CN103169148B - Moist tobacco sheet and manufacture method thereof - Google Patents
Moist tobacco sheet and manufacture method thereof Download PDFInfo
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- CN103169148B CN103169148B CN201310069262.9A CN201310069262A CN103169148B CN 103169148 B CN103169148 B CN 103169148B CN 201310069262 A CN201310069262 A CN 201310069262A CN 103169148 B CN103169148 B CN 103169148B
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- offal
- oroxylum indicum
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Abstract
The invention relates to the technical field of tobacco sheets and provides a protection and moist tobacco sheet and a manufacture method of the protection and moist tobacco sheet. A paper base of the tobacco sheet is mainly made of oroxylum indicum, giant knot weed, Chinese actinidia root, purple perilla, cabo and tobacco powder. The oroxylum indicum, the giant knot weed, the Chinese actinidia root, the purple perilla, the cabo and the tobacco powder size and extractives are manufactured in a specific method and all sorts of size is mixed in a ratio and papermaking is performed. A protection and moist tobacco sheet is obtained after coaling and drying. Compared with a normal sheet, the protection and moist tobacco sheet is stronger in sweetness, little in irritation, little in mixed gas, smooth in swallowing and capable of being used massively in cigarette production.
Description
Technical field
The present invention relates to reconstituted tobacoo technical field, more specifically, relate to a kind of humectation type reconstituted tobacoo and preparation method thereof.
Background technology
Reducing tar and reducing harm is study hotspot and the emphasis of current tobacco business, by adding reconstituted tobacoo in cigarette, reaches the object of reducing tar and reducing harm, is a kind of main stream approach.
At present, the reconstituted tobacoo extensive use in the world of paper process production.Conventional reconstituted tobacoo adopts the dead meal of tobacco leaf production, such as offal and offal lixiviate, the filter residue obtained is prepared sheet paper base through defibrination, handsheet, and on sheet paper base, applied coating solution prepares reconstituted tobacoo, gained reconstituted tobacoo is substituted a part of pipe tobacco and prepares cigarette.But, existing reconstituted tobacoo has the problem of coarse stimulation on aesthetic quality, join after in cigarette, inevitably affect the aesthetic quality of cigarette, also have and adopt wood-fibred slurry to starch to match with offal and offal and prepare the technical scheme of reconstituted tobacoo, although the physical property of reconstituted tobacoo strengthens to some extent, make an addition to after cigarette shreds still inevitable for the impact of the aesthetic quality of cigarette, thus also just limit a large amount of uses of reconstituted tobacoo.
Oroxylum indicum (
semen Oroxyli) containing Oroxylum indicum glucoside, baicalin, oroxylin isoreactivity material, can clearing lung-heat heat, throat, can treating acute and chronic bronchitis, cough, abscess of throat,
tonsillitisdeng; Giant knotweed (
rhizoma Polygoni Cuspidati) have clearing heat and detoxicating, relieving cough and reducing sputum, loose stasis of blood analgesic therapy effect; Chinese actinidia root is the root of Actinidiaceae plant tara vine (Actinidia arguta (Zucc.) Planch.ex Miq.), has clearing heat and detoxicating, effect of clearing heat and promoting diuresis; Purple perilla (
perilla frutescens), containing perillaldehyde, left-handed
citrene, perilla alcohols etc., have special
fragrance, there is effect of loose cold air, clearing lung-heat gas, wide middle gas, the gas that reduces phlegm.
At present after Oroxylum indicum, giant knotweed, Chinese actinidia root, purple perilla is compatible, be applied to the technology report preparing reconstituted tobacoo.
Summary of the invention
The technical problem to be solved in the present invention is the technical deficiency for existing reconstituted tobacoo, a kind of humectation type reconstituted tobacoo is provided, jointly prepare reconstituted tobacoo by after Oroxylum indicum, giant knotweed, Chinese actinidia root, purple perilla, offal, offal reasonable compatibility with offal and offal, overcome the problem of existing reconstituted tobacoo in the coarse stimulation of aesthetic quality.
Another technical problem that the present invention will solve is to provide the preparation method of described reconstituted tobacoo.
Object of the present invention is achieved by the following technical programs:
There is provided a kind of humectation type reconstituted tobacoo, coating fluid is put on sheet paper base and prepares, described sheet paper base prepares through copy paper after being mixed by following slurry: count in mass ratio, Oroxylum indicum slurry, 10 ~ 30%; Giant knotweed slurry, 10 ~ 30%; Chinese actinidia root slurry, 10 ~ 30%; Purple perilla slurry, 10 ~ 30%; Offal slurry, 10 ~ 30%; Offal slurry, 5 ~ 30%.
