CN103393186A - Method for preparing health care beverage by using waste pomegranate bark - Google Patents

Method for preparing health care beverage by using waste pomegranate bark Download PDF

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CN103393186A
CN103393186A CN2013103584698A CN201310358469A CN103393186A CN 103393186 A CN103393186 A CN 103393186A CN 2013103584698 A CN2013103584698 A CN 2013103584698A CN 201310358469 A CN201310358469 A CN 201310358469A CN 103393186 A CN103393186 A CN 103393186A
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pomegranate
juice
health care
pomegranate rind
extract
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CN103393186B (en
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毛健
郭燕飞
姬中伟
阳志锐
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Jiangnan University
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Abstract

The present invention discloses a method for preparing a health care beverage by using waste pomegranate bark, and belongs to the technical field of food. According to the present invention, a pomegranate bark extract, a pomegranate juice and xylitol are mixed to prepare the health care beverage, wherein per liter of the obtained health care beverage contains 10-20 g of the pomegranate bark extract, 400-600 mL of the pomegranate juice, and 30-60 g of the xylitol, the total flavone content is 1.361-2.149 mg/mL, and the ellagic acid content is 0.116-0.212 mg/mL; and the pomegranate bark is regarded as waste, with the present invention, problems of pomegranate bark discarding, resource waste and environmental pollution during a pomegranate processing process are solved, and the problem that the health care function of the pomegranate juice is not prominent is solved such that the pomegranate bark extract-containing health care beverage has characteristics of multiple health care functions, good taste, and body building.

