CN103254645A - 无机防火组合物、防火材料及其制备方法 - Google Patents
无机防火组合物、防火材料及其制备方法 Download PDFInfo
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- CN103254645A CN103254645A CN2012102886291A CN201210288629A CN103254645A CN 103254645 A CN103254645 A CN 103254645A CN 2012102886291 A CN2012102886291 A CN 2012102886291A CN 201210288629 A CN201210288629 A CN 201210288629A CN 103254645 A CN103254645 A CN 103254645A
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- 239000000463 material Substances 0.000 title claims abstract description 54
- 239000000203 mixture Substances 0.000 title claims abstract description 51
- 238000002360 preparation method Methods 0.000 title description 4
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 45
- 239000003063 flame retardant Substances 0.000 claims abstract description 42
- 239000000843 powder Substances 0.000 claims abstract description 25
- -1 polysiloxane Polymers 0.000 claims abstract description 21
- 230000000694 effects Effects 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims abstract description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 54
- 239000000377 silicon dioxide Substances 0.000 claims description 27
- 239000002245 particle Substances 0.000 claims description 26
- 229960001866 silicon dioxide Drugs 0.000 claims description 23
- 235000012239 silicon dioxide Nutrition 0.000 claims description 23
- 239000000178 monomer Substances 0.000 claims description 16
- 125000005401 siloxanyl group Chemical group 0.000 claims description 16
- 238000009833 condensation Methods 0.000 claims description 15
- 230000005494 condensation Effects 0.000 claims description 15
- 230000007062 hydrolysis Effects 0.000 claims description 14
- 238000006460 hydrolysis reaction Methods 0.000 claims description 14
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical group [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 13
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 13
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 10
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 8
- 239000002956 ash Substances 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 8
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 8
- 239000000347 magnesium hydroxide Substances 0.000 claims description 8
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 8
- 239000010703 silicon Substances 0.000 claims description 8
- 229910052710 silicon Inorganic materials 0.000 claims description 8
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 claims description 8
- 239000011248 coating agent Substances 0.000 claims description 7
- 238000000576 coating method Methods 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 239000002798 polar solvent Substances 0.000 claims description 5
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 4
- 239000012752 auxiliary agent Substances 0.000 claims description 4
- 238000005336 cracking Methods 0.000 claims description 4
- 238000009413 insulation Methods 0.000 claims description 4
- 239000011230 binding agent Substances 0.000 claims description 3
- 150000001721 carbon Chemical group 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 239000013543 active substance Substances 0.000 claims description 2
- 239000003086 colorant Substances 0.000 claims description 2
- 239000000975 dye Substances 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 238000005728 strengthening Methods 0.000 claims description 2
- 230000008719 thickening Effects 0.000 claims description 2
- PGCBRGRKKOCPAN-UHFFFAOYSA-N 4-triethoxysilylbutanamide Chemical compound CCO[Si](OCC)(OCC)CCCC(N)=O PGCBRGRKKOCPAN-UHFFFAOYSA-N 0.000 claims 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims 1
- 239000012796 inorganic flame retardant Substances 0.000 abstract 1
- 239000000499 gel Substances 0.000 description 29
- 239000004793 Polystyrene Substances 0.000 description 8
- 238000006116 polymerization reaction Methods 0.000 description 7
- 238000012360 testing method Methods 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 229920002223 polystyrene Polymers 0.000 description 4
- 229920005992 thermoplastic resin Polymers 0.000 description 4
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 125000000524 functional group Chemical group 0.000 description 3
- 239000003365 glass fiber Substances 0.000 description 3
- 229920002635 polyurethane Polymers 0.000 description 3
- 239000004814 polyurethane Substances 0.000 description 3
