CN102845748B - Composition containing tea polyphenol and cordyceps militaris and preparation method thereof - Google Patents
Composition containing tea polyphenol and cordyceps militaris and preparation method thereof Download PDFInfo
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- CN102845748B CN102845748B CN2012103360300A CN201210336030A CN102845748B CN 102845748 B CN102845748 B CN 102845748B CN 2012103360300 A CN2012103360300 A CN 2012103360300A CN 201210336030 A CN201210336030 A CN 201210336030A CN 102845748 B CN102845748 B CN 102845748B
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Abstract
The invention provides a composition containing tea polyphenol and cordyceps militaris, and a preparation method thereof. According to the invention, tea polyphenol, cordyceps militaris extraction liquid, citric acid and vitamin C are blended, and the mixture is subjected to homogenization, filtration, and a sterilization treatment, such that the composition is prepared. According to the invention, cordyceps militaris sporocarp is crushed and extracted, such that the cordyceps militaris extraction liquid is obtained. With the composition and the preparation method, tea polyphenol and cordyceps militari can be effectively combined, and health-care functions of tea polyphenol and cordyceps militari can be sufficiently developed.
Description
Technical field
The present invention relates to making and the production of teas health products, particularly a kind of composition and method of making the same that contains Tea Polyphenols and north cordyceps extracting liquid.
Background technology
Tealeaves from ancient times to the present continues thousands of years, except the delicate fragrance of tea itself, also has clear and definite health care.The record of " all medicines are the medicine of each disease; tea is the medicine of ten thousand diseases " is arranged in the supplement to the Herbal, modern study shows, tealeaves has and has effect anticancer, anti-ageing and the control cardiovascular and cerebrovascular disease, and the main functional component of tealeaves is polyphenols contained in the tealeaves---Tea Polyphenols (Tea Polyphenols), Tea Polyphenols is the biological flavone compounds, mainly is made up of flavanol compound and flavonols and glycoside, and good water-solubility is arranged.A series of researchs such as Japan, Britain, China find that also Tea Polyphenols has significantly antibacterial, bactericidal action, can effectively reduce large intestine to cholesterol absorption, prevent and treat atherosclerotic.The effect highly significant that Tea Polyphenols is anti-oxidant, anti-aging, its mechanism are (OH) can stop free chain reaction in the human body, have the effect of similar SOD because have the light base of a plurality of activity in the Tea Polyphenols molecule.Therefore, remove at present in free radical and the oxidation-resisting health-care food, China research at most, the longest actual conditions that also meets most China of time be Tea Polyphenols.Because the good function of preventing and curing diseases of Tea Polyphenols, scientist classifies Tea Polyphenols as the important component part of health food both at home and abroad.Toxicologic study shows that Tea Polyphenols is the natural adding ingredient of food, beverage, medicine and cosmetics of safety, no cumulative toxicity.
Northern Chinese caterpillar Fungus is a kind of rare dietotherapeutic bacterium, contain cordycepin, cordycepic acid, polysaccharide, vitamin and trace element, protein content height, amino acid kind are many, have significantly refresh oneself, anticancer and improve medical care effect such as body immunity, be a kind of can with the good raw material Tea Polyphenols compatibility, that increase health care.Patent application 201110171236.8 has proposed " manufacture craft of the white tea of a kind of Chinese caterpillar fungus ", in this application, utilizes Chinese caterpillar fungus and tealeaves as composition, with fresh tea leaf as raw material; Tealeaves is carried out drying handle, then dried white tea tealeaves is mixed in 4: 1 ratio with cordyceps militaris fruit body, make finished product after the packing.Compare with the white tea technology of tradition, the white tea of this application made, its tealeaves tea shape is curled and is tightly tied, and is convenient to packing and transportation, not only can remove assorted the flavor effectively, makes that white tea smell is stronger, and while Tea Polyphenols and amino acid whose content also have tangible increase.
Yet said method only is that the two simply mixes with tealeaves and Chinese caterpillar fungus, and its form still is tealeaves, can not give full play to the health-care efficacy of Tea Polyphenols and Chinese caterpillar fungus.
Summary of the invention
The object of the invention is to provide a kind of composition and method of making the same that contains Tea Polyphenols and north cordyceps extracting liquid, said composition and preparation method can make up Tea Polyphenols and northern Chinese caterpillar Fungus effectively, give full play to the health-care efficacy of Tea Polyphenols and northern Chinese caterpillar Fungus.