Description

A kind of method for preparing health drink with discarded granatum
Technical field
The present invention relates to a kind of method for preparing health drink with discarded granatum, belong to food technology field.
Background technology
Pomegranate is a kind of fruit of plucking and be planted in Ya Re or torrid areas from shrub or dungarunga.Pomegranate originates in Russia, Iran, Afghanistan, Turkey's one band, has passed to afterwards Mediterranean country westwards, has passed to India, China eastwards.
The pomegranate edible part accounts for pomegranate 10% left and right, and its squeezing is obtained to Carthaginian apple raw juice, and juice of my pomegranate contains the nutriments such as abundant sugar, acid, vitamin, pectin, tannin.According to Compendium of Material Medica verification, pomegranate have help digestion, helping digestion, detoxifcation are quenched the thirst, beauty treatment and medical care effect.Modern medicine study shows, juice of my pomegranate also contains the various active material, as determines anthocyanin of its tempting color and luster etc., has plurality of health care functions, but less because of its active component content, health care is outstanding not.
Flavonoids has biological function widely; comprise the effect that suppresses lipid peroxidation, reducing blood lipid, inhibition platelet aggregation, suppresses capillary saturating property increase and become fragile, have in vivo that angiocardiopathy preventing, cancer-resisting, adjusting are immune, anti-ageing, many pharmacological actions and effects such as antibiotic and sterilizing, absorption ultraviolet radiation, cough-relieving and liver protection.
The 1950's, abroad started ellagic acid is studied, and has been applied to the clinic trial stage eighties abroad.Anticancer, anti-sudden change that ellagic acid has, suppress the effects such as HIV, anti-oxidant, whitening, nti-freckle.In the developed countries such as the U.S., ellagic acid is the anticancer health-care product of two-way genetic modification salable, and international market product price is very high.Ellagic acid has excellent anti-sudden change, anticancer change effect, especially colon cancer, the cancer of the esophagus, liver cancer, tongue and cutaneum carcinoma etc. is had to good inhibitory action.Studies have shown that concentration is in the ellagic acid 24h of 100 μ mol/L, to suppress Caco-2 (colon adenocarcinoma cell), MCF-7(breast cancer cell), the Hs578T(breast cancer cell) etc. growth and the diffusion of cancer cell.
In China, the output of pomegranate is very high, but the granatum that produces in the pomegranate process mostly is used as discarded object, and this has not only caused the waste of resource, and the protection of environment is also had to certain negative effect.How fully developing granatum, improve its economic value added, is to be badly in need of the problem of taking seriously.On the other hand, for pomegranate juice, its flavones and ellagic acid content are low, if can increase the content of its active material, strengthen its health care, can win more wide market.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of method for preparing health drink with discarded granatum.
The preparation method of described health drink comprises the following steps: (1) Carthaginian apple raw juice preparation: the pretreatment of raw material, pull an oar, protect look, coarse filtration, enzymolysis, clarification; (2) preparation of pomegranate rind extract: pretreatment of raw material, oven dry, pulverize, sieve, lixiviate, suction filtration, concentration and evaporation, drying; (3) mixed preparing: allotment, homogeneous, degassed, filling, sterilizing obtain finished product.
The preparation method of described health drink comprises following concrete steps:
(1) Carthaginian apple raw juice preparation:
1. selecting fresh pomegranate is raw material, cleans up rear peeling, removes seed, is placed in juice extractor, pull an oar,
2. in order to prevent the change color of juice of my pomegranate in process, add 0.2%~0.4%(w/w) citric acid as color stabilizer,
3. with duplex strainer, juice of my pomegranate is filtered, fruit juice is separated with pomace, collect filtrate,
4. for pectin substance fully is hydrolyzed, in filtrate, add 0.05%~0.2%(w/w) pectase, under 40~50 ℃, process 2h~3h, colloidal substance loses protection and precipitates, the performance clarification;
(2) preparation of pomegranate rind extract:
1. get fresh pomegranate, clean, go stalk, 50~60 ℃ of oven dry, pulverize, and crosses 100 orders, is prepared into Pomegranate Rind, and brown bottle is preserved,
2. get the 20g Pomegranate Rind, use 60%(v/v) ethanol, according to solid-to-liquid ratio 1:30, mix, lixiviate 5h under the condition of 40 ℃ of temperature, suction filtration obtains the granatum extract,
3. by said extracted liquid 40~45 ℃ of lower evaporation and concentration, the oven dry, obtain pomegranate rind extract;
(3) mixed preparing:
The pomegranate rind extract 10-20g that 1. will prepare, Carthaginian apple raw juice 400-600mL, xylitol 30~60g, add water to 1L, allocates, stir,
2. adopt high pressure homogenizer to carry out strong shearing, shock and the cavitation under high pressure to mixed liquor, make solid particle in mixed liquor obtain the ultra micro refinement,
3. it is under 0.07~0.08MPa condition, to carry out degassed processing in 60~70 ℃ of temperature, vacuum,
4. treated juice of my pomegranate is packed in the 200mL vial by bottle placer, seals bottleneck, under 90~95 ℃, keeps 25~30min sterilization treatment, then is cooled to 30~40 ℃, is finished product.
Another technical problem that the present invention will solve is to provide a kind of health drink that contains pomegranate rind extract.
Described health drink contains water, pomegranate rind extract, Carthaginian apple raw juice and xylitol.
