CN103385825A - Peel-off type yellow orange whitening mask and preparation method thereof - Google Patents
Peel-off type yellow orange whitening mask and preparation method thereof Download PDFInfo
- Publication number
- CN103385825A CN103385825A CN2013102423928A CN201310242392A CN103385825A CN 103385825 A CN103385825 A CN 103385825A CN 2013102423928 A CN2013102423928 A CN 2013102423928A CN 201310242392 A CN201310242392 A CN 201310242392A CN 103385825 A CN103385825 A CN 103385825A
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- CN
- China
- Prior art keywords
- parts
- yellow orange
- skin
- peel
- exfoliated
- Prior art date
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- Granted
Links
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Abstract
The invention discloses a peel-off type yellow orange whitening mask and a preparation method thereof. The peel-off type yellow orange whitening mask is prepared by using a conventional method from the following raw materials by weight: 10 to 14 parts of polyvinyl alcohol, 8 to 12 parts of glycerin, 0.8 to 1.2 parts of 3-myristoylamidopropyl betaine, 4 to 6 parts of ethanol, 6 to 8 parts of sodium lauryl amphoacetate, 0.8 to 2 parts of a yellow orange extract, 0.03 to 0.08 part of a composite antiseptic and 100 parts of deionized water, wherein the composite antiseptic is composed of, by weight, 1 to 3 parts of carnosic acid, 3 to 5 parts of a bamboo leaf antioxidant, 1 to 3 parts of nisin and 1 to 3 parts of 3-iodo-2-propynyl butyl carbamate. The peel-off type yellow orange whitening mask provided by the invention can effectively prevent dryness, yellowing, roughness and the like of the face caused by fatigue, pollution, radiation, drying, an air-conditioner, etc., improves non-uniform skin colors of the face and enables the skin to rapidly become clean, white and uniform and to maintain moistened and glossy for a long time.
Description
Technical field
The present invention relates to facial film and preparation method thereof, be specifically related to clean flour film of a kind of exfoliated yellow orange and preparation method thereof.
Background technology
Facial film is the important content in skin nursing,, for the regular application facial film of all kinds of skin characteristics, can make the oily skin defat, and thick pore is restrained, and the skin of withered gauffer recovers gloss, and the inflammation of skin sore skin is inhibited.facial film makes skin seem salubrious after using, smooth and pure white delicacy, this is because when facial film is coated on skin, facial film and skin produce affinity, drying gradually along with facial film, the skin temperature rise, blood circulation is accelerated, skin-tightening and tension force are strengthened, the sebum of skin secretion and moisture reverse osmosis are in horny layer, the epidermis softness is unfolded, the pore instinct is opened, effective ingredient in facial film infiltrates skin and is absorbed, facial film tightly is connected with skin simultaneously, when removing facial film, aging cutin on skin, in pore, the deep layer dirt is also by the while leukorrhagia, make skin pure and fresh clean.
The principle of facial film, utilize exactly the blink that covers face, extraneous air and the pollution of temporary transient isolation, improve the skin temperature, the pore expansion of skin, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to skin and get rid of the oil substances of the metabolic product of epidermis cell and accumulation, the moisture in facial film infiltrates the horny layer of skin epidermis, it is soft that skin becomes, and skin light naturally is flexible.
Along with the raising of people's quality of the life and the people pursuit to U.S., the cosmetics kind is more and more various.At present, face mask of traditional Chinese medicine is one of beauty treatment educational circles effective whitening scheme, and especially some Chinese medicine extraction liquid have the effect of toxin expelling, speckle dispelling, reparation, skin care preferably, also by being applied in facial film gradually.
But because facial film is liquid condition, Chinese medicine extraction liquid is easy to grow mycete, and a lot of face mask of traditional Chinese medicine antiseptic effects in the market are not good, and the shelf-life is short.All can add antiseptic in therefore a lot of face mask of traditional Chinese medicines.Yet a lot of antiseptic in the microorganisms such as kill bacteria, fungus, also can produce zest to skin, even cause erythema and erythra, and the Long Term Contact antiseptic can increase organism material sensitization, cause the danger of anaphylactic reaction.
