CN103224238B - 一种纳米硅复合材料的制备方法 - Google Patents
一种纳米硅复合材料的制备方法 Download PDFInfo
- Publication number
- CN103224238B CN103224238B CN201310194569.1A CN201310194569A CN103224238B CN 103224238 B CN103224238 B CN 103224238B CN 201310194569 A CN201310194569 A CN 201310194569A CN 103224238 B CN103224238 B CN 103224238B
- Authority
- CN
- China
- Prior art keywords
- silicon
- preparation
- gas
- composite material
- nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 239000002131 composite material Substances 0.000 title claims abstract description 11
- 239000005543 nano-size silicon particle Substances 0.000 title claims abstract description 9
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 46
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 44
- 239000010703 silicon Substances 0.000 claims abstract description 44
- 238000006243 chemical reaction Methods 0.000 claims abstract description 22
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 60
- 239000007789 gas Substances 0.000 claims description 52
- 239000000377 silicon dioxide Substances 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 27
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 26
- 235000013312 flour Nutrition 0.000 claims description 25
- 229910052786 argon Inorganic materials 0.000 claims description 13
- 235000013339 cereals Nutrition 0.000 claims description 11
- 239000001257 hydrogen Substances 0.000 claims description 11
- 229910052739 hydrogen Inorganic materials 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- 238000002309 gasification Methods 0.000 claims description 5
- 239000001307 helium Substances 0.000 claims description 5
- 229910052734 helium Inorganic materials 0.000 claims description 5
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 5
- 229910000073 phosphorus hydride Inorganic materials 0.000 claims description 5
- UEXCJVNBTNXOEH-UHFFFAOYSA-N Ethynylbenzene Chemical group C#CC1=CC=CC=C1 UEXCJVNBTNXOEH-UHFFFAOYSA-N 0.000 claims description 4
- 238000001241 arc-discharge method Methods 0.000 claims description 4
- 239000004567 concrete Substances 0.000 claims description 4
- 238000010899 nucleation Methods 0.000 claims description 4
- 230000006911 nucleation Effects 0.000 claims description 4
- 229920001296 polysiloxane Polymers 0.000 claims description 4
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 229910000085 borane Inorganic materials 0.000 claims description 3
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 239000007858 starting material Substances 0.000 claims description 3
- UORVGPXVDQYIDP-UHFFFAOYSA-N trihydridoboron Substances B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 claims description 3
- 230000004913 activation Effects 0.000 claims description 2
- 150000001336 alkenes Chemical class 0.000 claims description 2
- 150000001345 alkine derivatives Chemical class 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000005984 hydrogenation reaction Methods 0.000 claims description 2
- 230000008676 import Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 229930195735 unsaturated hydrocarbon Natural products 0.000 claims description 2
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 11
- 239000002114 nanocomposite Substances 0.000 abstract description 9
- 239000011258 core-shell material Substances 0.000 abstract description 5
- 230000003647 oxidation Effects 0.000 abstract description 5
- 238000007254 oxidation reaction Methods 0.000 abstract description 5
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 4
- 238000009272 plasma gasification Methods 0.000 abstract description 3
- 239000004065 semiconductor Substances 0.000 abstract description 2
- 229910021419 crystalline silicon Inorganic materials 0.000 abstract 2
- 230000003213 activating effect Effects 0.000 abstract 1
- 238000004220 aggregation Methods 0.000 abstract 1
- 230000002776 aggregation Effects 0.000 abstract 1
- 238000010891 electric arc Methods 0.000 abstract 1
- 239000012467 final product Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 13
- 239000002994 raw material Substances 0.000 description 11
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 9
- 239000007788 liquid Substances 0.000 description 9
- 239000002245 particle Substances 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 239000011856 silicon-based particle Substances 0.000 description 8
- 238000002485 combustion reaction Methods 0.000 description 5
- 239000002105 nanoparticle Substances 0.000 description 5
