CN103361098A - Method for preparing instant-dissolving wood vinegar powder - Google Patents
Method for preparing instant-dissolving wood vinegar powder Download PDFInfo
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- CN103361098A CN103361098A CN2012100903659A CN201210090365A CN103361098A CN 103361098 A CN103361098 A CN 103361098A CN 2012100903659 A CN2012100903659 A CN 2012100903659A CN 201210090365 A CN201210090365 A CN 201210090365A CN 103361098 A CN103361098 A CN 103361098A
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- wood vinegar
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- vinegar
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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Abstract
The invention discloses a method for preparing instant-dissolving wood vinegar powder, relating to instant-dissolving powder preparations. According to the method, the wood vinegar powder is prepared from wood vinegar liquid. The method is characterized by comprising the steps of: putting the wood vinegar liquid in a long-necked test phial, heating in a water bath, and cooling the water bath to the temperature below 40 DEG C when the wood vinegar liquid is concentrated to the volume which is 45-60% of the original volume, wherein the heating temperature is 60-85 DEG C; then mixing the concentrated wood vinegar liquid with montmorillonite powder according to the weight ratio of 1: (1-0.05); cooking to the temperature of 100 DEG C, and then, homogenizing; and carrying out spray drying on the homogenized wood vinegar starch, cooling, and then, packaging, thereby obtaining finished products. The method has the beneficial effects that wood vinegar is heated by the water bath, so that the loss of soluble solids in the wood vinegar is avoided, the nutritional ingredients in the wood vinegar are preserved as much as possible, and the product yield of wood vinegar raw materials is increased; due to water-bath heating, the product yield of the raw materials and the solubility of the products are increased, and the instant solubility of the spray products is further improved; and the method disclosed by the invention is simple and convenient and is simple in operation.
Description
Technical field
The present invention relates to a kind of instant powder, specifically the making method of instant wooden vinegar powder.
Background technology
Wood vinegar is from the natural acetic acid composition in the timber, and timber extracts fat liquid through behind the high-temperature firing, extracts powder through purifying again, has exactly the wooden vinegar of nourishing function.Wood vinegar can be made environment-friendly deodorant agent, Snow Agent, insecticide etc.Wood vinegar is the byproduct during a kind of biomass of developing are used.
The common wood vinegar of existing market, and the preparation method of wood vinegar is simple, uses extensively, and wood vinegar contains higher acetic acid and phenols, water, reach the mineral substance such as K, Ca, Mg, Zn, Ge, Mn, Fe, contain in addition Vitamin B1 hcl and B2, organic composition acetic acid accounts for more than 47%; These product have stronger sterilization, antibiotic function under high density; Under lower concentration, can suppress the breeding of miscellaneous bacteria, have the effects such as fungi-proofing, insect protected; But since commercially available its be liquid, have the shortcomings such as the accumulating of being difficult for.Therefore, need a kind of wooden vinegar pulvis, so that its shelf time is long; It is namely water-soluble to add in use solution, and simple and practical, is widely used.
Summary of the invention
The present invention aims to provide the making method of instant wooden vinegar powder, and the method utilizes wood vinegar to prepare wooden vinegar pulvis, and the wooden vinegar powder of making has better instantly-soluble and flowability, has strengthened simultaneously the product nutritive ingredient, and is that product has the long quality guaranteed period.
For achieving the above object, the making method of instant wooden vinegar powder of the present invention is characterized in that:
One, wood vinegar is placed long-neck test tube bottle heating in water bath, Heating temperature is 60～85 ℃, when wood vinegar be concentrated into original volume 45～60% the time, then water-bath is but to below 40 ℃;
Two, the wood vinegar after then step 1 is concentrated mixes with montmorillonite powder, and the combined amount of wood vinegar and montmorillonite powder is 1: 1～0.05 to be weight ratio;
Three, carry out mashing off after adding montmorillonite powder, boil to 100 ℃ of boilings homogeneous; Wooden vinegar slurry after homogeneous carries out spraying drying, 95～100 ℃ of the inlet temperature of spray tower, and temperature of outgoing air is not higher than 70 ℃, collects spray product and crosses 20 mesh sieves, packs to get finished product after the cooling.