Preferably, described sheet paper base, prepares through copy paper after being mixed: count in mass ratio, Oroxylum indicum slurry, 10 ~ 20% by following slurry; Giant knotweed slurry, 10 ~ 20%; Chinese actinidia root slurry, 10 ~ 20%; Purple perilla slurry, 10 ~ 20%; Offal slurry, 20 ~ 30%; Offal slurry, 10 ~ 25%;
More preferred, described sheet paper base, prepares through copy paper after being mixed: count in mass ratio, Oroxylum indicum slurry, 10% by following slurry; Giant knotweed slurry, 15%; Chinese actinidia root slurry, 10%; Purple perilla slurry, 15%; Offal slurry, 30%; Offal slurry, 20%.
The preparation method of described Oroxylum indicum slurry is: with Chinese herbal medicine Oroxylum indicum for raw material, filters after adding the water soaking of the solid sodium hydroxide of Oroxylum indicum quality 2% ~ 10% and 4 ~ 10 times, collects filter residue and carries out defibrination and obtain Oroxylum indicum slurry.
Preferably, the addition of described NaOH is 5% of Oroxylum indicum quality; Amount of water is determined according to 4 ~ 10 times of Oroxylum indicum quality.
The most preferably, add NaOH according to 5% of Oroxylum indicum quality, add water according to 5 times of Oroxylum indicum quality, soak 3 ~ 4 days, filter, by filter residue defibrination, obtain Oroxylum indicum slurry.
The preparation method of described giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry, offal slurry or offal slurry is: filter after the refluxing extraction that Chinese herbal medicine giant knotweed, Chinese actinidia root, purple perilla and offal, offal added water respectively, collects gained filter residue defibrination and get final product.Collect the extract of offal refluxing extraction concentrated after can use as coating fluid.
Preferably, described amount of water determines according to 4 ~ 10 times of quality of giant knotweed, Chinese actinidia root, purple perilla, offal or offal respectively.
Preferably, described reflux extracting time is 1 ~ 5 hour.
The applied amount of described coating fluid accounts for 5 ~ 50% of sheet paper base oven dry weight.The most preferably, the applied amount of described coating fluid accounts for 36 % of sheet paper base oven dry weight.
As preferably, coating fluid of the present invention, by quality ratio, comprises the functional perfumery of 1 ~ 10% and the offal extract of 90 ~ 99%.Described functional perfumery is the fragrance product from the routine buying of spices company, and described offal extract is concentrated by the aqueous extract of offal and obtains.
Described functional perfumery can require to select according to the concrete fragrance of cigarette.Preferably, the most adaptive with reconstituted tobacoo paper substrate of the present invention functional perfumery comprises falling to stimulate plate spices, falls assorted gas plate spices and/or sweet plate spices.
The present invention provides the preparation method of described humectation type reconstituted tobacoo simultaneously, comprises the following steps:
S1. Oroxylum indicum slurry, giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry, offal slurry, offal slurry, offal extract is prepared respectively;
S2. example mixes the various slurry of S1 gained in mass ratio;
S3. by the slurry handsheet that S2 gained mixes, reconstituted tobacoo paper substrate is obtained;
S4. concentrated S1 gained offal extract, concentrates to obtain offal extract; Offal extract and functional perfumery are mixed to get tobacco coating fluid; Tobacco coating fluid is put on reconstituted tobacoo paper substrate, dry, to obtain final product.
The invention has the beneficial effects as follows:
The present invention is with Chinese herbal medicine Oroxylum indicum, giant knotweed, Chinese actinidia root, purple perilla is that primary raw material and offal and offal prepare and obtain reconstituted tobacoo, through the Oroxylum indicum of suitably process, giant knotweed, Chinese actinidia root, the fiber of purple perilla and offal, the fiber of offal extremely mates, the reconstituted tobacoo quality prepared and tobacco leaf close, fragrance nature after burning, assorted gas is few, excitant is little, to join in cigarette can with pipe tobacco perfect fit, the discordant problem of flue gas can not be brought, the effect of lowering harm and decreasing coking can be played, also give the odor characteristic that cigarette is special, be with a wide range of applications in the reducing tar and reducing harm of Chinese-style cigarette, cigarette can be widely used in, there is important practical application promotional value.
