CN103343487A - High-end cigarette paper containing black vanilla extract and preparation method thereof - Google Patents
High-end cigarette paper containing black vanilla extract and preparation method thereof Download PDFInfo
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- CN103343487A CN103343487A CN2013103166930A CN201310316693A CN103343487A CN 103343487 A CN103343487 A CN 103343487A CN 2013103166930 A CN2013103166930 A CN 2013103166930A CN 201310316693 A CN201310316693 A CN 201310316693A CN 103343487 A CN103343487 A CN 103343487A
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- Prior art keywords
- cigarette paper
- black vanilla
- extract
- black
- vanilla extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 235000009499 Vanilla fragrans Nutrition 0.000 title claims abstract description 80
- 235000012036 Vanilla tahitensis Nutrition 0.000 title claims abstract description 80
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 78
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 244000263375 Vanilla tahitensis Species 0.000 title claims abstract 22
- 238000000605 extraction Methods 0.000 title abstract description 7
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000011248 coating agent Substances 0.000 claims abstract description 19
- 238000000576 coating method Methods 0.000 claims abstract description 19
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 15
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 14
- 229940073505 ethyl vanillin Drugs 0.000 claims abstract description 13
- 239000000243 solution Substances 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 238000010992 reflux Methods 0.000 claims abstract description 6
- 239000012530 fluid Substances 0.000 claims description 18
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 239000012141 concentrate Substances 0.000 claims description 5
- 238000010790 dilution Methods 0.000 claims description 5
- 239000012895 dilution Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 3
- 238000002203 pretreatment Methods 0.000 claims description 3
- 230000000391 smoking effect Effects 0.000 abstract description 14
- 235000009508 confectionery Nutrition 0.000 abstract description 13
- 239000003205 fragrance Substances 0.000 abstract description 11
- 238000000034 method Methods 0.000 abstract description 9
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 abstract 2
- 235000012141 vanillin Nutrition 0.000 abstract 2
- 244000068988 Glycine max Species 0.000 abstract 1
- 235000010469 Glycine max Nutrition 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 230000002708 enhancing effect Effects 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 abstract 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- 230000001502 supplementing effect Effects 0.000 abstract 1
- 239000002023 wood Substances 0.000 abstract 1
- 244000290333 Vanilla fragrans Species 0.000 description 58
- 238000004519 manufacturing process Methods 0.000 description 15
- 241000208125 Nicotiana Species 0.000 description 11
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 11
- 238000002474 experimental method Methods 0.000 description 7
- 239000002304 perfume Substances 0.000 description 7
- 235000013599 spices Nutrition 0.000 description 6
- 239000007789 gas Substances 0.000 description 5
- 230000002045 lasting effect Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 244000046052 Phaseolus vulgaris Species 0.000 description 4
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 4
- 239000006071 cream Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229940089401 xylon Drugs 0.000 description 3
- 230000035807 sensation Effects 0.000 description 2
- 235000019615 sensations Nutrition 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 229930183419 Irisone Natural products 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- 235000009470 Theobroma cacao Nutrition 0.000 description 1
- UZFLPKAIBPNNCA-BQYQJAHWSA-N alpha-ionone Chemical compound CC(=O)\C=C\C1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-BQYQJAHWSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001303 quality assessment method Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229940098465 tincture Drugs 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a preparation method of cigarette paper containing a black vanilla extract. The method comprises the following steps of: uniformly cutting black vanilla and diluting vanillin and ethyl vanillin into 5wt%-15wt% of solutions by propanediol respectively; uniformly mixing the vanillin solution with the ethyl vanillin according to a volume ratio of (1-3) to 1; uniformly spraying the mixed solution to the surface of the black vanilla and baking for 1-3 hours at the temperature of 30+/-2 DEG C; performing heating reflux extraction by ethanol; performing low-temperature concentration to obtain the black vanilla extract; adding the black vanilla extract into a coating solution, and stirring by a high-speed dispersing machine for uniformly mixing to finally prepare the high-end cigarette paper containing the black vanilla extract. The prepared cigarette paper can be used for effectively covering wood gas of the cigarette paper, supplementing fresh and sweet paste fragrance, sweet fragrance and soybean fragrance, enhancing cigarette fragrance and improving the useful value and the smoking quality of the cigarette paper.
Description
Technical field
The present invention relates to the cigarette preparation field, be specifically related to a kind of high-grade cigarette paper that contains black vanilla extract and preparation method thereof.
Background technology
Cigarette paper belongs to tissue paper, as the cigarette auxiliary material, occupies than consequence in tobacco industry.Cigarette paper accounts for 5% of Cigarette weight, and the fiber in the cigarette paper accounts for more than 70% of overall weight, because it participates in burning directly, produces xylon gas in combustion process, and mouthfeel is sour and astringent, has influenced sucking quality.
