and preparation method thereof |
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| CN103404542B (en) | 2015-04-08 |
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