CN103393186B - Method for preparing health care beverage by using waste pomegranate bark - Google Patents
Method for preparing health care beverage by using waste pomegranate bark Download PDFInfo
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Abstract
The present invention discloses a method for preparing a health care beverage by using waste pomegranate bark, and belongs to the technical field of food. According to the present invention, a pomegranate bark extract, a pomegranate juice and xylitol are mixed to prepare the health care beverage, wherein per liter of the obtained health care beverage contains 10-20 g of the pomegranate bark extract, 400-600 mL of the pomegranate juice, and 30-60 g of the xylitol, the total flavone content is 1.361-2.149 mg/mL, and the ellagic acid content is 0.116-0.212 mg/mL; and the pomegranate bark is regarded as waste, with the present invention, problems of pomegranate bark discarding, resource waste and environmental pollution during a pomegranate processing process are solved, and the problem that the health care function of the pomegranate juice is not prominent is solved such that the pomegranate bark extract-containing health care beverage has characteristics of multiple health care functions, good taste, and body building.
Description
Technical field
The present invention relates to a kind of method preparing health drink with discarded granatum, belong to food technology field.
Background technology
Pomegranate is a kind ofly plucked from shrub or dungarunga and be planted in the fruit of Ya Re or torrid areas.Pomegranate originates in Russia, Iran, Afghanistan, Turkey one band, has passed to Mediterranean country afterwards westwards, and has passed to India, China eastwards.
Pomegranate edible part accounts for pomegranate about 10%, is squeezed and obtains Carthaginian apple raw juice, and juice of my pomegranate contains the nutriments such as abundant sugar, acid, vitamin, pectin, tannin.According to Compendium of Material Medica verification, pomegranate have help digestion, helping digestion, removing toxic substances quench the thirst, improve looks and medical care effect.Modern medicine study shows, juice of my pomegranate, also containing various active material, as determined the anthocyanin etc. of its tempting color and luster, has plurality of health care functions, but because of its active component content less, health care is outstanding not.
Flavonoids has biological function widely; comprise anti-lipid peroxidation, reducing blood lipid, suppression platelet aggregation, the effect that suppresses capillary permeability to increase and become fragile, have many pharmacological actions and the effects such as angiocardiopathy preventing, cancer-resisting, immunity moderation, anti-ageing, antibiotic and sterilizing, absorption ultraviolet radiation, cough-relieving and liver protection in vivo.
The 1950's, abroad started to study ellagic acid, the eighties has been applied to the clinic trial stage abroad.Ellagic acid has anticancer, anti-sudden change, suppresses the effects such as HIV, anti-oxidant, whitening, nti-freckle.In the developed countries such as the U.S., ellagic acid is the anticancer health-care product of two-way genetic modification salable, and international market product price is very high.Ellagic acid has excellent anti-sudden change, anticancer change effect, has good inhibitory action especially to colon cancer, the cancer of the esophagus, liver cancer, tongue and cutaneum carcinoma etc.Research prove concentration be 100 μm of ol/L ellagic acid 24h in suppress Caco-2 (colon adenocarcinoma cell), MCF-7(breast cancer cell), Hs578T(breast cancer cell) etc. the growth of cancer cell and diffusion.
In China, the output of pomegranate is very high, but the granatum produced in pomegranate process is mostly by as discarded object, and this not only causes the waste of resource, also has certain negative effect to the protection of environment.How fully developing granatum, improve its economic value added, is the problem being badly in need of taking seriously.On the other hand, for pomegranate juice, its flavones and ellagic acid content low, if the content of its active material can be increased, strengthen its health care, then can win more wide market.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of method preparing health drink with discarded granatum.
The preparation method of described health drink comprises the following steps: prepared by (1) Carthaginian apple raw juice: the pretreatment of raw material, pull an oar, protect look, coarse filtration, enzymolysis, clarification; (2) preparation of pomegranate rind extract: pretreatment of raw material, oven dry, pulverize, sieve, lixiviate, suction filtration, concentration and evaporation, drying; (3) mixed preparing: allotment, homogeneous, degassed, filling, sterilizing, obtain finished product.