Iodine propilolic alcohol butyl mephenesin Carbamate (being called for short IPBC) is a kind of novel cosmetic antiseptic, has good fungistatic effect, and dissolubility preferably arranged in surfactant, emulsifying agent, polar solvent, therefore be widely used in resident class and drip washing class cosmetic formulations, other antiseptic such as normal and diazolidinyl urea, hydantoin are used in conjunction with.In China's cosmetics health standard and European Union's regulatory affairs, regulation IPBC limits the use of antiseptic in components of cosmetics, and maximum permission working concentration is 0.05% in cosmetics, and can not be used for oral hygiene and lip product.But in facial film, addition is antiseptic effect and not obvious less than 0.05% the time.Therefore, there is little and antiseptic effect is poor, the shelf-life the is short problem of consumption in the antiseptic that uses in present facial film.Iodine propilolic alcohol butyl mephenesin Carbamate or other antiseptic large usage quantities in the part facial film are also arranged, can be produced pessimal stimulation by skin, with after need to clean facial, use and bother.
Yellow orange is the fruit of rutaceae orange Citrus aurantium.Another name: orange, yellow orange, gold ring, yellow fruit, gold goal, gold orange, swan shell, Fructus Citri sinensis, blood orange, Citrus sinensis Osbeck, sugar orange, Citrus aurantium Linn..Nature and flavor: cool, sweet, sour.Function: promoting the production of body fluid to quench thirst, stomach function regulating spleen invigorating.Composition: edible part 74%.Heat content 197kJ in every 100g, moisture 87.4g, protein 0.8g, fatty 0.2g, dietary fiber 0.6g, carbohydrate 10.5g, carotene 160 μ g, look yellow liquor-saturated equivalent 27 μ g, thiamine 0.05mg, riboflavin 0.04mg, nicotinic acid 0.3mg; Vitamin C 33mg, an E0.56mg supports one's family; Potassium 159mg, sodium 1.2mg, calcium 20mg, magnesium 14mg, ferrum 0.4mg, manganese 0.05mg, zinc 0.14mg, copper 0.03mg, phosphorus 22mg, selenium 0.31 μ g, still contain the organic acid such as citric acid, malic acid, succinic acid.
The yellow orange extract is rich in vitamin C, has whitening free radical resisting antioxidative effect.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of exfoliated yellow orange clean flour film.
Two of technical problem to be solved by this invention provides the preparation method of the clean flour film of above-mentioned exfoliated yellow orange.
The present invention seeks to be achieved through the following technical solutions:
The clean flour film of a kind of exfoliated yellow orange is prepared from according to a conventional method by the raw material of following weight parts:
10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part myristamide CAB, 4-6 part ethanol, 6-8 part LAA, 0.8-2 part yellow orange extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
Wherein, described compound preservative consists of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
, with carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
The clean flour film of described exfoliated yellow orange can adopt industry conventional method to be prepared from.
Further, the present invention also provides the preparation method of the clean flour film of a kind of exfoliated yellow orange, following step, consists of:
Polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, myristamide CAB, ethanol, LAA to stir, be cooled to 40 ℃, add yellow orange extracting solution and compound preservative, stir, can make the clean flour film of described exfoliated yellow orange.
Concrete, in the present invention:
Described polyvinyl alcohol can be selected the cosmetics-stage polyvinyl alcohol, and specifically can select as the trade mark is the polyvinyl alcohol of PVA1788, PVA1799 or PVA2488.
Glycerol has another name called: propylene glycol, English name: Glycerin, molecular formula C
3H
8O
3
The myristamide CAB, English name: MYRISTAMIDOPROPYL BETAINE, CAS accession number: 59272-84-3.
LAA, English name: SODIUM LAUROAMPHOACETATE, CAS accession number: 156028-14-7.
Yellow orange extracting solution of the present invention can pass through commercially available obtaining.Also can adopt following method preparation and obtain: after yellow orange is pulverized, add the deionized water of 6-10 times of weight, soak 1-3 hour, ultrasonic extraction, 10-15 minute, filter, and is centrifugal, discards precipitation with supernatant concentration, makes the yellow orange extracting solution.Preferably, after concentrating, controlling yellow orange extracting solution density is 1.02-1.10g/cm
3
Carnosic acid, molecular formula: C
20H
28O
4, No. CAS: 3650--09-7, source: Labiatae Rosmarinus plant rosemary Rosmarinus officinalis L.
AOB, No. CNS: 04.019, English name: antioxidant of bamboo leaves.AOB extracts from the tender leaf of Phyllostachys (phyllostachys) bamboo, natural, the nutrition take flavone and phenolic compound as effective ingredient, multi-functional food antioxidant.
Nisin also claims nisin, English name: Nisin, and by the synthetic a kind of polypeptide that is formed by 34 aminoacid of streptococcus acidi lactici metabolism, molecular formula C
143H
228O
37N
42S
7Molecular weight is 3348, and nisin consists of water-wet side and hydrophobic side, is typical surfactant, be efficient, nontoxic biological antiseptic, be widely used in the anticorrosion of milk and milk products, fermented beverage, filling food, vegetable protein food, meat and its products at present.
