CN103272646A - 用于制备L-薄荷醇中间体d-香茅醛的催化剂及其制备方法 - Google Patents
用于制备L-薄荷醇中间体d-香茅醛的催化剂及其制备方法 Download PDFInfo
- Publication number
- CN103272646A CN103272646A CN201310207962XA CN201310207962A CN103272646A CN 103272646 A CN103272646 A CN 103272646A CN 201310207962X A CN201310207962X A CN 201310207962XA CN 201310207962 A CN201310207962 A CN 201310207962A CN 103272646 A CN103272646 A CN 103272646A
- Authority
- CN
- China
- Prior art keywords
- catalyst
- binap
- menthol
- citronellal
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
反应时间(h) | 转换率(%) | 收率b(%) | |
Run1 | 15.0 | 100 | 99 |
Run2 | 15.0 | 100 | 99 |
Run3 | 18.0 | 100 | 99 |
Run4 | 18.0 | 100 | 98 |
Run5 | 18.0 | 100 | 98 |
Run6 | 18.0 | 100 | 98 |
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310207962.XA CN103272646B (zh) | 2013-05-29 | 2013-05-29 | 用于制备L-薄荷醇中间体d-香茅醛的催化剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310207962.XA CN103272646B (zh) | 2013-05-29 | 2013-05-29 | 用于制备L-薄荷醇中间体d-香茅醛的催化剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103272646A true CN103272646A (zh) | 2013-09-04 |
CN103272646B CN103272646B (zh) | 2015-02-11 |
Family
ID=49055326
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310207962.XA Active CN103272646B (zh) | 2013-05-29 | 2013-05-29 | 用于制备L-薄荷醇中间体d-香茅醛的催化剂及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103272646B (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109456157A (zh) * | 2018-12-10 | 2019-03-12 | 万华化学集团股份有限公司 | 一种由r-香茅醛制备l-薄荷酮的方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1060793A1 (en) * | 1999-06-17 | 2000-12-20 | Firmenich Sa | Stereospecific isomerisation of allylamines with the aid of immobilised phosphorated chiral ligands |
CN102143968A (zh) * | 2008-07-04 | 2011-08-03 | 约翰逊马西有限公司 | 制备阳离子铑络合物的方法 |
-
2013
- 2013-05-29 CN CN201310207962.XA patent/CN103272646B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1060793A1 (en) * | 1999-06-17 | 2000-12-20 | Firmenich Sa | Stereospecific isomerisation of allylamines with the aid of immobilised phosphorated chiral ligands |
CN102143968A (zh) * | 2008-07-04 | 2011-08-03 | 约翰逊马西有限公司 | 制备阳离子铑络合物的方法 |
Non-Patent Citations (3)
Title |
---|
HONG-BIN YU等: "Synthesis of a rigid and optically active poly(BINAP) and its application in asymmetric catalysis", 《TETRAHEDRON LETTERS》, vol. 41, 31 December 2000 (2000-12-31) * |
MAJA HEITBAUM等: "Asymmetric Heterogeneous Catalysis", 《ANGEW.CHEM.INT.ED.》, vol. 45, 27 June 2006 (2006-06-27) * |
乔振等: "不对称催化氢化反应中配体研究进展", 《合成化学》, vol. 10, no. 1, 31 December 2002 (2002-12-31) * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109456157A (zh) * | 2018-12-10 | 2019-03-12 | 万华化学集团股份有限公司 | 一种由r-香茅醛制备l-薄荷酮的方法 |
CN109456157B (zh) * | 2018-12-10 | 2021-09-07 | 万华化学集团股份有限公司 | 一种由r-香茅醛制备l-薄荷酮的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN103272646B (zh) | 2015-02-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102603607B (zh) | (r)-奥拉西坦的制备方法 | |
CN108503719A (zh) | 一种提取铁皮石斛多糖的方法 | |
CN102911022A (zh) | 一种天然姜黄素类物的人工合成方法 | |
CN111689878A (zh) | 一种三氟甲磺酸酐制备工艺 | |
CN103254047B (zh) | 制备L-薄荷醇中间体d-香茅醛的方法 | |
CN105111098A (zh) | 从玛咖中提取纯化玛咖酰胺单体化合物的方法 | |
CN108467345B (zh) | 一种从蒜头果中提取神经酸的方法及神经酸包合物 | |
CN103509133A (zh) | 一种香菇多糖快速分离的方法 | |
CN103172629B (zh) | 一种高纯度盐酸莫西沙星的合成方法 | |
CN108658987B (zh) | 一种敌草快合成及精制工艺 | |
CN103272646B (zh) | 用于制备L-薄荷醇中间体d-香茅醛的催化剂及其制备方法 | |
CN103086845A (zh) | 制备l-薄荷醇的方法 | |
CN104402973A (zh) | 一种卡非佐米无定型晶的制备方法 | |
CN101362740B (zh) | 亚硫酸氢钠穿心莲内酯的合成方法 | |
CN103012107B (zh) | 一种从产丁二酸的发酵液中制备丁二酸胺的方法 | |
CN101492350B (zh) | 从植物刺槐中制备d-松醇的方法 | |
CN103012140B (zh) | 吉法酯的制备方法 | |
CN103214421B (zh) | 2-巯基-1-甲基咪唑的工业化生产方法 | |
CN101781175B (zh) | 一种分离2,4-二氯苯酚和2,6-二氯苯酚的方法 | |
CN107537573A (zh) | 高选择性合成1,8‑桉叶素的方法 | |
CN101024609B (zh) | 一种莽草酸的生产工艺 | |
CN101805269A (zh) | 一种分离提取天然茶氨酸的方法 | |
CN100447129C (zh) | 姜酚肟及其合成与应用 | |
JPH0291035A (ja) | 天然ゴム漿液中のl−クエブラキトールの採取方法 | |
CN111302919A (zh) | 一种高含量二氢茉莉酮香料的合成方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: SHANGHAI TONGYI BIOTECHNOLOGY CO., LTD. Free format text: FORMER OWNER: SHANGHAI HAOXIANG BIOLOGICAL TECHNOLOGY CO.,LTD. Effective date: 20150311 |
|
C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 200443 BAOSHAN, SHANGHAI TO: 200444 BAOSHAN, SHANGHAI |
|
TR01 | Transfer of patent right |
Effective date of registration: 20150311 Address after: 200444, No. 2, Fai Fai Road, Baoshan District, Shanghai, building 255 Patentee after: SHANGHAI TOPYUM BIO-TECHNOLOGY CO.,LTD. Address before: 200443, Shanghai, Baoshan District, long road, 913 lane, 1115 business building, Beidou Patentee before: SHANGHAI HAOXIANG BIOLOG TECHNOLOGY Co.,Ltd. |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Catalyst and preparation method for preparing the intermediate d-citronellal of L-menthol Effective date of registration: 20230518 Granted publication date: 20150211 Pledgee: Industrial Bank Co.,Ltd. Shanghai Hongkou sub branch Pledgor: SHANGHAI TOPYUM BIO-TECHNOLOGY CO.,LTD. Registration number: Y2023310000196 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right |