The preparation method of described health drink comprises following concrete steps:
(1) Carthaginian apple raw juice preparation:
1. select fresh pomegranate to be raw material, clean up rear peeling, remove seed, be placed in juice extractor, pull an oar,
2. in order to prevent the color of juice of my pomegranate in process from changing, add 0.2% ~ 0.4%(w/w) citric acid as color stabilizer,
3. with duplex strainer, juice of my pomegranate is filtered, fruit juice is separated with pomace, collect filtrate,
4. in order to make pectin substance fully be hydrolyzed, in filtrate add 0.05% ~ 0.2%(w/w) pectase, at 40 ~ 50 DEG C, process 2h ~ 3h, colloidal substance lose protection and precipitate, play clarification;
(2) preparation of pomegranate rind extract:
1. get fresh pomegranate, clean, remove stalk, 50 ~ 60 DEG C of oven dry, pulverize, cross 100 orders, be prepared into Pomegranate Rind, brown bottle is preserved,
2. get 20g Pomegranate Rind, with 60%(v/v) ethanol, according to solid-to-liquid ratio 1:30 mixing, lixiviate 5h under the condition of temperature 40 DEG C, suction filtration obtains granatum extract,
3. by said extracted liquid evaporation and concentration at 40 ~ 45 DEG C, dry, obtain pomegranate rind extract;
(3) mixed preparing:
1. the pomegranate rind extract 10-20g, Carthaginian apple raw juice 400-600mL, the xylitol 30 ~ 60g that will prepare, add water to 1L, allocate, stir,
2. employing high pressure homogenizer carries out intensive shear, shock and the cavitation under high pressure to mixed liquor, makes solid particle in mixed liquor obtain micronization,
3. it carries out degassed process in temperature 60 ~ 70 DEG C, vacuum under being 0.07 ~ 0.08MPa condition,
4. treated juice of my pomegranate is loaded in 200mL vial by bottle placer, seals bottleneck, keeps 25 ~ 30min sterilization treatment, be then cooled to 30 ~ 40 DEG C, be finished product at 90 ~ 95 DEG C.
Another technical problem that the present invention will solve is to provide a kind of health drink containing pomegranate rind extract.
Described health drink contains water, pomegranate rind extract, Carthaginian apple raw juice and xylitol.
Described health drink is made up of following configuration proportion: pomegranate rind extract 10 ~ 20g, Carthaginian apple raw juice 400 ~ 600mL, and xylitol 30 ~ 60g adds water to 1L.
Carthaginian apple raw juice is obtained pomegranate rind extract and mixes with extracting in the granatum of giving it up from people by the present invention, obtains the beverage with plurality of health care functions, avoids granatum and go out of use, reduce the wasting of resources and environmental pollution.A kind of health-care granada beverage containing pomegranate rind extract obtained, general flavone content is 1.361 ~ 2.149mg/mL, ellagic acid content is 0.116 ~ 0.212mg/mL, there is angiocardiopathy preventing, cancer-resisting, immunity moderation, anti-ageing, antibiotic and sterilizing, absorption ultraviolet radiation, the effect such as cough-relieving and beauty treatment, to overcome in pomegranate drink active material as flavones with the shortcoming that ellagic acid content is few, health care is not given prominence to.
Detailed description of the invention
The preparation of embodiment 1 Carthaginian apple raw juice
(1) select fresh pomegranate to be raw material, clean up rear peeling, remove seed, be placed in juice extractor, pull an oar.
(2) in order to prevent the color of juice of my pomegranate in process from changing, the citric acid of 0.4% is added as color stabilizer.
(3) with duplex strainer, juice of my pomegranate is filtered, fruit juice is separated with pomace, collect filtrate.
(4) in order to make pectin substance fully be hydrolyzed, in filtrate, add the pectase of 0.1%, at 50 DEG C, process 3h, colloidal substance loses protection and precipitates, and plays clarification.
The preparation of embodiment 2 pomegranate rind extract
(1) get fresh pomegranate, clean, remove stalk, 50 DEG C of oven dry, pulverize, cross 100 orders, be prepared into Pomegranate Rind, brown bottle is preserved.
