CN103288141A - 一种用于生产三氯化铁的熔化氯化炉及其生产工艺 - Google Patents
一种用于生产三氯化铁的熔化氯化炉及其生产工艺 Download PDFInfo
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- CN103288141A CN103288141A CN2013102185385A CN201310218538A CN103288141A CN 103288141 A CN103288141 A CN 103288141A CN 2013102185385 A CN2013102185385 A CN 2013102185385A CN 201310218538 A CN201310218538 A CN 201310218538A CN 103288141 A CN103288141 A CN 103288141A
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- Prior art keywords
- iron
- chlorination furnace
- furnace
- iron trichloride
- fusing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 title claims abstract description 77
- 238000005660 chlorination reaction Methods 0.000 title claims abstract description 57
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 29
- 230000008018 melting Effects 0.000 title abstract 8
- 238000002844 melting Methods 0.000 title abstract 8
- 238000005516 engineering process Methods 0.000 title description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 123
- 229910052742 iron Inorganic materials 0.000 claims abstract description 62
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 33
- 239000000460 chlorine Substances 0.000 claims description 33
- 229910052801 chlorine Inorganic materials 0.000 claims description 33
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 32
- 238000010521 absorption reaction Methods 0.000 claims description 32
- 238000003723 Smelting Methods 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 13
- 238000002425 crystallisation Methods 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 10
- 229960002089 ferrous chloride Drugs 0.000 claims description 9
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 claims description 9
- 238000004804 winding Methods 0.000 claims description 7
- 239000003513 alkali Substances 0.000 claims description 6
- 238000010924 continuous production Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 abstract 1
- 230000008022 sublimation Effects 0.000 abstract 1
- 238000000859 sublimation Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 37
- 238000004821 distillation Methods 0.000 description 10
- 239000012535 impurity Substances 0.000 description 9
- 238000001514 detection method Methods 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 5
- 238000004062 sedimentation Methods 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000002912 waste gas Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229940013618 stevioside Drugs 0.000 description 1
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 description 1
- 235000019202 steviosides Nutrition 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
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- Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)
Abstract
Description
Claims (9)
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CN201310218538.5A CN103288141B (zh) | 2013-06-04 | 2013-06-04 | 一种用于生产三氯化铁的熔化氯化炉及其生产工艺 |
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CN201310218538.5A CN103288141B (zh) | 2013-06-04 | 2013-06-04 | 一种用于生产三氯化铁的熔化氯化炉及其生产工艺 |
Publications (2)
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CN103288141A true CN103288141A (zh) | 2013-09-11 |
CN103288141B CN103288141B (zh) | 2015-05-20 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103771342A (zh) * | 2013-12-24 | 2014-05-07 | 滨州坤宝化工有限责任公司 | 一种用三氯化铁生产废气生产次氯酸钙的方法 |
CN104326502A (zh) * | 2014-11-06 | 2015-02-04 | 赣州有色冶金研究所 | 气相法制备无水氯化稀土的方法和装置 |
CN106000076A (zh) * | 2015-07-08 | 2016-10-12 | 黄立维 | 一种脱硝用氯化铁固体颗粒及其制备方法及装置 |
CN111701537A (zh) * | 2020-06-24 | 2020-09-25 | 滨州坤宝化工有限责任公司 | 一种三氯化铁的制备装置以及制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3729544A (en) * | 1969-07-17 | 1973-04-24 | Nordstjernan Rederi Ab | Separation of iron by chlorination of a ferro-alloy |
CN101448741A (zh) * | 2006-03-23 | 2009-06-03 | 基斯顿金属回收有限公司 | 由含金属氧化物材料获得的金属氯化物和金属 |
CN202894246U (zh) * | 2012-11-29 | 2013-04-24 | 涂国坚 | 一种用于铸造母合金材料的单流水平连铸机 |
-
2013
- 2013-06-04 CN CN201310218538.5A patent/CN103288141B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3729544A (en) * | 1969-07-17 | 1973-04-24 | Nordstjernan Rederi Ab | Separation of iron by chlorination of a ferro-alloy |
CN101448741A (zh) * | 2006-03-23 | 2009-06-03 | 基斯顿金属回收有限公司 | 由含金属氧化物材料获得的金属氯化物和金属 |
CN202894246U (zh) * | 2012-11-29 | 2013-04-24 | 涂国坚 | 一种用于铸造母合金材料的单流水平连铸机 |
Non-Patent Citations (6)
Title |
---|
倪如宝等: "无氧铜杆连铸机组连接式分体炉的构思和实践", 《江苏冶金》, no. 5, 31 December 1995 (1995-12-31), pages 32 - 33 * |
王兆绪: "浅议无水三氯化铁生产中的几个问题", 《中国氯碱》, no. 1, 31 December 1991 (1991-12-31), pages 38 - 39 * |
蚌埠自来水厂等: "《三氯化铁生产工艺》", 31 March 1972, article "火法生产三氯化铁", pages: 2-3 * |
马慧娟: "《钛冶金学》", 31 January 1982, article "氯化过程的三废回收处理", pages: 99-100 * |
高玉兵等: "无水三氯化铁生产中悬料问题探讨", 《氯碱工业》, vol. 45, no. 8, 31 August 2009 (2009-08-31) * |
黄宁军: "分连体炉在无氧铜杆生产线上的应用", 《电线电缆》, no. 2, 30 April 2001 (2001-04-30), pages 42 - 44 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103771342A (zh) * | 2013-12-24 | 2014-05-07 | 滨州坤宝化工有限责任公司 | 一种用三氯化铁生产废气生产次氯酸钙的方法 |
CN104326502A (zh) * | 2014-11-06 | 2015-02-04 | 赣州有色冶金研究所 | 气相法制备无水氯化稀土的方法和装置 |
CN104326502B (zh) * | 2014-11-06 | 2015-11-18 | 赣州有色冶金研究所 | 气相法制备无水氯化稀土的方法和装置 |
CN106000076A (zh) * | 2015-07-08 | 2016-10-12 | 黄立维 | 一种脱硝用氯化铁固体颗粒及其制备方法及装置 |
CN111701537A (zh) * | 2020-06-24 | 2020-09-25 | 滨州坤宝化工有限责任公司 | 一种三氯化铁的制备装置以及制备方法 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: A melting chlorination furnace for producing ferric chloride and its production process Effective date of registration: 20210115 Granted publication date: 20150520 Pledgee: Agricultural Bank of China Limited by Share Ltd. Binzhou Zhanhua sub branch Pledgor: BINZHOU KUN BAO CHEMICAL Co.,Ltd. Registration number: Y2021370000006 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
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Date of cancellation: 20220214 Granted publication date: 20150520 Pledgee: Agricultural Bank of China Limited by Share Ltd. Binzhou Zhanhua sub branch Pledgor: BINZHOU KUN BAO CHEMICAL CO.,LTD. Registration number: Y2021370000006 |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
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Granted publication date: 20150520 |