Summing up on the tobacco sheet material compatibility basis obtained, the present invention is based on and in conjunction with a large amount of experimental summaries, accurate ratio composition is obtained to the analysis of each compatibility ingredient properties.
Accompanying drawing explanation
Fig. 1 Oroxylum indicum, giant knotweed, Chinese actinidia root, purple perilla, offal slurry preparation flow schematic diagram.
The preparation flow schematic diagram of Fig. 2 offal slurry and offal extract.
Fig. 3 reconstituted tobacoo preparation technology of the present invention schematic diagram.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described, but embodiments of the present invention is not limited in any way.Unless stated otherwise, the Oroxylum indicum that example of the present invention adopts, giant knotweed, Chinese actinidia root, purple perilla are conventional commercial herbal raw material, and the offal of employing and offal are the dead meal of tobacco leaf production enterprise, and other reagent are conventional reagent.
Embodiment 1
S1. slurry preparation
As shown in Figure 1, Oroxylum indicum slurry, giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry and offal slurry is prepared respectively; As shown in Figure 2, offal extract (offal extract) and offal slurry is prepared;
Wherein, add solid sodium hydroxide and water in Chinese herbal medicine Oroxylum indicum, the quality of solid sodium hydroxide is 5% of Oroxylum indicum quality, and the quality of water is 5 times of Oroxylum indicum quality, soaks after 4 days, filters, filter residue defibrination is obtained Oroxylum indicum slurry.
In giant knotweed, add the water of 4 times of giant knotweed quality, refluxing extraction, after 4 hours, is got filter residue defibrination and is obtained giant knotweed slurry.
In Chinese actinidia root, add the water of 4 times of Chinese actinidia root quality, refluxing extraction, after 4 hours, is got filter residue defibrination and is obtained Chinese actinidia root slurry.
In purple perilla, add the water of 6 times of purple perilla quality, refluxing extraction, after 4 hours, is got filter residue defibrination and is obtained purple perilla slurry.
In offal, add the water of 6 times of tobacco stalk qualities, refluxing extraction, after 2 hours, is got filter residue defibrination and is obtained offal slurry.
In offal, add the water of 8 times of offal quality, refluxing extraction, after 3 hours, is filtered, is got filter residue defibrination and obtain offal slurry; Get after filtrate concentrates according to reconstituted tobacoo conventional method and obtain offal extract.
Defibrination is with reference to refining process in existing reconstituted tobacoo preparation method.
S2. mixed slurry, mixes each for S1 gained slurry by mass ratio described in table 1:
Table 1 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 10% |
Giant knotweed | 15% |
Chinese actinidia root | 10% |
Purple perilla | 15% |
Offal | 30% |
Offal | 20% |
S3. copy paper
By shaping for the slurry copy paper on general paper machine after mixed, obtain sheet paper base;
S4. be coated with
According to the percentages accounting for S3 gained sheet paper base absolute dry mass, by the offal extract of the S1 gained of 10%, 0.2% fall stimulate plate spices, 0.25% fall assorted gas plate spices, 0.3% sweet plate spices mix, then be coated with on general paper making equipment, dry, obtain humectation type reconstituted tobacoo.
Embodiment 2
S1. slurry preparation
Prepared by the slurry with reference to embodiment 1.
S2. mixed slurry, each slurry mixes by the ratio of according to the form below 2
Table 2 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 15% |
Giant knotweed | 10% |
Chinese actinidia root | 15% |
Purple perilla | 10% |
Offal | 20% |
Offal | 30% |
Copy paper and coating, with reference to the method for embodiment 1, obtain humectation type reconstituted tobacoo.
Embodiment 3
Slurry preparation, copy paper and application step are with reference to embodiment 1, and mixed slurry ratio is implemented by table 3.
Table 3 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 15% |
Giant knotweed | 10% |
Chinese actinidia root | 15% |
Purple perilla | 10% |
Offal | 30% |
Offal | 20% |
Embodiment 4
Slurry preparation, copy paper and application step are with reference to embodiment 1, and mixed slurry ratio is implemented by table 4.
Table 4 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 10% |
Giant knotweed | 30% |
Chinese actinidia root | 15% |
Purple perilla | 30% |
Offal | 10% |
Offal | 5% |
Embodiment 5
Slurry preparation, copy paper and application step are with reference to embodiment 1, and mixed slurry ratio is implemented by table 5.