(2) get 20g Pomegranate Rind, with 60%(v/v) ethanol, according to solid-to-liquid ratio 1:30 mixing, lixiviate 5h under the condition of temperature 40 DEG C, suction filtration obtains granatum extract.
(3) by said extracted liquid evaporation and concentration at 40 DEG C, dry, obtain pomegranate rind extract.
The mixed preparing of embodiment 3 health-care granada beverage
(1) the pomegranate rind extract 15g prepared, Carthaginian apple raw juice 550mL, 42g xylitol are mixed, add water to 1L, allocate, stir;
(2) employing high pressure homogenizer carries out intensive shear, shock and the cavitation under high pressure to mixed liquor, makes solid particle in mixed liquor obtain micronization;
(3) because pomegranate drink in mixed process is mixed with a large amount of oxygen, can oxidizing brown stain be there is, therefore it is carried out degassed process in temperature 70 C, vacuum under being 0.08MPa condition;
(4) treated juice of my pomegranate is loaded in 200mL vial by bottle placer, seals bottleneck.At 90 DEG C, keep 30min sterilization treatment, be then cooled to 40 DEG C, be finished product 1.
According to above-mentioned same condition, do not add pomegranate rind extract, preparation pomegranate drink, is finished product 2.
The index of correlation of embodiment 4 health-care granada beverage and pomegranate drink detects
In order to verify effect of the present invention, the index of correlation of the health-care granada beverage (finished product 1) that the present inventor prepares above-mentioned enforcement and the pomegranate drink (finished product 2) that do not add pomegranate rind extract detects, and testing result is as follows.
(1) organoleptic examination
Table 1 health-care granada beverage and pomegranate drink organoleptic examination result
(2) technical target of the product detects
For the health-care granada beverage that above-mentioned enforcement prepares, measure the content of its pH value, pomegranate flavones and ellagic acid.PH value measures pH meter method in the method for inspection (GB/T10786-2006) with reference to national standard tinned food, the mensuration of pomegranate brass content is with reference to aluminum nitrate-nitrous acid colorimetric method (taking rutin as standard items), and the content of ellagic acid measures with reference to high-efficient liquid phase technique (taking ellagic acid as standard items).
Table 2 health-care granada beverage and pomegranate drink technical indicator testing result
As shown in Table 2, the flavones content of finished product 1 is close to 3 times of finished product 2, and ellagic acid content differs 10 times especially, and this shows that the health-care granada beverage adding pomegranate rind extract is not compared with adding the pomegranate drink of pomegranate rind extract, its flavones and ellagic acid content improve greatly, and health care is more outstanding.
(3) product sanitary index detects
The health-care granada beverage prepared the invention process carries out the detection of sanitary index by national standard fruit, vegetables juice beverages health standard (GB19297-2003).
The testing result of table 3 health-care granada beverages health index
As can be seen from Table 3, the content of health-care granada Arsenic in Drink prepared by the present invention, lead, copper and total plate count, coliform, saccharomycete, mould, pathogenic bacteria, all meet the standard of national standard fruit, vegetables juice beverages health standard (GB19297-2003).
Although the present invention with preferred embodiment openly as above; but it is also not used to limit the present invention, any person skilled in the art, without departing from the spirit and scope of the present invention; all can do various changes and modification, what therefore protection scope of the present invention should define with claims is as the criterion.
