CN103266501A - Low-temperature cashmere dyeing method adopting ionic liquid for pretreatment - Google Patents
Low-temperature cashmere dyeing method adopting ionic liquid for pretreatment Download PDFInfo
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- CN103266501A CN103266501A CN201310232949XA CN201310232949A CN103266501A CN 103266501 A CN103266501 A CN 103266501A CN 201310232949X A CN201310232949X A CN 201310232949XA CN 201310232949 A CN201310232949 A CN 201310232949A CN 103266501 A CN103266501 A CN 103266501A
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Abstract
The invention discloses a low-temperature cashmere dyeing method adopting an ionic liquid for pretreatment. The method is characterized by after pretreating cashmere with an ionic liquid with volume concentration of 5-10%, using a dye with volume concentration of 5-10%, 6g/l anhydrous sodium sulfate and 8g/l peregal 0, regulating the PH value to 4-5, carrying out water bathing and adding a low-temperature aid for dyeing at 80 DEG C, wherein the pretreatment temperature is 80 DEG C; the bath ratio is 1:50 and water bathing time is 10-20 minutes; the bath ratio of water bathing in the dyeing step is 1:50 and the time is 60-80 minutes; the low-temperature aid is JL-D or ZJ-W; and the volume concentration of the low-temperature aid is 0.5-2%. The method has the obvious advantages that the strength of the yarns after low-temperature dyeing is 10.5% higher than that after normal dehaired wool dyeing; the yarn spinnability can be greatly improved; and the damages of dyeing to fibers can be reduced.
Description
Technical field
The present invention relates to a kind of cashmere low-temperature dyeing method, specifically is the pretreated cashmere low-temperature dyeing method of a kind of employing ionic liquid.
Background technology
Cashmere fiber is behind normal dyeing, yarn strength in spinning process, often occurs and do not reach standard-required, even be lower than the situation of standard 20% to 30%, and problems such as top, garment piece broken hole appear falling in the braiding process, have a strong impact on quality and the manufacturing schedule of product.
Summary of the invention
Goal of the invention: the object of the present invention is to provide the preliminary treatment of a kind of employing ionic liquid, by low temperature dyeing, improve worsted cashmere yarn row yielding, improve spinnability, reduce the method for the damage that dyeing causes fiber.
In order to realize the foregoing invention purpose, the technical solution adopted in the present invention is:
The pretreated cashmere low-temperature dyeing method of a kind of employing ionic liquid, after using volumetric concentration to be 5% ~ 10% ionic liquid preliminary treatment the cashmere, the use volumetric concentration is 5% ~ 10% dyestuff, the glauber salt of 6g/l, the peregal of 8g/l 0, transfer pH value to 4 ~ 5, water-bath is added cryogenic booster dyeing down at 80 ℃.
Described preliminary treatment is in 80 ℃ of temperature, bath raio 1:50, water-bath 10 ~ 20min.
The bath raio of water-bath is 1:50 in the described staining procedure, time 60 ~ 80min.
Described cryogenic booster is cryogenic booster JL-D or cryogenic booster ZJ-W.
The volumetric concentration of described cryogenic booster is 0.5% ~ 2%
Beneficial effect: compared with prior art, remarkable advantage of the present invention is: powerful dyeing than normal woolenless cloth exceeds 10.5 % after the low temperature dyeing of the present invention, can greatly improve the yarn spinnability, reduces the damage that dyeing causes fiber.
The specific embodiment
The present invention is further described below by specific embodiment; should be pointed out that for the person of ordinary skill of the art, under the prerequisite that does not break away from the principle of the invention; can also make some modification and improvement, these also should be considered as belonging to protection scope of the present invention.
Embodiment 1
It is 5% ionic liquid that cashmere is used volumetric concentration, in 80 ℃ of temperature; bath raio 1:50, after the water-bath 10min preliminary treatment, the use volumetric concentration is 5% dyestuff; the glauber salt of 6g/l, the peregal of 8g/l 0; transfer pH value to 4, water-bath, and bath raio is 1:50; time 60min, the interpolation volumetric concentration is 0.5% cryogenic booster JL-D dyeing under 80 ℃.