Black vanilla is called as " the vanilla queen that 21 century causes a sensation most ", and its fragrance and cigarette perfume (or spice) are coordinated very much, and it can improve the quality scale of cigarette greatly.For a long time, black vanilla majority all is used for making extract, tincture, medicinal extract for traditional tobacco perfuming, this research in the auxilliary material perfuming aspect of cigarette of black vanilla extract is very few, the xylon gas that the fragrance of black vanilla can effectively be covered cigarette paper, augment fresh and sweet cream perfume (or spice), fragrant and sweet, beans are fragrant, make that cigarette is fragrant to be strengthened, and promoted the use value of cigarette paper and the suction quality of cigarette.
Summary of the invention
Technical problem to be solved by this invention just provides a kind of cigarette paper preparation method who contains black vanilla extract.
For solving the problems of the technologies described above, a kind of cigarette paper preparation method who contains black vanilla extract of the present invention may further comprise the steps:
1) black vanilla pre-treatment: will deceive vanilla and shear evenly;
2) vanillic aldehyde and Ethyl vanillin are diluted to the solution of mass fraction 5 ~ 15% respectively with propylene glycol;
3) with step 2) dilution vanillic aldehyde solution and Ethyl vanillin mix according to volume ratio 1 ~ 3 ︰ 1;
4) mixed liquor with the step 3) preparation evenly is sprayed to black vanilla surface, places under 30 ± 2 ℃ of conditions and toasts 1 ~ 3h; Return to normal temperature after the taking-up;
5) extract with alcohol heating reflux then, obtain extract, with extracting liquid filtering, decompression concentrates and obtains black vanilla extract;
6) black vanilla extract in the step 5) is added in the coating fluid, stir with high speed dispersor, make its even mixing, make the high-grade cigarette paper that contains this extract at last.
Further, in the described step 1), the black vanilla section of being cut into shape, its specification is 1 ~ 1.5cm.
Again further, in the described step 4), mixed liquor accounts for 5% of black vanilla weight in wet base.
Again further, in the described step 5), the volume fraction of ethanol is 70%, and consumption of ethanol is 5 ~ 8 times of black vanilla weight in wet base.
Again further, in the described step 6), black vanilla extract accounts for 0.5 ~ 4.0% of coating fluid gross weight.
Again further, in the described step 6), the high speed dispersor rotating speed is 200 ~ 250 rev/mins.
Black vanilla among the present invention is described as " the vanilla queen that 21 century causes a sensation most " and has fresh and sweet beans perfume (or spice), has cream perfume (or spice), the fragrant and sweet suffering perfume of powder.Have like the sweet blue and white perfume (or spice) of irisone with like the fragrant and sweet gas of cream behind the tobacco fermentation.The fragrance gentleness, lasting is lasting.Can cooperate with tobacco, set off the natural fragrance of tobacco leaf, improve quality, improve flue gas and inhale flavor.Because of expensive, so can only be with being used for high-grade tobacco product; Vanillic aldehyde mainly is present in the vanilla, has the feature breath of dense and sweet vanilla beans, and fragrance is lasting.Coordinate very much with tobacco flavor, give tobacco plentiful soft cigarette fragrant breeze flavor; Ethyl vanillin has obvious and strong fragrant and sweet, as the fragrant and sweet gas of suckling, and lasting is lasting, and for vanillic aldehyde 2.5 times share with vanillic aldehyde, can make fragrance more plentiful.Be the modulation vanilla in tobacco, the important source material of fragrance such as cocoa, consumption is unsuitable excessive.
Beneficial effect of the present invention is:
The present invention carries out pre-treatment by deceiving vanilla, make black vanilla extract, mix with coating fluid afterwards, make the high-grade cigarette paper that contains black vanilla extract at last, the high-grade cigarette paper making technology that contains this extract is simple, the xylon gas that the cigarette paper that makes with the method can effectively be covered cigarette paper, augment fresh and sweet cream perfume (or spice), fragrant and sweet, beans are fragrant, make that cigarette is fragrant to be strengthened, and promoted the use value of cigarette paper and the suction quality of cigarette.The cigarette paper that production contains this extract utilizes current production devices fully, need not production equipment is improved, and operating procedure is simple, difference is produced unit all be suitable for, and can effectively reduce production costs.
The specific embodiment
In order to explain the present invention better, further illustrate main contents of the present invention below in conjunction with specific embodiment, but content of the present invention not only is confined to following examples.
