CN103156271B - Shisha paste containing extractive from natural plant Tacca chantrieri Andre and preparation method thereof - Google Patents
Shisha paste containing extractive from natural plant Tacca chantrieri Andre and preparation method thereof Download PDFInfo
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- CN103156271B CN103156271B CN201110405563.5A CN201110405563A CN103156271B CN 103156271 B CN103156271 B CN 103156271B CN 201110405563 A CN201110405563 A CN 201110405563A CN 103156271 B CN103156271 B CN 103156271B
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Abstract
The invention discloses a shisha paste containing extractive from natural plant Tacca chantrieri Andre and a preparation method thereof, and belongs to the technical field of tobacco. The shisha paste containing the extractive from the natural plant Tacca chantrieri Andre is formed by mixing pipe tobacco and Tacca chantrieri Andre blending material diluent. 0.5-1.5 parts by weight of the Tacca chantrieri Andre blending material diluent are evenly sprayed into 100 parts by weight of the pipe tobacco. Tacca chantrieri Andre blending materials A are formed by blending of the extractive from the Tacca chantrieri Andre and honey. Tacca chantrieri Andre blending materials B are formed by blending of the extractive from the Tacca chantrieri Andre, the honey and oil. Tacca chantrieri Andre blending materials C are formed by blending of the extractive from the Tacca chantrieri Andre, the honey, the oil and the wine. The Tacca chantrieri Andre blending material diluent is mixed liquor which is obtained by diluting the Tacca chantrieri Andre blending materials A or the Tacca chantrieri Andre blending materials B or the Tacca chantrieri Andre blending materials C with water for 2-10 times. Raw materials used in the shisha paste containing the extractive from the natural plant Tacca chantrieri Andre are abundant in source and low in cost. The method processes are simple and easy to practice, the steps are few, repeatability of processes is high, processes can be freely combined, and effects of adding aroma and reducing harm are achieved.
Description
Technical field
The invention belongs to technical field of tobacco, be specifically related to a kind of prepared opium paste for shredded tobacco for water pipes suction containing extractive from natural plant Tacca chantrieri Andre, and the preparation method of this prepared opium paste.
Background technology
Flue gas filters by shredded tobacco for water pipes, endangers less compared with cigarette.At present, China's Some Minority Races area and all very popular employing hookah smoking of country in Southeast Asia and Arab countries, and be generally traditional Virginia tobacco for the tobacco of water pipe, comparatively large to the excitant of throat, mouthfeel is poor.Arabic shredded tobacco for water pipes is popular in America and Europe, and add the fruit cigarette that fruit meat makes various taste, tobacco only accounts for about 30%, and pulp accounts for 70%.Although the smell of fruits is very sweet for this shredded tobacco for water pipes, smoke is light, strictly speaking substantially can only a kind of fruit cigarette at last, and it is be difficult to adapt to and accept for inhaling the people of used cigarette or old smoker.
Tiger's whiskers is the root of Campanulaceae Lady bell plant apricot leaf the root of straight ladybell (Adenophorastricta Miq.) and adenophora tetraphylla (Adenophoratertrphylla (Thunb.) Fisch.), be born in clivia thick grass, border or roadside, originate in East China, Central-South and Sichuan.Tiger's whiskers begins to be loaded in Shennong's Herbal: " taste is sweet to be slightly cold, and main blood amasss frightened gas, except fever and chills, bowl spares benefit lung qi, takes sharp people for a long time." be one of the conventional Chinese herbal medicine of clearing lung and nourishing yin, eliminating phlegm and relieving cough, there is nourishiing yin to clear away the lung-heat, effect of reduce phlegm beneficial gas, expelling phlegm and arresting coughing.For controlling lung-heat type cough, void coughs chronic cough, cloudy wound is swallowed in laryngalgia etc., and quantity is 9 ~ 15g.Now in extensive use among the people, its fresh succulence, taste are sweet, fresh and crisp, and mouthfeel is good, nutrition price is high, are a kind of Chinese medicine of medicine-food two-purpose.Therefore tiger's whiskers has wide development prospect.The principle active component of tiger's whiskers is saponins, is a kind of triterpenoid saponin be present in natural plants, has important physiology and pharmacologically active, has good eliminating phlegm and relieving cough effect, can treat the disease such as pneumonia, acute episode of chronic tracheitis.The infringement of bibliographical information moistening lung Chinese medicine to active smoking mice respiratory tract has protective effect.Tiger's whiskers help composition is mainly polysaccharide, more to the research of tiger's whiskers polysaccharide at present, but less to its saponin component research with relieving cough and reducing sputum effect.Extractive from natural plant Tacca chantrieri Andre is used for the prepared opium paste of shredded tobacco for water pipes suction, and the preparation method of this prepared opium paste is not reported.