Another object of the present invention is to provide a kind of composition and method of making the same that contains Tea Polyphenols and north cordyceps extracting liquid, and said composition and preparation method thereof technology is simple, and processing ease is convenient to carry out the production of scale.
To achieve these goals, the invention provides following technical scheme:
A kind of composition that contains Tea Polyphenols and north cordyceps extracting liquid is characterized in that, said composition is to be prepared from by the following raw materials in part by weight proportioning:
Tea Polyphenols 8 ~ 10
North cordyceps extracting liquid 10 ~ 25
Citric acid 1 ~ 2
Vitamin C 5 ~ 10
Wherein, north cordyceps extracting liquid prepares by following manner:
1), pulverize cordyceps militaris fruit body, be crushed to the above particle of 100 orders and get final product;
2), lixiviate, add the water of 5 ~ 10 times of weight of cordyceps militaris fruit body, lixiviate is more than 1.5 hours;
3), filtering and concentrating, leaching liquor is filtered, and is concentrated into 1/10 of leaching liquor volume.
The another kind of embodiment of composition of the present invention is that described vitamin C can be replaced by vitamin A, Cobastab, vitamin D, vitamin E, vitamin K.
Another embodiment of composition of the present invention is that described citric acid can be replaced by mineral matter, amino acid, compound sugar, dietary fiber, prebiotics, lecithin, nucleotides.
A kind of preparation of compositions method that contains Tea Polyphenols and north cordyceps extracting liquid of the present invention is characterized in that this preparation method comprises the steps:
A, preparation north cordyceps extracting liquid:
1), pulverize cordyceps militaris fruit body, be crushed to the above particle of 100 orders and get final product;
2), lixiviate, add the water of 5 ~ 10 times of weight of cordyceps militaris fruit body, lixiviate is more than 1.5 hours;
3), filtering and concentrating, leaching liquor is filtered, and is concentrated into 1/10 of leaching liquor volume;
B, mixing preparation: Tea Polyphenols, north cordyceps extracting liquid, citric acid and vitamin C are mixed by above-mentioned weight proportion;
C, sterilization: adopt flash pasteurization to sterilize, the solution of gained is the composition that contains Tea Polyphenols and north cordyceps extracting liquid of the present invention.
In preparation method of composition of the present invention, the preparation north cordyceps extracting liquid comprises the steps:
1), pulverize, cordyceps militaris fruit body is pulverized, be crushed to the above particle of 100 orders and get final product;
2), lixiviate, with the cordyceps militaris fruit body after pulverizing with hot water refluxing extraction 2 times: add the water of 5 ~ 10 times of amounts of cordyceps militaris fruit body weight the 1st time, extraction time is 90 ~ 120 minutes, and extracting temperature is 70 ℃ ~ 80 ℃, obtains leaching liquor for the first time; Add the water of 5 ~ 10 times of amounts of cordyceps militaris fruit body weight the 2nd time, extraction time is 120 ~ 180 minutes, extracts 80 ℃ ~ 90 ℃ of temperature, obtains leaching liquor for the second time;
3), filtering and concentrating, for the first time leaching liquor and for the second time leaching liquor filter respectively, the leaching liquor after will filtering then merges, and is concentrated by vacuum decompression again, is concentrated into 1/10 of leaching liquor cumulative volume, namely obtains north cordyceps extracting liquid after the cooling.
In preparation method of composition of the present invention, described mixing preparation step is specially: the weight proportion by above-mentioned composition takes by weighing Tea Polyphenols, north cordyceps extracting liquid, citric acid and vitamin C, fully mix, and remove by filter the precipitation that the allotment back produces.
In preparation method of composition of the present invention, after the described mixing preparation step, also further include homogenizing step: the mixed solution after mixing preparation is filtered is poured in the homogenizer homogenization pressure 15 MPa ~ 20Mpa, obtained performance stable compositions solution into.
In preparation method of composition of the present invention, before the described sterilization steps, also further include filtration step: the composition solution behind the homogeneous is filtered through diatomite filter or flame filter press, further separate fine suspension.Then, adopt flash pasteurization to sterilize, the solution of gained is the composition of Tea Polyphenols and north cordyceps extracting liquid.
The can under aseptic condition of prepared composition, sealing can be preserved standbyly in freezer, can be used as the stoste of making drink, perhaps, the composition concentrate drying is made powder, utilize powder to be raw material, be used for making products such as capsule, tablet, electuary, granule.