Iodine propilolic alcohol butyl mephenesin Carbamate, English name: 3-Iodo-2-propynyl butylcarbamate, be abbreviated as IPBC, No. CAS: 55406-53-6, molecular formula: C
8H
12INO
2, molecular weight is 281.10.
The present invention uses carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate composite as antiseptic, and antiseptic effect is significantly improved, the long shelf-life of facial film.And, use Compositional antiseptic agent, greatly reduce the consumption of iodine propilolic alcohol butyl mephenesin Carbamate, the consumption of iodine propilolic alcohol butyl mephenesin Carbamate is controlled at below 0.03%, meet the IPBC that stipulates in China's cosmetics health standard and European Union's regulatory affairs and limit the use of antiseptic in components of cosmetics, maximum permission working concentration is 0.05% in cosmetics.Carnosic acid, AOB, nisin are the nontoxic biological antiseptic, be widely used in food service industry, in the present invention, it is diverted to cosmetic mask, can't brings ill effect to human body or skin, and can not produce harmful effect to the stability of facial film.
The using method of the clean flour film of exfoliated yellow orange of the present invention is: before using facial film, first deeply cleaning is facial, again facial film is coated on face, after 15-25 minute, the facial film active substance is absorbed by the skin, the moisture evaporation, form gradually thin film at face, this thin film is peeled off from face, and the dirt on skin of face, scurf also stick on thin film in company with and are eliminated, and it is clean, smooth that face seems.
The clean flour film of exfoliated yellow orange of the present invention, can the deep layer cleaning skin of face, desalinates facial microgroove, makes skin elasticity compact, and the water profit is plentiful.Continue to use, skin water profit is flexible, reproduces youthful vigor.
The clean flour film of exfoliated yellow orange of the present invention, can effectively stop the phenomenons such as the face that causes because of factors such as fatigue, pollution, radiation, drying, air-conditionings is withered and yellow, coarse, improve the colour of skin of facial depth inequality, make skin clean evenly white fast, keep for a long time moistening glossy.
The clean flour film of exfoliated yellow orange of the present invention, adopt carnosic acid, AOB, nisin, the composite antiseptic of iodine propilolic alcohol butyl mephenesin Carbamate, and shelf life of products is long, and can not produce harmful effect to skin.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1
Take each raw material according to corresponding embodiment 1 data in table 1,, with carnosic acid, AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate simple agitation mix homogeneously, can make described compound preservative.
Polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, myristamide CAB, ethanol, LAA to stir, be cooled to 40 ℃, add yellow orange extracting solution and compound preservative, stir, can make the clean flour film of described exfoliated yellow orange.
Wherein, the yellow orange extracting solution in embodiment 1 and Comparative Examples 1-5 adopts following method to be prepared from: after yellow orange is pulverized, add the deionized water of 8 times of weight, soaked 2 hours, ultrasonic extraction, 12 minutes, filter, centrifugal, discard precipitation with supernatant concentration, after concentrating, making density is 1.06g/cm
3The yellow orange extracting solution.
Table 1: face pack prescription list position: kilogram
| ? | Embodiment 1 | Comparative Examples 1 | Comparative Examples 2 | Comparative Examples 3 | Comparative Examples 4 | Comparative Examples 5 |
| Deionized water | 100 | 100 | 100 | 100 | 100 | 100 |
| PVA-124 88 | 12 | 12 | 12 | 12 | 12 | 12 |
| Glycerol | 10 | 10 | 10 | 10 | 10 | 10 |
| The myristamide CAB | 1 | 1 | 1 | 1 | 1 | 1 |
| Ethanol | 5 | 5 | 5 | 5 | 5 | 5 |
| LAA | 7 | 7 | 7 | 7 | 7 | 7 |
| The yellow orange extracting solution | 1 | 1 | 1 | 1 | 1 | 1 |
| Carnosic acid | 0.01 | / | / | / | / | / |
| AOB | 0.02 | 0.02 | 0.02 | 0.03 | / | / |
| Nisin | 0.01 | 0.01 | 0.02 | 0.01 | / | / |
| Iodine propilolic alcohol butyl mephenesin Carbamate | 0.01 | 0.02 | 0.01 | 0.01 | / | / |
| Methyl parahydroxybenzoate | / | / | / | / | 0.05 | / |
Comparative Examples 1
Take each raw material according to corresponding Comparative Examples 1 data in table 1.Adopt the described method of embodiment 1 to prepare the clean flour film of exfoliated yellow orange of Comparative Examples 1.