Embodiment 2
It is 10% ionic liquid that cashmere is used volumetric concentration, in 80 ℃ of temperature; bath raio 1:50, after the water-bath 20min preliminary treatment, the use volumetric concentration is 10% dyestuff; the glauber salt of 6g/l, the peregal of 8g/l 0; transfer pH value to 5, water-bath, and bath raio is 1:50; time 80min, the interpolation volumetric concentration is 2% cryogenic booster ZJ-W dyeing under 80 ℃.
Claims (5)
1. one kind is adopted the pretreated cashmere low-temperature dyeing method of ionic liquid, it is characterized in that: after using volumetric concentration to be 5% ~ 10% ionic liquid preliminary treatment in cashmere, the use volumetric concentration is 5% ~ 10% dyestuff, add the glauber salt of 6g/l, the peregal 0 of 8g/l, transfer pH value to 4 ~ 5, water-bath is added cryogenic booster dyeing down at 80 ℃.
2. the pretreated cashmere sweater low-temperature dyeing method of a kind of employing ionic liquid according to claim 1, it is characterized in that: described preliminary treatment is in 80 ℃ of temperature, bath raio 1:50, water-bath 10 ~ 20min.
3. the pretreated cashmere sweater low-temperature dyeing method of a kind of employing ionic liquid according to claim 1, it is characterized in that: the bath raio of water-bath is 1:50 in the described staining procedure, time 60 ~ 80min.
4. the pretreated cashmere sweater low-temperature dyeing method of a kind of employing ionic liquid according to claim 1, it is characterized in that: described cryogenic booster is cryogenic booster JL-D or cryogenic booster ZJ-W.
5. the pretreated cashmere sweater low-temperature dyeing method of a kind of employing ionic liquid according to claim 1, it is characterized in that: the volumetric concentration of described cryogenic booster is 0.5% ~ 2%.
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CN201310232949XA CN103266501A (en) | 2013-06-13 | 2013-06-13 | Low-temperature cashmere dyeing method adopting ionic liquid for pretreatment |
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CN201310232949XA CN103266501A (en) | 2013-06-13 | 2013-06-13 | Low-temperature cashmere dyeing method adopting ionic liquid for pretreatment |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103924455A (en) * | 2014-04-02 | 2014-07-16 | 湖州思祺服饰染整有限公司 | Cashmere dye and dying technology |
CN105908538A (en) * | 2016-05-19 | 2016-08-31 | 太仓协大申泰羊毛衫有限公司 | Process for printing and dyeing wool fabric |
CN113463414A (en) * | 2021-08-12 | 2021-10-01 | 西安工程大学 | Low-temperature dyeing auxiliary agent of wool or cashmere reactive dye, preparation method and application |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102277754A (en) * | 2011-06-28 | 2011-12-14 | 湖南工程学院 | Method of wool surface modification and low temperature dyeing |
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2013
- 2013-06-13 CN CN201310232949XA patent/CN103266501A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102277754A (en) * | 2011-06-28 | 2011-12-14 | 湖南工程学院 | Method of wool surface modification and low temperature dyeing |
Non-Patent Citations (1)
Title |
---|
叶其林: "超薄羊绒衫强力和抗起毛起球性能及其改进的研究", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103924455A (en) * | 2014-04-02 | 2014-07-16 | 湖州思祺服饰染整有限公司 | Cashmere dye and dying technology |
CN105908538A (en) * | 2016-05-19 | 2016-08-31 | 太仓协大申泰羊毛衫有限公司 | Process for printing and dyeing wool fabric |
CN113463414A (en) * | 2021-08-12 | 2021-10-01 | 西安工程大学 | Low-temperature dyeing auxiliary agent of wool or cashmere reactive dye, preparation method and application |
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Application publication date: 20130828 |