Table 5 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 30% |
Giant knotweed | 10% |
Chinese actinidia root | 15% |
Purple perilla | 30% |
Offal | 10% |
Offal | 5% |
Embodiment 6
S1. slurry preparation
As shown in Figure 1, Oroxylum indicum slurry, giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry and offal slurry is prepared respectively; As shown in Figure 2, offal extract (offal extract) and offal slurry is prepared;
Wherein, add solid sodium hydroxide and water in Chinese herbal medicine Oroxylum indicum, the quality of solid sodium hydroxide is 20% of Oroxylum indicum quality, and the quality of water is 10 times of Oroxylum indicum quality, soaks after 3 days, filters, filter residue defibrination is obtained Oroxylum indicum slurry.
In giant knotweed, add the water of 5 times of giant knotweed quality, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained giant knotweed slurry.
In Chinese actinidia root, add the water of 4 times of Chinese actinidia root quality, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained Chinese actinidia root slurry.
In purple perilla, add the water of 6 times of purple perilla quality, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained purple perilla slurry.
In offal, add the water of 5 times of tobacco stalk qualities, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained offal slurry.
In offal, add the water of 10 times of offal quality, refluxing extraction, after 3 hours, is filtered, is got filter residue defibrination and obtain offal slurry; Get after filtrate concentrates according to reconstituted tobacoo conventional method and obtain offal extract.
Defibrination is with reference to refining process in existing reconstituted tobacoo preparation method.
S2. mixed slurry, mixes each for S6 gained slurry by mass ratio described in table 6:
Table 6 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 10% |
Giant knotweed | 15% |
Chinese actinidia root | 10% |
Purple perilla | 15% |
Offal | 30% |
Offal | 20% |
Embodiment 7
S1. slurry preparation
As shown in Figure 1, Oroxylum indicum slurry, giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry and offal slurry is prepared respectively; As shown in Figure 2, offal extract (offal extract) and offal slurry is prepared;
Wherein, add solid sodium hydroxide and water in Chinese herbal medicine Oroxylum indicum, the quality of solid sodium hydroxide is 10% of Oroxylum indicum quality, and the quality of water is 6 times of Oroxylum indicum quality, soaks after 4 days, filters, filter residue defibrination is obtained Oroxylum indicum slurry.
In giant knotweed, add the water of 4 times of giant knotweed quality, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained giant knotweed slurry.
In Chinese actinidia root, add the water of 4 times of Chinese actinidia root quality, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained Chinese actinidia root slurry.
In purple perilla, add the water of 6 times of purple perilla quality, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained purple perilla slurry.
In offal, add the water of 5 times of tobacco stalk qualities, refluxing extraction, after 3 hours, is got filter residue defibrination and is obtained offal slurry.
In offal, add the water of 8 times of offal quality, refluxing extraction, after 3 hours, is filtered, is got filter residue defibrination and obtain offal slurry; Get after filtrate concentrates according to reconstituted tobacoo conventional method and obtain offal extract.
Defibrination is with reference to refining process in existing reconstituted tobacoo preparation method.
S2. mixed slurry, mixes each for S7 gained slurry by mass ratio described in table 7:
Table 7 mixes slurry ratio
Slurry | Slurry ratio (by over dry) |
Oroxylum indicum | 10% |
Giant knotweed | 15% |
Chinese actinidia root | 10% |
Purple perilla | 15% |
Offal | 30% |
Offal | 20% |
Embodiment 8 applies experiment of smokeing panel test
By the chopping on filament cutter of gained reconstituted tobacoo, roll into cigarette, chopping on filament cutter to make cigarette device, roll into cigarette to make cigarette device, carry out experiment of smokeing panel test, experimental result is as shown in table 8.Experimental result shows, as compared to ordinary sheet (ordinary sheet is the thin slice that existing employing offal wood pulp with slurry with offal and that add more than 10% obtains), the moisture feeling of the cigarette smoke of application the present embodiment reconstituted tobacoo obviously strengthens, stimulate little, assorted gas is few, enters larynx and along (because thin slice is not cigarette, smokeing panel test can not completely according to the requirement of cigarette, but method of smokeing panel test is with reference to the method for smokeing panel test of cigarette, the aesthetic quality of thin slice suction of the relatively high low reaction between score value).