According to test, in the preparation of compositions process, the factor of nutrient composition content in the north cordyceps extracting liquid of influencing mainly contains the ratio of water temperature, extraction time and raw material and water.In view of this, we have carried out orthogonal test to the factor that influences northern Chinese caterpillar Fungus nutritional labeling yield, determined optimal processing parameter, wherein: 70 ~ 90 ℃ of water temperatures, extraction time 90 ~ 120 minutes for the first time, be for the second time that 120 ~ 180 minutes, the solid-liquid ratio (weight ratio) of each lixiviate are 1:5 ~ 10.Nutrient composition content is the highest in the north cordyceps extracting liquid that according to said method makes.Through check, the nutrition that contains in the composition, wherein, and cordycepic acid 38mg/g, Cordyceps sinensis polysaccharide 95mg/g, cordycepin are 1.05mg/g.
Because said composition contains a large amount of Tea Polyphenols and nutritional labelings such as cordycepin and cordycepic acid, therefore have anti-ageing, increase body immunity, produce refreshing effect to the mind rapidly, health care such as reducing weight and beautifying features.Studies show that: take in the 160mg Tea Polyphenols for each person every day and namely nitrosation process in the human body is produced obvious suppression and blocking effect, thereby reach the removing active oxygen radical, blocking-up lipid peroxidation process, improve the activity of human body endoenzyme, the Tea Polyphenols of absorption 480mg then inhibitory action reaches the highest, and cordycepin can suppress the generation of proleulzin simultaneously by inducing the generation il-1, thereby has stronger immunoloregulation function.
The specific embodiment
Below, in conjunction with the embodiments the composition and method of making the same that contains Tea Polyphenols and north cordyceps extracting liquid of the present invention is described in further detail.
Embodiment 1:
A, preparation north cordyceps extracting liquid.
A1, the cordyceps militaris fruit body after will cleaning are pulverized, and are crushed to the above particle of 100 orders and get final product.
A2, the particle after will pulverizing place extractor, add water by weight the ratio of 1:20, are heated to 70-80 ℃ and carry out lixiviate.
Lixiviate is at twice: adding 10 times of amounts the 1st time carries out lixiviate, and extraction time is 120 minutes, obtains leaching liquor for the first time, and leaching liquor filters for the first time, puts into holding vessel to preserve; The water that filter residue adds 10 times of amounts again carries out the 2nd lixiviate, is heated to 80 ℃ and carries out lixiviate, and extraction time is 120 minutes, obtains leaching liquor for the second time, and leaching liquor is put into holding vessel after filtering for the second time.
A3,2 times leaching liquors (for the first time leaching liquor and for the second time leaching liquor) are merged, after cooling is left standstill 12 hours, filter again and obtain making up leaching liquor; The combination leaching liquor is concentrated into 1/10 of original volume through the vacuum drying thickener; This concentrate is north cordyceps extracting liquid.
B, mixing preparation: take by weighing north cordyceps extracting liquid 200g, place Agitation Tank; Take by weighing Tea Polyphenols 100g, citric acid 10g, vitamin C 100g more respectively, these three kinds of materials are added respectively in the Agitation Tank that north cordyceps extracting liquid is housed, fully stir, solution mixes the back and filters, and removes the precipitation that the allotment back produces.
C, homogeneous: the mixed solution that will allocate after filtering is poured in the homogenizer, and homogenization pressure 15M Pa ~ 20M Pa kept 30 minutes, can strengthen the stability of composition by homogeneous.
D, filtration and sterilization: filter through diatomite filter or flame filter press, further separate fine suspension, obtain filtrate, filtrate is adopted high-temperature short-time sterilization, and the settled solution of gained is the composition that contains Tea Polyphenols and north cordyceps extracting liquid.
Then, this composition can be at filling and sealing under the aseptic condition, for allocating the liquid drink or making other formulation and use.Such as, be that this composition of 410g places material-compound tank with above-mentioned gross weight, add 350g xylitol and 10L deionized water again, fully stir, can prepare total amount is the liquid drink of 10L.
Embodiment 2:
A, preparation north cordyceps extracting liquid.
A1, the cordyceps militaris fruit body after will cleaning are pulverized, and are crushed to the above particle of 100 orders and get final product.
A2, the particle after will pulverizing place extractor, add water by weight the ratio of 1:10, are heated to 70-90 ℃ and carry out lixiviate.