Claims (4)
1. prepare a method for health drink with discarded granatum, it is characterized in that, comprise the following steps:
(1) Carthaginian apple raw juice preparation: pretreatment of raw material, pull an oar, protect look, coarse filtration, enzymolysis, clarification;
1. select fresh pomegranate to be raw material, clean up rear peeling, get seed, be placed in juice extractor, pull an oar,
2. in order to prevent the color of juice of my pomegranate in process from changing, 0.2% ~ 0.4% adds citric acid as color stabilizer in mass ratio,
3. with duplex strainer, juice of my pomegranate is filtered, fruit juice is separated with pomace, collect filtrate,
4. in order to make pectin substance fully be hydrolyzed, in filtrate, add the pectase of 0.05% ~ 0.2% in mass ratio, at 40 ~ 50 DEG C, process 2h ~ 3h, colloidal substance loses protection and precipitates, and plays clarification;
(2) preparation of pomegranate rind extract: pretreatment of raw material, oven dry, pulverize, sieve, lixiviate, suction filtration, concentration and evaporation, drying;
1. get fresh pomegranate, clean, remove stalk, 50 ~ 60 DEG C of oven dry, pulverize, cross 100 orders, be prepared into Pomegranate Rind, brown bottle is preserved,
2. get 20g Pomegranate Rind, with the ethanol of 60%, according to solid-to-liquid ratio 1:30, under the condition of temperature 40 DEG C lixiviate 5h, suction filtration obtains granatum extract,
3. by said extracted liquid evaporation and concentration at 40 ~ 45 DEG C, dry, obtain pomegranate rind extract;
(3) mixed preparing: allotment, homogeneous, degassed, filling, sterilizing, obtain finished product;
1. the pomegranate rind extract 10 ~ 20g, the Carthaginian apple raw juice 400 ~ 600mL that prepare, xylitol 30 ~ 60g are mixed, add water to 1L, allocate, stir,
2. employing high pressure homogenizer carries out intensive shear, shock and the cavitation under high pressure to mixed liquor, makes solid particle in mixed liquor obtain micronization,
3. degassed process is carried out in temperature 60 ~ 70 DEG C, vacuum under being 0.07 ~ 0.08MPa condition,
4. treated juice of my pomegranate is loaded in 200mL vial by bottle placer, seals bottleneck, keeps 25 ~ 30min sterilization treatment, be then cooled to 30 ~ 40 DEG C, be finished product at 90 ~ 95 DEG C.
2. the health drink that described in a claim 1 prepared by method.
3. health drink according to claim 2, it is characterized in that, general flavone content is 1.361 ~ 2.149mg/mL, and ellagic acid content is 0.116 ~ 0.212mg/mL.
4. the application of health drink described in claim 2, is characterized in that, for the preparation of the product with angiocardiopathy preventing, cancer-resisting, immunity moderation, anti-ageing, antibiotic and sterilizing, absorption ultraviolet radiation, cough-relieving and beautification function.
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| CN104921248B (en) * | 2015-05-13 | 2017-03-08 | 怀远县荆涂山石榴科技有限公司 | A kind of manufacture method of Pericarpium Granati electuary |
| CN106047584A (en) * | 2016-08-24 | 2016-10-26 | 安徽省怀远县亚太石榴酒有限公司 | Brewing method of mellow and sweet pomegranate brandy |
| CN109588486A (en) * | 2018-11-14 | 2019-04-09 | 抚顺盛芝堂生物科技有限公司 | A kind of health drink |
| CN115191540A (en) * | 2021-07-23 | 2022-10-18 | 贵阳单宁科技有限公司 | Ellagic acid-containing composition and preparation method and application thereof |
| TW202310865A (en) * | 2021-09-13 | 2023-03-16 | 澤生生技股份有限公司 | Compositions for anti-aging and extending lifespan and the use thereof |
| CN116326701A (en) * | 2023-02-13 | 2023-06-27 | 西安丹若尔石榴酒业有限责任公司 | Composite pericarpium Granati juice beverage |
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| US7780998B2 (en) * | 1999-04-19 | 2010-08-24 | Stewart And Lynda Resnick Revocable Trust | Process for producing a therapeutically effective amount of an extract from pomegranate and compositions relating to same |
| CN102551135A (en) * | 2011-11-09 | 2012-07-11 | 辽宁悦喜堂养生科技有限公司 | Method for preparing natural and nutritional health-care pomegranate juice |
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Patent Citations (2)
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| US7780998B2 (en) * | 1999-04-19 | 2010-08-24 | Stewart And Lynda Resnick Revocable Trust | Process for producing a therapeutically effective amount of an extract from pomegranate and compositions relating to same |
| CN102551135A (en) * | 2011-11-09 | 2012-07-11 | 辽宁悦喜堂养生科技有限公司 | Method for preparing natural and nutritional health-care pomegranate juice |
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