Comparative Examples 2
Take each raw material according to corresponding Comparative Examples 2 data in table 1.Adopt the described method of embodiment 1 to prepare the clean flour film of exfoliated yellow orange of Comparative Examples 2.
Comparative Examples 3
Take each raw material according to corresponding Comparative Examples 3 data in table 1.Adopt the described method of embodiment 1 to prepare the clean flour film of exfoliated yellow orange of Comparative Examples 3.
Comparative Examples 4
Take each raw material according to corresponding Comparative Examples 4 data in table 1.Adopt the described method of embodiment 1 to prepare the clean flour film of exfoliated yellow orange of Comparative Examples 4.
Comparative Examples 5
Take each component according to Comparative Examples 5 data corresponding in table 1, adopt the described method of embodiment 1, namely obtain the clean flour film of exfoliated yellow orange of Comparative Examples 5.
Test case 1
The clean flour film of exfoliated yellow orange that respectively embodiment 1 and Comparative Examples 1-5 is made, carry out fill with the dark brown vial, opens wide bottle cap, is placed under 40 ℃ of ambient temperatures, relative humidity 85% environment, continues to observe and test, and concrete outcome sees the following form.Detect the microorganism level, concrete test item, detection method and examination criteria carry out according to QB/T2872-2007.
| ? | Observe phenomena |
| Embodiment 1 | No abnormality seen after 60 days, abnormal smells from the patient is pure |
| Comparative Examples 1 | After 50 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 2 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 3 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 4 | After 40 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
| Comparative Examples 5 | After 5 days, mildew occurs, microorganism exceeds standard, and gives out unhappy abnormal smells from the patient |
The antiseptic methyl parahydroxybenzoate that uses in Comparative Examples 4 is one of the most frequently used cosmetics preservative in this area.Belong to antiseptic phenols, generally effective to mycete, yeast, antibacterial, the effect that suppresses growth of microorganism is arranged, effectively extend the shelf-life (40 days shelf-lifves under test condition of the present invention) of cosmetics after adding, but long-term this antiseptic of excessive use, the Diazolidinyl Urea epidermis cell, cause the epidermis transition aging.
Can significantly be drawn by test data, the embodiment of the present invention 1 is used carnosic acid, AOB, nisin and the composite Synergistic of iodine propilolic alcohol butyl mephenesin Carbamate, and antiseptic effect (60 days shelf-lifves under test condition of the present invention) obviously is better than Comparative Examples 1-3 and only adopts AOB, nisin and iodine propilolic alcohol butyl mephenesin Carbamate three composite (in the shelf-life under test condition of the present invention below 50 days).
The facial film of the embodiment of the present invention 1 is placed in accelerated test under 40 ℃ of ambient temperatures, relative humidity 85% environment at opening, can reach 60 days antiseptic effects, the long shelf-life of facial film, and conversion shady and cool dry its shelf-life of place under sealing state far surpasses 3 years.
Test case 2
With CorneometerCM820 moisture of skin measuring instrument, measure the skin surface moisture at tested position, tested position is respectively the abundant forehead of sebaceous gland.Operating ambient temperature is 22-24 ℃, and relative humidity is 46%-55%, and the unit of skin moisture content is au (arbitraryunit).Female consumer forehead skin to a use embodiment of the present invention 1 is tested, and concrete data see the following form.
| ? | Before use, au | After use, au | Used au rear 1 hour |
| Embodiment 1 | 37.3 | 88.1 | 82.3 |
The above; it is only the specific embodiment of the present invention; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work, within all should being encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (3)
1. clean flour film of exfoliated yellow orange, it is characterized in that, raw material by following weight parts is prepared from according to a conventional method: 10-14 part polyvinyl alcohol, 8-12 part glycerol, 0.8-1.2 part myristamide CAB, 4-6 part ethanol, 6-8 part LAA, 0.8-2 part yellow orange extracting solution, 0.03-0.08 part compound preservative, 100 parts of deionized waters.
2. the clean flour film of exfoliated yellow orange as claimed in claim 1, it is characterized in that, described compound preservative consists of by weight following component: 1-3 part carnosic acid, 3-5 part AOB, 1-3 part nisin, 1-3 part iodine propilolic alcohol butyl mephenesin Carbamate.
3. the preparation method of the clean flour film of exfoliated yellow orange as claimed in claim 2, it is characterized in that, formed by following step: polyvinyl alcohol is added in deionized water, be heated to 70-90 ℃, dissolve, be cooled to 45-55 ℃, add glycerol, myristamide CAB, ethanol, LAA to stir, be cooled to 40 ℃, add yellow orange extracting solution and compound preservative, stir.
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