Lixiviate is at twice: the 1st time extraction time is 90 minutes, adds water by weight the ratio of 1:5, and extraction temperature is 90 ℃, obtains leaching liquor for the first time, and leaching liquor filters for the first time, puts into holding vessel to preserve; The water that filter residue adds 5 times of amounts again carries out the 2nd lixiviate, and the ratio of 1:5 adds water by weight, is heated to 70 ℃ and extracts, and extraction time is 180 minutes, obtains leaching liquor for the second time, and leaching liquor is put into holding vessel after filtering for the second time.
A3,2 leaching liquors are merged, after cooling is left standstill 24 hours, filter again and obtain making up leaching liquor; The combination leaching liquor is concentrated into 1/4 of original volume through the vacuum drying thickener; This concentrate is north cordyceps extracting liquid.
B, mixing preparation: take by weighing north cordyceps extracting liquid 250g, place Agitation Tank; Take by weighing Tea Polyphenols 80g, citric acid 20g, vitamin C 50g more respectively, these three kinds of materials are added respectively in the Agitation Tank that north cordyceps extracting liquid is housed, fully stir, solution mixes the back and filters, and removes the precipitation that the allotment back produces.
C, homogeneous: the mixed solution that will allocate after filtering is poured in the homogenizer, and homogenization pressure 15M Pa ~ 20M Pa kept 90 minutes, can strengthen the stability of composition by homogeneous.
D, filtration and sterilization: filter through diatomite filter or flame filter press, further separate fine suspension, obtain filtrate, filtrate is adopted high-temperature short-time sterilization, and the settled solution of gained is the composition that contains Tea Polyphenols and north cordyceps extracting liquid.
After above-mentioned gross weight was this composition vacuum drying of 400g, resulting powder can be made into capsule, oral and buccal tablet etc.
Embodiment 3:
A, preparation north cordyceps extracting liquid.
A1, the cordyceps militaris fruit body after will cleaning are pulverized, and are crushed to the above particle of 100 orders and get final product.
Particle after A2, the pulverizing places extractor, and the ratio of 1:15 adds water by weight, is heated to 75-85 ℃ and carries out lixiviate.
Lixiviate is at twice: the 1st time extraction time is 100 minutes, adds water by weight the ratio of 1:9, and extraction temperature is 85 ℃, obtains leaching liquor for the first time, and leaching liquor filters for the first time, puts into holding vessel to preserve; The water that filter residue adds 6 times of amounts again carries out the 2nd lixiviate, is heated to 75 ℃ and extracts, and extraction time is 150 minutes, obtains leaching liquor for the second time, and leaching liquor is put into holding vessel after filtering for the second time.
A3,2 leaching liquors are merged, after cooling is left standstill 18 hours, filter again; Filtrate is concentrated into 1/9 of original volume through the vacuum drying thickener; This concentrate is north cordyceps extracting liquid.
B, mixing preparation: take by weighing north cordyceps extracting liquid 235g, place Agitation Tank; Take by weighing Tea Polyphenols 90g, citric acid 15g, vitamin C 80g more respectively, these three kinds of materials are added respectively in the Agitation Tank that north cordyceps extracting liquid is housed, fully stir, solution mixes the back and filters, and removes the precipitation that the allotment back produces.
C, homogeneous: the mixed solution that will allocate after filtering is poured in the homogenizer, and homogenization pressure 15M Pa ~ 20M Pa kept 120 minutes, can strengthen the stability of composition by homogeneous.
D, filtration and sterilization: filter through diatomite filter or flame filter press, further separate fine suspension, obtain filtrate, filtrate is adopted high-temperature short-time sterilization, and the settled solution of gained is the composition that contains Tea Polyphenols and north cordyceps extracting liquid.
After above-mentioned gross weight was the composition vacuum drying of 420g, resulting powder was equipped with auxiliary material by wet granulation, can oral granule processed.
In a word, the above only is preferred embodiment of the present invention, not in order to limiting the present invention, all any modifications of doing within the spirit and principles in the present invention, is equal to and replaces and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a composition that contains Tea Polyphenols and north cordyceps extracting liquid is characterized in that, said composition is to be prepared from by the following raw materials in part by weight proportioning:
Tea Polyphenols 8 ~ 10
North cordyceps extracting liquid 10 ~ 25
Citric acid 1 ~ 2
Vitamin C 5 ~ 10
Wherein, north cordyceps extracting liquid prepares by following manner:
1), pulverize cordyceps militaris fruit body, be crushed to the above particle of 100 orders and get final product;
2), lixiviate, with the cordyceps militaris fruit body after pulverizing with hot water refluxing extraction 2 times: add the water of 5 ~ 10 times of amounts of cordyceps militaris fruit body weight the 1st time, extraction time is 90 ~ 120 minutes, and extracting temperature is 70 ℃ ~ 80 ℃, obtains leaching liquor for the first time; Add the water of 5 ~ 10 times of amounts of cordyceps militaris fruit body weight the 2nd time, extraction time is 120 ~ 180 minutes, extracts 80 ℃ ~ 90 ℃ of temperature, obtains leaching liquor for the second time;
3), filtering and concentrating, for the first time leaching liquor and for the second time leaching liquor filter respectively, the leaching liquor after will filtering then merges, and is concentrated by vacuum decompression again, is concentrated into 1/10 of leaching liquor cumulative volume, namely obtains north cordyceps extracting liquid after the cooling.
