CN103351675A - Washing resistive exterior wall coating and preparation method thereof - Google Patents
Washing resistive exterior wall coating and preparation method thereof Download PDFInfo
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- CN103351675A CN103351675A CN2013102476130A CN201310247613A CN103351675A CN 103351675 A CN103351675 A CN 103351675A CN 2013102476130 A CN2013102476130 A CN 2013102476130A CN 201310247613 A CN201310247613 A CN 201310247613A CN 103351675 A CN103351675 A CN 103351675A
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- 238000000576 coating method Methods 0.000 title claims abstract description 29
- 239000011248 coating agent Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims description 7
- 238000005406 washing Methods 0.000 title abstract description 3
- 239000000839 emulsion Substances 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 15
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000440 bentonite Substances 0.000 claims abstract description 7
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 239000003365 glass fiber Substances 0.000 claims abstract description 7
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims abstract description 4
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 claims abstract description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 36
- 238000003756 stirring Methods 0.000 claims description 15
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- 238000004581 coalescence Methods 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical group O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- -1 dimethyl dimercapto 2-ethyl hexyl ethanoate tin Chemical compound 0.000 claims description 3
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims description 3
- 150000002170 ethers Chemical class 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 239000005543 nano-size silicon particle Substances 0.000 claims description 3
- 239000002105 nanoparticle Substances 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 239000001632 sodium acetate Substances 0.000 claims description 3
- 235000017281 sodium acetate Nutrition 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 abstract description 3
- 230000001070 adhesive effect Effects 0.000 abstract description 3
- 238000005034 decoration Methods 0.000 abstract description 3
- 229910001385 heavy metal Inorganic materials 0.000 abstract description 2
- 238000000034 method Methods 0.000 abstract description 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- DMAXMXPDVWTIRV-UHFFFAOYSA-N 2-(2-phenylethyl)phenol Chemical compound OC1=CC=CC=C1CCC1=CC=CC=C1 DMAXMXPDVWTIRV-UHFFFAOYSA-N 0.000 abstract 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 abstract 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 abstract 1
- 239000001768 carboxy methyl cellulose Substances 0.000 abstract 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 239000002932 luster Substances 0.000 abstract 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 abstract 1
- 229910052753 mercury Inorganic materials 0.000 abstract 1
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract 1
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 abstract 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 abstract 1
- 229920001909 styrene-acrylic polymer Polymers 0.000 abstract 1
- PKDCQJMRWCHQOH-UHFFFAOYSA-N triethoxysilicon Chemical compound CCO[Si](OCC)OCC PKDCQJMRWCHQOH-UHFFFAOYSA-N 0.000 abstract 1
- 239000003039 volatile agent Substances 0.000 abstract 1
- 239000003973 paint Substances 0.000 description 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 230000004087 circulation Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000001846 repelling effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention relates to an exterior wall coating which comprises the following raw materials in parts by weight: 80-90 parts of a water based acrylic emulsion, 15-20 parts of a styrene-acrylic emulsion, 30-60 parts of nano bentonite, 3-4 parts of sodium carboxymethylcellulose, 2-3 parts of butyl methacrylate, 1-2 parts of dimethyl dimercaptoacetic tin isooctylate, 0.6-1 part of phenethyl phenol polyoxyethylene ether, 0.5-1 part of glass fiber, 0.8-1 part of 1, 2-di(triethoxy silicon base) ethane, 0.1-0.2 part of tributyl phosphate, 3-5 parts of a coalescing agent and 10-20 parts of deionized water. The produced coating disclosed by the invention is less in raw material loss, less in gel generation, simple in process, hard in film, good in luster, strong in impact resistance, difficult to crack, flexible in texture, strong in decoration, high in weather resistance and washing resistance, strong in adhesive force, long in service life, and free from special smell, heavy metals such as mercury and lead, and formaldehyde volatiles, so that the coating is in accordance with technical demand of environmental-friendly coatings. The coalescing agent is added, so that the coating is very high in stability, and efficient in adhesiveness and film-forming property. The compactness of the coating film is increased, and the film-forming quality is improved, so that a film has the advantages of strong adhesive force, no holes and rifts, uniform compactness and the like.
Description
Technical field
The present invention relates generally to a kind of coating, relates in particular to a kind of washability exterior coating and preparation method thereof.