Described health drink is comprised of following configuration proportion: pomegranate rind extract 10~20g, and Carthaginian apple raw juice 400~600mL, xylitol 30~60g adds water to 1L.
The present invention obtains pomegranate rind extract and mixes Carthaginian apple raw juice and the granatum of giving it up from people, extracting, and has obtained having the beverage of plurality of health care functions, has avoided granatum to go out of use, reduce the wasting of resources and environmental pollution.Resulting a kind of health-care granada beverage that contains pomegranate rind extract, general flavone content is 1.361~2.149mg/mL, ellagic acid content is 0.116~0.212mg/mL, have that angiocardiopathy preventing, cancer-resisting, adjusting are immune, anti-ageing, the effects such as antibiotic and sterilizing, absorption ultraviolet radiation, cough-relieving and beauty treatment, overcome active material such as flavones in the pomegranate drink and ellagic acid content is few, health care is outstanding shortcoming.
The specific embodiment
The preparation of embodiment 1 Carthaginian apple raw juice
(1) selecting fresh pomegranate is raw material, cleans up rear peeling, removes seed, is placed in juice extractor, pulls an oar.
(2), in order to prevent the change color of juice of my pomegranate in process, add 0.4% citric acid as color stabilizer.
(3) with duplex strainer, juice of my pomegranate is filtered, fruit juice is separated with pomace, collect filtrate.
(4) for pectin substance fully is hydrolyzed, in filtrate, add 0.1% pectase, under 50 ℃, process 3h, colloidal substance loses protection and precipitates, the performance clarification.
The preparation of embodiment 2 pomegranate rind extracts
(1) get fresh pomegranate, clean, go stalk, 50 ℃ of oven dry, pulverize, and crosses 100 orders, is prepared into Pomegranate Rind, and brown bottle is preserved.
(2) get the 20g Pomegranate Rind, use 60%(v/v) ethanol, according to solid-to-liquid ratio 1:30, mix, lixiviate 5h under the condition of 40 ℃ of temperature, suction filtration obtains the granatum extract.
(3) by said extracted liquid 40 ℃ of lower evaporation and concentration, the oven dry, obtain pomegranate rind extract.
The mixed preparing of embodiment 3 health-care granada beverages
(1) the pomegranate rind extract 15g that will prepare, Carthaginian apple raw juice 550mL, 42g xylitol mix, and add water to 1L, allocate, and stir;
(2) adopt high pressure homogenizer to carry out strong shearing, shock and the cavitation under high pressure to mixed liquor, make solid particle in mixed liquor obtain the ultra micro refinement;
(3) because pomegranate drink in mixed process is mixed with a large amount of oxygen, oxidizing brown stain can occur, therefore in temperature 70 C, vacuum, be under the 0.08MPa condition, to carry out degassed processing by it;
(4) treated juice of my pomegranate is packed in the 200mL vial by bottle placer, seals bottleneck.Under 90 ℃, keep the 30min sterilization treatment, then be cooled to 40 ℃, be finished product 1.
According to above-mentioned same condition, do not add pomegranate rind extract, the preparation pomegranate drink, be finished product 2.
The index of correlation of embodiment 4 health-care granada beverages and pomegranate drink detects
In order to verify effect of the present invention, health-care granada beverage prepared above-mentioned enforcement by the present inventor (finished product 1) and the index of correlation that does not add the pomegranate drink (finished product 2) of pomegranate rind extract detect, and testing result is as follows.
(1) organoleptic examination
Table 1 health-care granada beverage and pomegranate drink organoleptic examination result
Figure BDA0000367548020000041
(2) technical target of the product detects
For the health-care granada beverage that above-mentioned enforcement prepares, measure the content of its pH value, pomegranate flavones and ellagic acid.The pH pH-value determination pH is with reference to pH meter method in the method for inspection (GB/T10786-2006) of national standard tinned food, the mensuration of pomegranate brass content is with reference to aluminum nitrate-nitrous acid colorimetric method (take rutin as standard items), and the content of ellagic acid is measured with reference to high-efficient liquid phase technique (take ellagic acid as standard items).
Table 2 health-care granada beverage and pomegranate drink technical indicator testing result
Figure BDA0000367548020000042
As shown in Table 2, the flavones content of finished product 1 is close to 3 times of finished product 2, and ellagic acid content differs 10 times especially, and this shows that the health-care granada beverage that adds pomegranate rind extract compares with the pomegranate drink that does not add pomegranate rind extract, its flavones and ellagic acid content improve greatly, and health care is more outstanding.
(3) the product sanitary index detects
Health-care granada beverage prepared by the invention process carries out the detection of sanitary index by national standard fruit, vegetables juice beverages health standard (GB19297-2003).
The testing result of table 3 health-care granada beverages health index
Figure BDA0000367548020000043
Figure BDA0000367548020000051
As can be seen from Table 3, the content of health-care granada Arsenic in Drink prepared by the present invention, lead, copper and total plate count, coliform, saccharomycete, mould, pathogenic bacteria, all meet the standard of national standard fruit, vegetables juice beverages health standard (GB19297-2003).
Although the present invention with preferred embodiment openly as above; but it is not in order to limit the present invention, any person skilled in the art, without departing from the spirit and scope of the present invention; all can do various changes and modification, so protection scope of the present invention should be with being as the criterion that claims were defined.