Table 8 smoking result
Project | Fragrance | Harmony | Assorted gas | Stimulate | Pleasant impression | Total score |
Control sample | 24.0 | 4.0 | 8.0 | 16.0 | 17.0 | 69.0 |
Embodiment 1 | 25.0 | 4.5 | 8.0 | 17.0 | 19.0 | 73.5 |
Embodiment 2 | 25.0 | 4.5 | 8.5 | 17.0 | 19.0 | 74.0 |
Embodiment 3 | 25.5 | 4.5 | 8.5 | 17.0 | 19.0 | 74.5 |
Embodiment 4 | 25.5 | 4.5 | 8.0 | 17.0 | 19.0 | 74.0 |
Embodiment 5 | 25.0 | 4.5 | 8.5 | 17.0 | 19.5 | 75.5 |
Embodiment 6 | 25.5 | 4.5 | 8.5 | 17.0 | 19.0 | 74.5 |
Embodiment 7 | 25.0 | 4.5 | 8.5 | 17.0 | 19.0 | 74.0 |
Claims (10)
1. a humectation type reconstituted tobacoo, prepares coating solution in sheet paper base, it is characterized in that, described sheet paper base prepares through copy paper after being mixed by following slurry: count in mass ratio, Oroxylum indicum slurry, 10 ~ 30%; Giant knotweed slurry, 10 ~ 30%; Chinese actinidia root slurry, 10 ~ 30%; Purple perilla slurry, 10 ~ 30%; Offal slurry, 10 ~ 30%; Offal slurry, 5 ~ 30%;
The preparation method of described Oroxylum indicum slurry is: be raw material with Oroxylum indicum, filters after adding the water soaking of the solid sodium hydroxide of Oroxylum indicum quality 2% ~ 10% and 4 ~ 10 times, collects filter residue and carries out defibrination and obtain Oroxylum indicum slurry;
The preparation method of described giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry, offal slurry or offal slurry is: filter after the refluxing extraction that giant knotweed, Chinese actinidia root, purple perilla, offal or offal added water respectively, collects gained filter residue defibrination and get final product.
2. humectation type reconstituted tobacoo according to claim 1, is characterized in that, described sheet paper base prepares through copy paper after being mixed by following slurry: count in mass ratio, Oroxylum indicum slurry, 10 ~ 20%; Giant knotweed slurry, 10 ~ 20%; Chinese actinidia root slurry, 10 ~ 20%; Purple perilla slurry, 10 ~ 20%; Offal slurry, 20 ~ 30%; Offal slurry, 10 ~ 25%.
3. humectation type reconstituted tobacoo according to claim 1, is characterized in that described coating fluid is by quality ratio, comprises the functional perfumery of 1 ~ 10% and the offal extract of 90 ~ 99%.
4. humectation type reconstituted tobacoo according to claim 3, is characterized in that described coating fluid is by quality ratio, comprises the functional perfumery of 5 ~ 8% and the offal extract of 92 ~ 95%.
5. humectation type reconstituted tobacoo according to claim 1, is characterized in that, the applied amount of described coating fluid accounts for 5 ~ 50% of sheet paper base oven dry weight.
6. humectation type reconstituted tobacoo according to claim 5, is characterized in that, the applied amount of described coating fluid accounts for 30 ~ 36% of sheet paper base oven dry weight.
7. humectation type reconstituted tobacoo according to claim 1, it is characterized in that, the preparation method of described Oroxylum indicum slurry is: be raw material with Oroxylum indicum, filters after adding the water soaking of the solid sodium hydroxide of Oroxylum indicum quality 5% and 4 ~ 10 times, collects filter residue and carries out defibrination and obtain Oroxylum indicum slurry.
8. humectation type reconstituted tobacoo according to claim 1, is characterized in that, described in the add water amount of water of refluxing extraction be determine according to 4 ~ 10 times of quality of giant knotweed, Chinese actinidia root, purple perilla, offal or offal respectively; The reflux extracting time of the described refluxing extraction that adds water is 1 ~ 5 hour.
9. a preparation method for the arbitrary described humectation type reconstituted tobacoo of claim 1 to 8, is characterized in that, comprise the following steps:
S1. Oroxylum indicum slurry, giant knotweed slurry, Chinese actinidia root slurry, purple perilla slurry, offal slurry, offal slurry, offal extract is prepared respectively;
S2. example mixes the various slurry of S1 gained in mass ratio;
S3. by the slurry handsheet on a papermaking machine that S2 gained mixes, reconstituted tobacoo paper substrate is obtained;
S4. concentrated S1 gained offal extract, concentrates to obtain offal extract; By coating on reconstituted tobacoo paper substrate after offal extract and functional perfumery mixing, dry, to obtain final product.
10. the humectation type reconstituted tobacoo for preparing of preparation method described in claim 9.
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