Background technology
In recent years; along with the raising of living standards of the people and the development of society; people are to the selection pay attention to day by day of building decoration coating, and are more simple better to the construction requirement of coating, for particularly in exterior coating; not only rest in the most basic protection to ground; decorative effect to coating is had higher requirement, and exterior coating requires to have water repelling property, requires to have from washing property; it is hard and smooth, dirty once rushing that paint film is wanted.
But the acrylic coating of throwing on the domestic market exists, and gloss is low, poor adhesive force, winter hardiness are poor, not water-fast, water vapour, soda acid, salts solution and organic polar solvent, poor flexibility under the room temperature, the shortcoming such as wear no resistance, and high temperature easily returns sticking, fragile under low temperature splitting, cause coating easily to ftracture, peel off, rainwater etc. easily infiltrate metope, corrosion body of wall, and this not only affects the beautiful decoration of buildings, and will reduce the work-ing life of buildings.
Summary of the invention
The object of the invention is exactly in order to remedy the defective of prior art, exterior coating that a kind of paint film is stable, glossiness is good, tolerance is strong and preparation method thereof to be provided.
The present invention is achieved by the following technical solutions:
A kind of washability exterior coating, it is comprised of the raw material of following weight parts:
Aqueous acrylic emulsion 80-90, benzene emulsion 15-20, nano-bentonite 30-60, Xylo-Mucine 3-4, butyl methacrylate 2-3, dimethyl dimercapto 2-ethyl hexyl ethanoate tin 1-2, styroyl phenol polyethenoxy ether 0.6-1, glass fibre 0.5-1,1, two (triethoxy is silica-based) ethane 0.8-1 of 2-, tributyl phosphate 0.1-0.2, film coalescence aid 3-5, deionized water 10-20;
Described film coalescence aid is comprised of the raw material of following weight parts:
Nano silicon 30-40, polyvinyl alcohol 4-6, vinyltriethoxysilane 6-10, alkylphenol Polyoxyalkylene ethers 0.8-1, benzene emulsion 3-4, nano-sized carbon 1-2;
Polyvinyl alcohol is joined in the 4-5 times of water, be steam heated to 95-100 ℃, stirring and dissolving adds benzene emulsion, and reducing temperature is 60-70 ℃, constant temperature stirred 3-4 minute, add each raw material of residue, low speed 300-400 rev/min was disperseed 2-3 minute, and 100-120 ℃ of insulation left standstill 1-2 hour, be cooled to normal temperature, namely get described film coalescence aid.
A kind of preparation method of washability exterior coating may further comprise the steps:
The butyl methacrylate of above-mentioned weight part is joined in the benzene emulsion, add the styroyl phenol polyethenoxy ether after fully stirring, it is 90-100 ℃ of lower dispersed with stirring 3-4 minute in temperature, be incubated 20-30 minute, be cooled to normal temperature, add Xylo-Mucine, 500-600 rev/min was stirred 6-8 minute; Add aqueous acrylic emulsion, deionized water, 900-1000 rev/min was stirred 8-10 minute; Add again nano-bentonite, glass fibre, stirred 15-20 minute at 700-800 rev/min; Add each raw material of residue, under 600-700 rev/min speed, fully stir, add acetic acid or sodium acetate, adjusting PH is 8-9, stirs to be described exterior coating.
Advantage of the present invention is:
The coating raw material loss that the present invention produces is few, gel generates few, technique is simple, paint film is hard, glossiness is good, anti-impact force is strong, be not easy cracking, texture is soft, ornamental strong, high weather resisteant is arranged, brushing resistance, strong adhesion, long service life, without special odor, not mercurous, the plumbous heavy metal that waits, formaldehydeless volatile matter, meet the technical requirements of environmental protection coating material, the film coalescence aid of adding has very high stability, efficient binding property, film-forming properties has increased the density of coated membrane, improved quality of forming film, so that rete has strong adhesion, without the cavity, split sunken, the fine and close advantage such as even.