Summary of the invention
For the above-mentioned deficiency of prior art, the technical problem to be solved in the present invention is to provide a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre and preparation method thereof, Shisha paste of the present invention is based on pipe tobacco, be furnished with tiger's whiskers extract and relieving cough and reducing sputum function is provided, make Shisha paste can adapt to the demand of most smoker, there is the advantage reducing throat's excitant, reduce infringement simultaneously.
Technical scheme of the present invention is: a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre is mixed by pipe tobacco and tiger's whiskers composite dilution, and in the pipe tobacco of 100 parts of weight, evenly spray adds the tiger's whiskers composite dilution of 0.5 ~ 1.5 part of weight; Described tiger's whiskers composite A is allocated by tiger's whiskers extract and honey to form, and described tiger's whiskers composite B allocate by tiger's whiskers extract and honey and oil to form, and described tiger's whiskers composite C to be allocated with oily and wine by tiger's whiskers extract and honey to form; Described tiger's whiskers composite dilution tiger's whiskers composite A or tiger's whiskers composite B or tiger's whiskers composite C is diluted with water the mixed liquor of 2 ~ 10 times.
Tiger's whiskers extract in described tiger's whiskers composite A: the mass ratio of honey is 80 ~ 95 parts: 5 ~ 20 parts.Tiger's whiskers extract in described tiger's whiskers composite B: honey: the mass ratio of oil is 80 ~ 95 parts: 2.5 ~ 15 parts: 2.5 ~ 5 parts.Tiger's whiskers extract in described tiger's whiskers composite C: honey: oil: the mass ratio of wine is 80 ~ 90 parts: 4 ~ 10 parts: 3 ~ 5 parts: 3 ~ 5 parts.Described oil is olive oil or sesame oil; Described wine is white wine or grape wine or Rum.
A kind of preparation method of the Shisha paste containing extractive from natural plant Tacca chantrieri Andre carries out according to the following steps successively:
[1] dry tiger's whiskers root is crushed to meal, load in filter opening specification 0.5 μm of filter bag, put into the extraction still of pressure fluid abstraction instrument, add percentage by weight 95% ethanol, ratio is tiger's whiskers meal 20g: 95% ethanol 300 ~ 400mL, soaked overnight;
[2] setting program of pressure fluid abstraction instrument is pressurization 3min, normal pressure 3min, circulates 240 times, carries out continuous circulation extraction, remove filter bag and interior tiger's whiskers powder thereof after extraction, retain extract;
[3] in extract, add absolute ethyl alcohol, volume ratio is extract: absolute ethyl alcohol=0.5 ~ 1: 1, is placed in after 4 DEG C of environment precipitate a night and filters, get supernatant and continue to employ, be called tiger's whiskers extract after filtration;
[4] to be relative density by tiger's whiskers extract reduced pressure concentration be 1.2 ~ 1.3 medicinal extract, be called tiger's whiskers extract;
[5] tiger's whiskers extract is made tiger's whiskers composite
(1) tiger's whiskers extract: the mass percent of honey is 80 ~ 95 parts: 5 ~ 20 parts, mixes, and is called tiger's whiskers composite A;
(2) tiger's whiskers extract: honey: the mass percent of oil is 80 ~ 95 parts: 2.5 ~ 15 parts: 2.5 ~ 5 parts, mix, be called tiger's whiskers composite B;
(3) tiger's whiskers extract: honey: oil: the mass ratio of wine is 80 ~ 90 parts: 4 ~ 10 parts: 3 ~ 5 parts: 3 ~ 5 parts, mixes, is called tiger's whiskers composite C;
[6] tiger's whiskers composite diluent A or tiger's whiskers composite dilution B or tiger's whiskers composite dilution C are made in the cold boiling water dilution 2 ~ 10 times of tiger's whiskers composite A or tiger's whiskers composite B or tiger's whiskers composite C;
[7] tiger's whiskers composite diluent A or tiger's whiskers composite dilution B or tiger's whiskers composite dilution C are sprayed onto in pipe tobacco by the ratio uniform of pipe tobacco gross weight 0.5 ~ 1.5%, in placing container airtight 5 ~ 10 days, namely obtain the Shisha paste containing extractive from natural plant Tacca chantrieri Andre of the present invention.
Described oil is olive oil or sesame oil; Described wine is white wine or grape wine or Rum.Described pipe tobacco adopts the better-than-average level tobacco leaf combination both domestic and external of one to multiple kind, will combine tobacco leaf and remove after leaf obstructs also chopping, then to stir-fry the pipe tobacco obtained for 5 ~ 10 minutes through little fire; Described little fire stir-fries and refers to that the temperature that stir-fries is 60 ~ 80 DEG C.
The abundant raw material source that the present invention is used, cost is low; Method technical process is simple, and step is few, and technical process repeatability is high, and can independent assortment, produces flavouring harm reduction effect.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is described in further detail.Be necessary that herein means out following specific embodiment just further illustrates of the present invention, does not represent limiting the scope of the invention.Some nonessential amendment and adjustment that other people make according to the present invention, still belong to protection scope of the present invention.