Embodiment 1
Contain the cigarette paper preparation method of black vanilla extract, may further comprise the steps:
To deceive vanilla and shear the section shape that lattice are 1 ~ 1.5cm, it is 10% solution that vanillic aldehyde and Ethyl vanillin are diluted to mass fraction respectively with propylene glycol; Vanillic aldehyde solution and the Ethyl vanillin of dilution are mixed according to volume ratio 3 ︰ 1; Mixed liquor evenly is sprayed to black vanilla surface, places under 30 ± 2 ℃ of conditions and toast 2h; Return to normal temperature after the taking-up; Wherein, mixed liquor accounts for 5% of black vanilla weight in wet base.
The volume fraction of using 5 times of black vanilla weight in wet bases then is 70% alcohol heating reflux extraction; Obtain extract, with extracting liquid filtering, low temperature concentrates and obtains black vanilla extract;
The black vanilla extract of 0.5kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.
Other gets not the cigarette paper that the above-mentioned coating fluid that adds black vanilla extract is made, and makes cigarette sample in contrast with blank pipe tobacco equally, smokes panel test, and smoking result sees Table 1.
Embodiment 2
Contain the cigarette paper preparation method of black vanilla extract, may further comprise the steps:
To deceive vanilla and shear the section shape that lattice are 1 ~ 1.5cm, vanillic aldehyde and Ethyl vanillin will be diluted to the solution of mass fraction 5% with propylene glycol respectively; Vanillic aldehyde solution and the Ethyl vanillin of dilution are mixed according to volume ratio 1 ︰ 1; Mixed liquor evenly is sprayed to black vanilla surface, places under 30 ± 2 ℃ of conditions and toast 3h; Return to normal temperature after the taking-up; Wherein, mixed liquor accounts for 5% of black vanilla weight in wet base.
The volume fraction of using 8 times of black vanilla weight in wet bases then is 70% alcohol heating reflux extraction; Obtain extract, with extracting liquid filtering, low temperature concentrates and obtains black vanilla extract;
The black vanilla extract of 1kg is added in the 100kg coating fluid, is 250 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.
Other gets not the cigarette paper that the above-mentioned coating fluid that adds black vanilla extract is made, and makes cigarette sample in contrast with blank pipe tobacco equally, smokes panel test, and smoking result sees Table 1.
Embodiment 3
Contain the cigarette paper preparation method of black vanilla extract, may further comprise the steps:
To deceive vanilla and shear the section shape that lattice are 1 ~ 1.5cm, it is 15% solution that vanillic aldehyde and Ethyl vanillin are diluted to mass fraction respectively with propylene glycol; Vanillic aldehyde solution and the Ethyl vanillin of dilution are mixed according to volume ratio 2 ︰ 1; Mixed liquor evenly is sprayed to black vanilla surface, places under 30 ± 2 ℃ of conditions and toast 1h; Return to normal temperature after the taking-up; Wherein, mixed liquor accounts for 5% of black vanilla weight in wet base.
The volume fraction of using 5 times of black vanilla weight in wet bases then is 70% alcohol heating reflux extraction; Obtain extract, with extracting liquid filtering, low temperature concentrates and obtains black vanilla extract;
The black vanilla extract of 1kg is added in the 100kg coating fluid, is 225 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.
Other gets not the cigarette paper that the above-mentioned coating fluid that adds black vanilla extract is made, and makes cigarette sample in contrast with blank pipe tobacco equally, smokes panel test, and smoking result sees Table 1.
Embodiment 4
Repeating embodiment 1, the black vanilla extract of 2kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
Embodiment 5
Repeating embodiment 1, the black vanilla extract of 2.5kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
Embodiment 5
Repeating embodiment 1, the black vanilla extract of 2.5kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
Embodiment 5
Repeating embodiment 1, the black vanilla extract of 3kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
Embodiment 6
Repeating embodiment 1, the black vanilla extract of 3kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
Embodiment 7
Repeating embodiment 1, the black vanilla extract of 3.5kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
Embodiment 8
Repeating embodiment 1, the black vanilla extract of 4kg is added in the 100kg coating fluid, is 200 rev/mins high speed dispersor stirring with rotating speed, makes its even mixing, makes the high-grade cigarette paper that contains this extract at last.Make cigarette paper according to conventional production process.Other adding method and experiment condition are constant, and smoking result sees Table 1.
According to the cigarette sensory quality assessment standard among the GB GB 5606.5-2005, cigarette sample to be smoked panel test, smoking result is as shown in table 1.Smoking result shows, the aesthetic quality of each sample score of smokeing panel test is compared the raising that has in various degree with the contrast sample, and wherein example 4, example 5, example 6 action effects are more remarkable.
The different sample sensory evaluating smoking of table 1 score contrast table
The present invention will deceive in the vanilla extract adding cigarette paper does not almost have influence to the cigarette paper change color, and the cigarette paper tensile strength does not have obvious change, can satisfy the technological requirement of production of cigarettes fully, and the cigarette paper routine data detects contrast and sees Table 2.