Embodiment
Embodiment 1
A kind of washability exterior coating, it is comprised of the raw material of following weight parts (kilogram):
Aqueous acrylic emulsion 90, benzene emulsion 20, nano-bentonite 46, Xylo-Mucine 4, butyl methacrylate 3, dimethyl dimercapto 2-ethyl hexyl ethanoate tin 2, styroyl phenol polyethenoxy ether 0.6, glass fibre 0.5,1, two (triethoxy the is silica-based) ethane 0.8 of 2-, tributyl phosphate 0.2, film coalescence aid 5, deionized water 20;
Described film coalescence aid is comprised of the raw material of following weight parts:
Nano silicon 40, polyvinyl alcohol 6, vinyltriethoxysilane 10, alkylphenol Polyoxyalkylene ethers 0.8, benzene emulsion 4, nano-sized carbon 1;
Polyvinyl alcohol is joined in 5 times of water, be steam heated to 100 ℃, stirring and dissolving adds benzene emulsion, reducing temperature is 70 ℃, and constant temperature stirred 4 minutes, adds each raw material of residue, 400 rev/mins of dispersions of low speed 3 minutes, 120 ℃ of insulations were left standstill 2 hours, were cooled to normal temperature, namely got described film coalescence aid.
A kind of preparation method of washability exterior coating may further comprise the steps:
The butyl methacrylate of above-mentioned weight part being joined in the benzene emulsion, add the styroyl phenol polyethenoxy ether after fully stirring, is 100 ℃ of lower dispersed with stirring 4 minutes in temperature, be incubated 30 minutes, be cooled to normal temperature, add Xylo-Mucine, 600 rev/mins were stirred 8 minutes; Add aqueous acrylic emulsion, deionized water, 1000 rev/mins were stirred 10 minutes; Add again nano-bentonite, glass fibre, stirred 20 minutes at 800 rev/mins; Add each raw material of residue, under 700 rev/mins speed, fully stir, add acetic acid or sodium acetate, regulating PH is 9, and stirring is described exterior coating.
Performance test:
Paint film appearance is full, smooth, good without lump, glossiness;
Abrasion resistance test: pass through for 10000 times, paint film is without breakage;
The artificial ageing resistance test: 2000 hours non-foaming, do not peel off, flawless;
Temperature-change resistance (5 circulations): without unusual;
Alkali resistance: 200 hours without unusual.
Claims (2)
1. washability exterior coating is characterized in that what it was comprised of the raw material of following weight parts:
Aqueous acrylic emulsion 80-90, benzene emulsion 15-20, nano-bentonite 30-60, Xylo-Mucine 3-4, butyl methacrylate 2-3, dimethyl dimercapto 2-ethyl hexyl ethanoate tin 1-2, styroyl phenol polyethenoxy ether 0.6-1, glass fibre 0.5-1,1, two (triethoxy is silica-based) ethane 0.8-1 of 2-, tributyl phosphate 0.1-0.2, film coalescence aid 3-5, deionized water 10-20;
Described film coalescence aid is comprised of the raw material of following weight parts:
Nano silicon 30-40, polyvinyl alcohol 4-6, vinyltriethoxysilane 6-10, alkylphenol Polyoxyalkylene ethers 0.8-1, benzene emulsion 3-4, nano-sized carbon 1-2;
Polyvinyl alcohol is joined in the 4-5 times of water, be steam heated to 95-100 ℃, stirring and dissolving adds benzene emulsion, and reducing temperature is 60-70 ℃, constant temperature stirred 3-4 minute, add each raw material of residue, low speed 300-400 rev/min was disperseed 2-3 minute, and 100-120 ℃ of insulation left standstill 1-2 hour, be cooled to normal temperature, namely get described film coalescence aid.