- 230000000979 retarding effect Effects 0.000 description 3
- 229910000077 silane Inorganic materials 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 238000007429 general method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910000000 metal hydroxide Inorganic materials 0.000 description 2
- 150000004692 metal hydroxides Chemical class 0.000 description 2
- 239000011490 mineral wool Substances 0.000 description 2
- 229920003987 resole Polymers 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- QENGRZQSSNEJHW-UHFFFAOYSA-N NCCC[Si](OCC)(OCC)OCC.NC(=O)CCC[Si](OCC)(OCC)OCC Chemical compound NCCC[Si](OCC)(OCC)OCC.NC(=O)CCC[Si](OCC)(OCC)OCC QENGRZQSSNEJHW-UHFFFAOYSA-N 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229920006248 expandable polystyrene Polymers 0.000 description 1
- 238000004079 fireproofing Methods 0.000 description 1
- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- GPRLSGONYQIRFK-UHFFFAOYSA-N hydron Chemical compound [H+] GPRLSGONYQIRFK-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- VWBWQOUWDOULQN-UHFFFAOYSA-N nmp n-methylpyrrolidone Chemical compound CN1CCCC1=O.CN1CCCC1=O VWBWQOUWDOULQN-UHFFFAOYSA-N 0.000 description 1
- 125000000962 organic group Chemical group 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 125000005375 organosiloxane group Chemical class 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 239000002491 polymer binding agent Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000011342 resin composition Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000004154 testing of material Methods 0.000 description 1
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 description 1
Abstract
Description
氢氧化铝(55μm) | 14g |
氢氧化铝(8μm) | 4.2g |
氢氧化铝(1μm) | 1.26g |
硅粉 | 0.54g |
玻璃纤维(6.4mm) | 0.2g |
硅烷组合物 | 1g |
pH=2的乙醇水溶液 | 6g |
Claims (17)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
TW101105361A TW201335344A (zh) | 2012-02-17 | 2012-02-17 | 無機防火組合物、防火材料及其形成方法 |
TW101105361 | 2012-02-17 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN103254645A true CN103254645A (zh) | 2013-08-21 |
Family
ID=48958877
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2012102886291A Pending CN103254645A (zh) | 2012-02-17 | 2012-08-14 | 无机防火组合物、防火材料及其制备方法 |
Country Status (2)
Country | Link |
---|---|
CN (1) | CN103254645A (zh) |
TW (1) | TW201335344A (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104927491A (zh) * | 2015-07-02 | 2015-09-23 | 龚灿锋 | 一种抗菌阻燃涂料及其制备方法 |
CN110028876A (zh) * | 2019-06-11 | 2019-07-19 | 广讯检测(广东)有限公司 | 一种电路板用高温阻燃涂料组合及其制备方法 |
CN111187571A (zh) * | 2018-06-26 | 2020-05-22 | 王春林 | 一种无卤阻燃硅烷水性涂料及其制备和应用 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2511140A (en) * | 2013-02-26 | 2014-08-27 | Shayonano Singapore Pte Ltd | Flame retardant composite particles |
-
2012
- 2012-02-17 TW TW101105361A patent/TW201335344A/zh unknown
- 2012-08-14 CN CN2012102886291A patent/CN103254645A/zh active Pending
Non-Patent Citations (1)
Title |
---|
张治华: ""水镁石复合阻燃剂的制备及其应用试验"", 《塑料助剂》 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104927491A (zh) * | 2015-07-02 | 2015-09-23 | 龚灿锋 | 一种抗菌阻燃涂料及其制备方法 |
CN111187571A (zh) * | 2018-06-26 | 2020-05-22 | 王春林 | 一种无卤阻燃硅烷水性涂料及其制备和应用 |
CN111234697A (zh) * | 2018-06-26 | 2020-06-05 | 王春林 | 一种无卤阻燃硅烷水性涂料及其制备和应用 |
CN111269658A (zh) * | 2018-06-26 | 2020-06-12 | 王春林 | 一种无卤阻燃硅烷水性涂料及其制备和应用 |
CN111286270A (zh) * | 2018-06-26 | 2020-06-16 | 王春林 | 一种无卤阻燃硅烷水性涂料及其制备和应用 |
CN111363475A (zh) * | 2018-06-26 | 2020-07-03 | 王春林 | 一种无卤阻燃硅烷水性涂料及其制备和应用 |
CN110028876A (zh) * | 2019-06-11 | 2019-07-19 | 广讯检测(广东)有限公司 | 一种电路板用高温阻燃涂料组合及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
TW201335344A (zh) | 2013-09-01 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
ASS | Succession or assignment of patent right |
Owner name: JUSEN CO., LTD. Free format text: FORMER OWNER: CHI LIN TECHNOLOGY CO., LTD. Effective date: 20150123 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20150123 Address after: Based Chinese Taiwan Lake Road, Neihu district of Taipei City No. 37 12 floor Applicant after: Chi Lin Technology Co., Ltd. Address before: Tainan City, Taiwan, China Applicant before: Chi Lin Technology Co., Ltd. |
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RJ01 | Rejection of invention patent application after publication |
Application publication date: 20130821 |
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RJ01 | Rejection of invention patent application after publication |