Table 2 cigarette paper routine data detects contrast table
Claims (6)
1. contain the cigarette paper preparation method of black vanilla extract, it is characterized in that: may further comprise the steps:
1) black vanilla pre-treatment: will deceive vanilla and shear evenly;
2) vanillic aldehyde and Ethyl vanillin being diluted to mass fraction respectively with propylene glycol is 5 ~ 15% solution;
3) with step 2) dilution vanillic aldehyde solution and Ethyl vanillin mix according to volume ratio 1 ~ 3 ︰ 1;
4) mixed liquor with the step 3) preparation evenly is sprayed to black vanilla surface, places under 30 ± 2 ℃ of conditions and toasts 1 ~ 3h; Return to normal temperature after the taking-up;
5) extract with alcohol heating reflux then, obtain extract, with extracting liquid filtering, low temperature concentrates and obtains black vanilla extract;
6) black vanilla extract in the step 5) is added in the coating fluid, stir with high speed dispersor, make its even mixing, make the high-grade cigarette paper that contains this extract at last.
2. according to the described cigarette paper preparation method who contains black vanilla extract of claim 1, it is characterized in that: in the described step 1), the black vanilla section of being cut into shape, its specification is 1 ~ 1.5cm.
3. according to claim 1 or the 2 described cigarette paper preparation methods that contain black vanilla extract, it is characterized in that: in the described step 4), mixed liquor accounts for 5% of black vanilla weight in wet base.
4. according to the described cigarette paper preparation method who contains black vanilla extract of claim 1, it is characterized in that: in the described step 5), the volume fraction of ethanol is 70%, and consumption of ethanol is 5 ~ 8 times of black vanilla weight in wet base.
5. according to the described cigarette paper preparation method who contains black vanilla extract of claim 1, it is characterized in that: in the described step 6), black vanilla extract accounts for 0.5 ~ 4.0% of coating fluid gross weight.
6. according to the described cigarette paper preparation method who contains black vanilla extract of claim 5, it is characterized in that: in the described step 6), the high speed dispersor rotating speed is 200 ~ 250 rev/mins.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310316693.0A CN103343487B (en) | 2013-07-25 | 2013-07-25 | High-end cigarette paper containing black vanilla extract and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310316693.0A CN103343487B (en) | 2013-07-25 | 2013-07-25 | High-end cigarette paper containing black vanilla extract and preparation method thereof |
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| CN103343487A true CN103343487A (en) | 2013-10-09 |
| CN103343487B CN103343487B (en) | 2015-07-22 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104480791A (en) * | 2014-11-11 | 2015-04-01 | 湖北中烟工业有限责任公司 | Temperature-sensitive low ignition propensity cigarette paper, and preparation method thereof |
| CN107474959A (en) * | 2017-06-09 | 2017-12-15 | 珠海市美绿达香料有限公司 | A kind of spices and its preparation method and application |
| CN107905036A (en) * | 2017-11-17 | 2018-04-13 | 高邮市卫星卷烟材料有限公司 | A kind of production method of long-acting cigarette with sweet taste tipping paper |
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| JPS59129298A (en) * | 1983-01-17 | 1984-07-25 | 長谷川香料株式会社 | Extraction of vanilla flavor |
| US20050115580A1 (en) * | 2003-11-03 | 2005-06-02 | Quinter Phillip F. | Flavored smokeless tobacco and methods of making |
| CN102051266A (en) * | 2010-12-13 | 2011-05-11 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of vanilla perfume for cigarettes |
| CN102876455A (en) * | 2010-12-13 | 2013-01-16 | 云南瑞升烟草技术（集团）有限公司 | Three-step preparation method of vanillic spices for tobacco |
-
2013
- 2013-07-25 CN CN201310316693.0A patent/CN103343487B/en active Active
Patent Citations (4)
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| JPS59129298A (en) * | 1983-01-17 | 1984-07-25 | 長谷川香料株式会社 | Extraction of vanilla flavor |
| US20050115580A1 (en) * | 2003-11-03 | 2005-06-02 | Quinter Phillip F. | Flavored smokeless tobacco and methods of making |
| CN102051266A (en) * | 2010-12-13 | 2011-05-11 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of vanilla perfume for cigarettes |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104480791A (en) * | 2014-11-11 | 2015-04-01 | 湖北中烟工业有限责任公司 | Temperature-sensitive low ignition propensity cigarette paper, and preparation method thereof |
| CN107474959A (en) * | 2017-06-09 | 2017-12-15 | 珠海市美绿达香料有限公司 | A kind of spices and its preparation method and application |
| CN107905036A (en) * | 2017-11-17 | 2018-04-13 | 高邮市卫星卷烟材料有限公司 | A kind of production method of long-acting cigarette with sweet taste tipping paper |
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| CN103343487B (en) | 2015-07-22 |
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