Described montmorillonite ground 200 mesh sieves.
Described heating in water bath is traditional method, so that vinegar solution is not volatile, and bath temperature avoids too much wood vinegar to contain thing volatilization, sex change at 60～85 ℃.
Described water-bath with wood vinegar be concentrated into original liquid 50% the time, add montmorillonite powder, the volatilization that can slow down solution is so that wood vinegar is adsorbed in the montmorillonite powder surface.
The making method of instant wooden vinegar powder of the present invention, its beneficial effect is: the present invention avoids the loss of soluble solid in the wooden vinegar with heating in water bath wood vinegar, and the nutritive ingredient in the reserve vinegar most possibly improves the yield rate of wooden vinegar raw material; Heating in water bath has improved the solubleness of yield rate and the product of raw material, further improves the instantly-soluble of spray product; The inventive method is easy, and is simple to operate.
Embodiment
Following examples are that the present invention further goes out to set forth.
Embodiment 1
One, wood vinegar is placed long-neck test tube bottle heating in water bath, Heating temperature is 70 ℃, when wood vinegar be concentrated into original volume 50% the time, then water-bath is but to below 40 ℃;
Two, the wood vinegar after then step 1 is concentrated mixes with montmorillonite powder, and described montmorillonite ground 200 mesh sieves, the combined amount of wood vinegar and montmorillonite powder be 1: 0.05 be weight ratio;
Three, carry out mashing off after adding montmorillonite powder, boil to 100 ℃ of boilings homogeneous; Wooden vinegar slurry after homogeneous carries out spraying drying, 95 ℃ of the inlet temperature of spray tower, and temperature of outgoing air is not higher than 70 ℃, collects spray product and crosses 20 mesh sieves, packs to get finished product after the cooling.
Claims (2)
1. the making method of instant wooden vinegar powder, it is characterized in that: wood vinegar is placed long-neck test tube bottle heating in water bath, and Heating temperature is 60～85 ℃, when wood vinegar be concentrated into original volume 45～60% the time, then water-bath is but to below 40 ℃; Then the wood vinegar after step 1 is concentrated mixes with montmorillonite powder, and the combined amount of wood vinegar and montmorillonite powder is 1: 1～0.05 to be weight ratio; Carry out mashing off after adding montmorillonite powder, boil to 100 ℃ of boilings homogeneous; Wooden vinegar slurry after homogeneous carries out spraying drying, 95～100 ℃ of the inlet temperature of spray tower, and temperature of outgoing air is not higher than 70 ℃, collects spray product and crosses 20 mesh sieves, packs to get finished product after the cooling.
2. the making method of instant wooden vinegar powder as claimed in claim 1, it is characterized in that: described montmorillonite ground 200 mesh sieves.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100903659A CN103361098A (en) | 2012-03-30 | 2012-03-30 | Method for preparing instant-dissolving wood vinegar powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100903659A CN103361098A (en) | 2012-03-30 | 2012-03-30 | Method for preparing instant-dissolving wood vinegar powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103361098A true CN103361098A (en) | 2013-10-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012100903659A Pending CN103361098A (en) | 2012-03-30 | 2012-03-30 | Method for preparing instant-dissolving wood vinegar powder |
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| CN (1) | CN103361098A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112159280A (en) * | 2020-09-30 | 2021-01-01 | 山西中农化生物技术有限公司 | Powder soil conditioner and preparation method thereof |
-
2012
- 2012-03-30 CN CN2012100903659A patent/CN103361098A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112159280A (en) * | 2020-09-30 | 2021-01-01 | 山西中农化生物技术有限公司 | Powder soil conditioner and preparation method thereof |
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| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20131023 |