- 238000005457 optimization Methods 0.000 description 5
- 230000001276 controlling effect Effects 0.000 description 4
- 238000006356 dehydrogenation reaction Methods 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 3
- 230000033228 biological regulation Effects 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 239000002086 nanomaterial Substances 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 239000004484 Briquette Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000000498 ball milling Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000003989 dielectric material Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000002620 method output Methods 0.000 description 2
- 229910021487 silica fume Inorganic materials 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910008045 Si-Si Inorganic materials 0.000 description 1
- 229910006411 Si—Si Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000007806 chemical reaction intermediate Substances 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229920000548 poly(silane) polymer Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011863 silicon-based powder Substances 0.000 description 1
- 150000003384 small molecules Chemical group 0.000 description 1
- 238000010183 spectrum analysis Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
Landscapes
- Silicon Compounds (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310194569.1A CN103224238B (zh) | 2013-05-23 | 2013-05-23 | 一种纳米硅复合材料的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310194569.1A CN103224238B (zh) | 2013-05-23 | 2013-05-23 | 一种纳米硅复合材料的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103224238A CN103224238A (zh) | 2013-07-31 |
CN103224238B true CN103224238B (zh) | 2014-12-17 |
Family
ID=48834918
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310194569.1A Active CN103224238B (zh) | 2013-05-23 | 2013-05-23 | 一种纳米硅复合材料的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103224238B (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105032330B (zh) * | 2015-05-12 | 2017-03-01 | 青岛科技大学 | 一种纳米复合材料的制备装置 |
CN106698437A (zh) * | 2017-01-03 | 2017-05-24 | 昆明理工大学 | 一种利用热等离子法制备球形纳米硅的方法 |
CN113387360A (zh) * | 2021-05-25 | 2021-09-14 | 河南硅烷科技发展股份有限公司 | 一种抑制区熔级多晶硅cvd过程中硅枝晶生长的界面浸润性调控方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101559946B (zh) * | 2009-04-27 | 2011-01-05 | 浙江大学 | 利用等离子体制备硅纳米颗粒的方法及装置 |
CN102347223B (zh) * | 2011-09-30 | 2013-04-24 | 浙江大学 | 一种利用胶态硅纳米颗粒对硅片进行掺杂的方法 |
-
2013
- 2013-05-23 CN CN201310194569.1A patent/CN103224238B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN103224238A (zh) | 2013-07-31 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103311511B (zh) | 一种壳核结构纳米硅复合材料的制备方法 | |
CN104549658B (zh) | 冷场等离子体放电辅助高能球磨粉体装置 | |
CN105185970A (zh) | 一种包覆硅的碳颗粒复合材料、制备方法和设备及用途 | |
CN108907210A (zh) | 一种制备增材制造用实心球形金属粉末的方法 | |
CN103224238B (zh) | 一种纳米硅复合材料的制备方法 | |
CN104772473A (zh) | 一种3d打印用细颗粒球形钛粉的制备方法 | |
CN106698437A (zh) | 一种利用热等离子法制备球形纳米硅的方法 | |
CN108217612A (zh) | 制备球形氮化钛粉末的方法及设备 | |
CN102320606B (zh) | 一种生长纳米晶硅粉体的方法 | |
CN103972495B (zh) | 一种锂离子电池正极材料镍锰酸锂的制备方法 | |
CN203339107U (zh) | 一种用来制备纳米硅粉的电弧放电-等离子体复合装置 | |
CN107706398A (zh) | 硅基锂离子电池的负极材料的制备方法 | |
CN203333311U (zh) | 一种用来制备纳米硅粉的等离子体装置 | |
CN103072961A (zh) | 纳米氮化铝粉的生产方法 | |
CN113290249A (zh) | 一种电弧辅助的等离子雾化制备球形金属粉末的方法及设备 | |
CN108163821A (zh) | 球形氮化钛的制备方法 | |
CN102909386B (zh) | 微细球形铝粉的生产方法 | |
CN108046268A (zh) | 等离子体化学气相合成法制备高纯纳米碳化硼粉末的方法 | |
CN110890537A (zh) | 一种高纯纳米晶硅的生产方法 | |
CN108101061A (zh) | 纳米硅粉的制备方法 | |
CN215429502U (zh) | 一种连续低温等离子体粉末处理和球磨生产装置 | |
CN107188216B (zh) | 一种纳米球形铈组轻稀土氧化物的制备方法 | |
CN113130857B (zh) | 一种纳米硅材料及其制备方法 | |
CN114349011A (zh) | 一种纳米氧化亚硅粉体的制备方法 | |
CN106887571B (zh) | 一种组成可控的钛酸锂/二氧化钛纳米复合颗粒、制备方法及其应用 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200527 Address after: 435000 Fushui street, Fushui Town, Yangxin County, Huangshi City, Hubei Province 098 Patentee after: Zheng Yuehua Address before: 436000 Ezhou city of Hubei Province Liu Xian Cun, Echeng District Tingzu town Liu Xian No. 8 Patentee before: Liu Guojun |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210127 Address after: Room 491, building 2, Chuangye building, 66 Yuanshi Road, hi tech Zone, Ningbo, Zhejiang Province, 315000 Patentee after: NINGBO GEXIN NEW ENERGY TECHNOLOGY Co.,Ltd. Address before: 435000 Fushui Street 098, Fushui Town, Yangxin County, Huangshi City, Hubei Province Patentee before: Zheng Yuehua |
|
TR01 | Transfer of patent right |