2. the preparation method of a washability exterior coating as claimed in claim 1 is characterized in that may further comprise the steps:
The butyl methacrylate of above-mentioned weight part is joined in the benzene emulsion, add the styroyl phenol polyethenoxy ether after fully stirring, it is 90-100 ℃ of lower dispersed with stirring 3-4 minute in temperature, be incubated 20-30 minute, be cooled to normal temperature, add Xylo-Mucine, 500-600 rev/min was stirred 6-8 minute; Add aqueous acrylic emulsion, deionized water, 900-1000 rev/min was stirred 8-10 minute; Add again nano-bentonite, glass fibre, stirred 15-20 minute at 700-800 rev/min; Add each raw material of residue, under 600-700 rev/min speed, fully stir, add acetic acid or sodium acetate, adjusting PH is 8-9, stirs to be described exterior coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310247613.0A CN103351675B (en) | 2013-06-20 | 2013-06-20 | A kind of washability exterior coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310247613.0A CN103351675B (en) | 2013-06-20 | 2013-06-20 | A kind of washability exterior coating and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103351675A true CN103351675A (en) | 2013-10-16 |
| CN103351675B CN103351675B (en) | 2015-12-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310247613.0A Active CN103351675B (en) | 2013-06-20 | 2013-06-20 | A kind of washability exterior coating and preparation method thereof |
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| Country | Link |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103602165A (en) * | 2013-11-19 | 2014-02-26 | 青岛广联达精密机械有限公司 | High-viscosity waterproof coating |
| CN103756417A (en) * | 2013-12-27 | 2014-04-30 | 安徽省美域节能环保技术应用有限公司 | Wear-resistant coating for external wall and preparation method thereof |
| CN104119732A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Architectural water-resistant paint |
| CN104119757A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Waterproof paint for exterior wall |
| CN104119755A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Anti-crack waterproof coating |
| CN104119756A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Low-temperature-resistant water-resistant paint |
| CN104327565A (en) * | 2014-10-23 | 2015-02-04 | 招远鸿瑞印染有限公司 | Preparation of water-based paint |
| CN104356776A (en) * | 2014-09-03 | 2015-02-18 | 天长市开林化工有限公司 | Anti-wear smooth internal wall coating |
| CN106280594A (en) * | 2016-08-17 | 2017-01-04 | 柳州市亿廷贸易有限责任公司 | The preparation method of washability coating |
| CN107236374A (en) * | 2017-06-02 | 2017-10-10 | 安徽喜宝高分子材料有限公司 | A kind of emulsion paint with excellent abrasion resistance |
| CN114672201A (en) * | 2020-12-24 | 2022-06-28 | 湖南腾丰铸造有限公司 | Waterproof coating |
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| US20040134378A1 (en) * | 2003-01-09 | 2004-07-15 | Batdorf Vernon Harland | Protective barrier coating composition |
| CN101429367A (en) * | 2007-11-06 | 2009-05-13 | 苏华远 | Special-purpose cement paint for exterior wall |
| CN101857752A (en) * | 2010-05-28 | 2010-10-13 | 中华制漆（深圳）有限公司 | Aqueous exterior wall coating material with high solid content and low viscosity |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103602165B (en) * | 2013-11-19 | 2016-03-23 | 青岛祥嘉知识产权服务有限公司 | A kind of full-bodied waterproof paint |
| CN103602165A (en) * | 2013-11-19 | 2014-02-26 | 青岛广联达精密机械有限公司 | High-viscosity waterproof coating |
| CN103756417A (en) * | 2013-12-27 | 2014-04-30 | 安徽省美域节能环保技术应用有限公司 | Wear-resistant coating for external wall and preparation method thereof |
| CN104119732A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Architectural water-resistant paint |
| CN104119757A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Waterproof paint for exterior wall |
| CN104119755A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Anti-crack waterproof coating |
| CN104119756A (en) * | 2014-06-26 | 2014-10-29 | 安徽快来防水防腐有限公司 | Low-temperature-resistant water-resistant paint |
| CN104356776A (en) * | 2014-09-03 | 2015-02-18 | 天长市开林化工有限公司 | Anti-wear smooth internal wall coating |
| CN104327565A (en) * | 2014-10-23 | 2015-02-04 | 招远鸿瑞印染有限公司 | Preparation of water-based paint |
| CN106280594A (en) * | 2016-08-17 | 2017-01-04 | 柳州市亿廷贸易有限责任公司 | The preparation method of washability coating |
| CN107236374A (en) * | 2017-06-02 | 2017-10-10 | 安徽喜宝高分子材料有限公司 | A kind of emulsion paint with excellent abrasion resistance |
| CN107236374B (en) * | 2017-06-02 | 2018-08-24 | 安徽喜宝高分子材料有限公司 | A kind of emulsion paint with excellent abrasion resistance |
| CN114672201A (en) * | 2020-12-24 | 2022-06-28 | 湖南腾丰铸造有限公司 | Waterproof coating |
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| Publication number | Publication date |
|---|---|
| CN103351675B (en) | 2015-12-23 |
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Denomination of invention: A washable exterior wall coating and its preparation method Effective date of registration: 20231026 Granted publication date: 20151223 Pledgee: Lai An county Jinan financing Company limited by guarantee Pledgor: CHUZHOU BEST NEW BUILDING MATERIAL CO.,LTD. Registration number: Y2023980062875 |