Claims (6)

1. a method for preparing health drink with discarded granatum, is characterized in that, comprises the following steps: the preparation of (1) Carthaginian apple raw juice: pretreatment of raw material, pull an oar, protect look, coarse filtration, enzymolysis, clarification; (2) preparation of pomegranate rind extract: pretreatment of raw material, oven dry, pulverize, sieve, lixiviate, suction filtration, concentration and evaporation, drying; (3) mixed preparing: allotment, homogeneous, degassed, filling, sterilizing obtain finished product.
2. method according to claim 1, is characterized in that, specifically comprises the following steps:
(1) preparation of Carthaginian apple raw juice:
1. selecting fresh pomegranate is raw material, cleans up rear peeling, removes seed, is placed in juice extractor, pull an oar,
2. in order to prevent the change color of juice of my pomegranate in process, 0.2%~0.4% adds citric acid as color stabilizer in mass ratio,
3. with duplex strainer, juice of my pomegranate is filtered, fruit juice is separated with pomace, collect filtrate,
4. for pectin substance fully is hydrolyzed, in filtrate, add 0.05%~0.2% pectase in mass ratio, under 40~50 ℃, process 2h~3h, colloidal substance loses protection and precipitates, the performance clarification;
(2) preparation of pomegranate rind extract:
1. get fresh pomegranate, clean, go stalk, 50~60 ℃ of oven dry, pulverize, and crosses 100 orders, is prepared into Pomegranate Rind, and brown bottle is preserved,
2. get the 20g Pomegranate Rind, the ethanol with 60%, according to solid-to-liquid ratio 1:30, under the condition of 40 ℃ of temperature lixiviate 5h, suction filtration obtains the granatum extract,
3. by said extracted liquid 40~45 ℃ of lower evaporation and concentration, the oven dry, obtain pomegranate rind extract;
(3) mixed preparing:
Pomegranate rind extract 10~the 20g that 1. will prepare, Carthaginian apple raw juice 400~600mL, xylitol 30~60g mix, and add water to 1L, allocate, stir,
2. adopt high pressure homogenizer to carry out strong shearing, shock and the cavitation under high pressure to mixed liquor, make solid particle in mixed liquor obtain the ultra micro refinement,
3. in 60~70 ℃ of temperature, vacuum, be under 0.07~0.08MPa condition, to carry out degassed processing,
4. treated juice of my pomegranate is packed in the 200mL vial by bottle placer, seals bottleneck, under 90~95 ℃, keeps 25~30min sterilization treatment, then is cooled to 30~40 ℃, is finished product.
3. a health drink prepared by the described method of claim 1, is characterized in that, contains water, pomegranate rind extract, Carthaginian apple raw juice and xylitol.
4. health drink according to claim 3, is characterized in that, every liter contains pomegranate rind extract 10~20g, Carthaginian apple raw juice 400~600mL, xylitol 30~60g.
5. health drink according to claim 3, is characterized in that, general flavone content is 1.361~2.149mg/mL, and ellagic acid content is 0.116~0.212mg/mL.
6. the application of the described health drink of claim 3, is characterized in that, can be used for preparing have angiocardiopathy preventing, cancer-resisting, adjusting are immune, anti-ageing, the product of antibiotic and sterilizing, absorption ultraviolet radiation, cough-relieving and beautification function.
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Publication number Priority date Publication date Assignee Title
CN104921248A (en) * 2015-05-13 2015-09-23 怀远县荆涂山石榴科技有限公司 Making method for pomegranate rind electuary
CN106047584A (en) * 2016-08-24 2016-10-26 安徽省怀远县亚太石榴酒有限公司 Brewing method of mellow and sweet pomegranate brandy
CN109588486A (en) * 2018-11-14 2019-04-09 抚顺盛芝堂生物科技有限公司 A kind of health drink
CN115191540A (en) * 2021-07-23 2022-10-18 贵阳单宁科技有限公司 Ellagic acid-containing composition and preparation method and application thereof
CN115779012A (en) * 2021-09-13 2023-03-14 泽生生技股份有限公司 Composition with anti-aging effect and application thereof

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104921248A (en) * 2015-05-13 2015-09-23 怀远县荆涂山石榴科技有限公司 Making method for pomegranate rind electuary
CN106047584A (en) * 2016-08-24 2016-10-26 安徽省怀远县亚太石榴酒有限公司 Brewing method of mellow and sweet pomegranate brandy
CN109588486A (en) * 2018-11-14 2019-04-09 抚顺盛芝堂生物科技有限公司 A kind of health drink
CN115191540A (en) * 2021-07-23 2022-10-18 贵阳单宁科技有限公司 Ellagic acid-containing composition and preparation method and application thereof
CN115779012A (en) * 2021-09-13 2023-03-14 泽生生技股份有限公司 Composition with anti-aging effect and application thereof

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