2. the composition that contains Tea Polyphenols and north cordyceps extracting liquid as claimed in claim 1 is characterized in that, described vitamin C can be replaced by vitamin A, Cobastab, vitamin D, vitamin E, vitamin K.
3. the composition that contains Tea Polyphenols and north cordyceps extracting liquid as claimed in claim 1 is characterized in that, described citric acid can be replaced by mineral matter, amino acid, compound sugar, dietary fiber, prebiotics, lecithin, nucleotides.
4. a preparation of compositions method that contains Tea Polyphenols and north cordyceps extracting liquid is characterized in that this preparation method comprises the steps:
A, preparation north cordyceps extracting liquid:
1), pulverize cordyceps militaris fruit body, be crushed to the above particle of 100 orders and get final product;
2), lixiviate, with the cordyceps militaris fruit body after pulverizing with hot water refluxing extraction 2 times: add the water of 5 ~ 10 times of amounts of cordyceps militaris fruit body weight the 1st time, extraction time is 90 ~ 120 minutes, and extracting temperature is 70 ℃ ~ 80 ℃, obtains leaching liquor for the first time; Add the water of 5 ~ 10 times of amounts of cordyceps militaris fruit body weight the 2nd time, extraction time is 120 ~ 180 minutes, extracts 80 ℃ ~ 90 ℃ of temperature, obtains leaching liquor for the second time;
3), filtering and concentrating, for the first time leaching liquor and for the second time leaching liquor filter respectively, the leaching liquor after will filtering then merges, and is concentrated by vacuum decompression again, is concentrated into 1/10 of leaching liquor cumulative volume, namely obtains north cordyceps extracting liquid after the cooling;
B, mixing preparation: Tea Polyphenols, north cordyceps extracting liquid, citric acid and vitamin C are mixed by the described weight proportion of claim 1;
C, sterilization: adopt flash pasteurization to sterilize, the solution of gained is the composition that contains Tea Polyphenols and north cordyceps extracting liquid of the present invention.
5. the preparation of compositions method that contains Tea Polyphenols and north cordyceps extracting liquid as claimed in claim 4, it is characterized in that, described mixing preparation step is specially: take by weighing Tea Polyphenols, north cordyceps extracting liquid, citric acid and vitamin C by the described weight proportion of claim 1, fully mix, and remove by filter the precipitation that the allotment back produces.
6. the preparation of compositions method that contains Tea Polyphenols and north cordyceps extracting liquid as claimed in claim 4, it is characterized in that, after the described mixing preparation step, also further include homogenizing step: the mixed solution after mixing preparation is filtered is poured in the homogenizer, homogenization pressure 15 MPa ~ 20Mpa, obtained performance stable compositions solution.
7. the preparation of compositions method that contains Tea Polyphenols and north cordyceps extracting liquid as claimed in claim 4, it is characterized in that, before the described sterilization steps, also further include filtration step: the composition solution behind the homogeneous is filtered through diatomite filter or flame filter press, further separate fine suspension.
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| CN104920753A (en) * | 2015-06-19 | 2015-09-23 | 陈政 | Traditional Chinese medicine tabletting candy and preparation method thereof |
| CN104887831A (en) * | 2015-06-19 | 2015-09-09 | 陈政 | Traditional Chinese medicine pressed candy and preparation method thereof |
| CN104872365A (en) * | 2015-06-19 | 2015-09-02 | 陈政 | Tartary buckwheat dextrose candy and making method thereof |
| CN106754116A (en) * | 2016-11-23 | 2017-05-31 | 青海七彩花生物科技有限公司 | A kind of northern Chinese caterpillar Fungus health liquor |
| CN110302108A (en) * | 2019-07-01 | 2019-10-08 | 上海欧润化妆品有限公司 | A kind of extracting method and its application of Cordyceps extract |
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