First the present invention is described compared with the prior art below, its advantage and beneficial effect as follows: the present invention takes normal temperature circulation of pressurized fluid reflux extraction mode, will extract with extraction two steps is combined, minimizing method step; The impurity such as protein, starch major part in tiger's whiskers extract being affected shredded tobacco for water pipes suction taste is abandoned in residue, direct extraction bioactive ingredients tiger's whiskers total saposins and aroma volatile are in extract, higher than traditional cold soaking (generally need 3 months even half a year more than) efficiency, specific heat alcohol lixiviate impurity is few, and aroma volatile and bioactive ingredients retain many; Gained tiger's whiskers extract and honey are allocated, and suck through shredded tobacco for water pipes, and make flue gas fine and smooth, smooth and easy, enrich cigarette perfume (or spice), have back sweet sense, sweet felling, excitement is less.Gained tiger's whiskers extract and honey, oil are allocated, make medicinal extract surface produce oil film to be beneficial to and to reduce volatile ingredient dissipation and bioactive ingredients oxidation deterioration, and can coordinate with flue gas after oil and pipe tobacco mixed combustion, fine and smooth smooth and easy, enrich cigarette perfume (or spice), increase flue gas light fragrant and sweet, excitement is less.Gained tiger's whiskers extract is allocated together with honey, oil, wine, can coordinate with flue gas, increase fine and smooth smooth and easy sense, enrich cigarette perfume (or spice), increase flue gas return sweet sense and aroma, excitement is less.Tiger's whiskers bioactive ingredients total saposins etc. are along with imperfect combustion flue gas fast and by entering respiratory system after water filtration, the discomfort that smoking produces human body throat can be alleviated, make flue gas fine and smooth, soft, reduce the stimulation degree to throat, and play the effect of certain cough-relieving apophlegmatic, reduce the harmfulness of shredded tobacco for water pipes flue gas.The abundant raw material source that the present invention is used, cost is low; Method technical process is simple, and step is few, and technical process repeatability is high, and can independent assortment, produces flavouring harm reduction effect.
Dry tiger's whiskers root is crushed to meal by embodiment 1., and load in filter opening specification 0.5 μm of filter bag, put into the extraction still of pressure fluid abstraction instrument, add the ethanol of percentage by weight 95%, ratio is tiger's whiskers meal 20g: 95% ethanol 350mL, soaked overnight; The setting program of pressure fluid abstraction instrument is pressurization 3min, normal pressure 3min, circulates 240 times, carries out continuous circulation extraction, remove filter bag and interior tiger's whiskers powder thereof after extraction, retain extract; Absolute ethyl alcohol is added in extract, volume ratio is extract: absolute ethyl alcohol=0.5: 1, be placed in after 4 DEG C of environment precipitate a night and filter, get supernatant after filtration to continue to employ, to be relative density by supernatant reduced pressure concentration be 1.225 medicinal extract, allocate with honey, mass percent is tiger's whiskers extract: honey is 85 parts: 15 parts, mix, be called tiger's whiskers composite A; Dilute 2 times with cold boiling water and become tiger's whiskers composite diluent A, be sprayed onto in pipe tobacco by the ratio uniform of pipe tobacco gross weight 0.5%, in placing container airtight 7 days, namely obtain the Shisha paste containing extractive from natural plant Tacca chantrieri Andre of the present invention.
Dry tiger's whiskers root is crushed to meal by embodiment 2., and load in filter opening specification 0.5 μm of filter bag, put into the extraction still of pressure fluid abstraction instrument, add percentage by weight 95% ethanol, ratio is tiger's whiskers meal 20g: 95% ethanol 400mL, soaked overnight; The setting program of pressure fluid abstraction instrument is pressurization 3min, normal pressure 3min, circulates 240 times, carries out continuous circulation extraction, remove filter bag and interior tiger's whiskers powder thereof after extraction, retain extract; Absolute ethyl alcohol is added in extract, volume ratio is extract: absolute ethyl alcohol=0.5: 1, be placed in after 4 DEG C of environment precipitate a night and filter, get supernatant after filtration to continue to employ, to be relative density by supernatant reduced pressure concentration be 1.212 medicinal extract, allocate with honey, oil, tiger's whiskers extract: honey: oily mass percent is 80 parts: 10 parts: 10 parts, mix, be called tiger's whiskers composite B; Dilute 5 times with cold boiling water and become tiger's whiskers composite dilution B, be sprayed onto in pipe tobacco by the ratio uniform of pipe tobacco gross weight 1.0%, in placing container airtight 6 days, namely obtain the Shisha paste containing extractive from natural plant Tacca chantrieri Andre of the present invention.
Dry tiger's whiskers root is crushed to meal by embodiment 3., and load in filter opening specification 0.5 μm of filter bag, put into the extraction still of pressure fluid abstraction instrument, add percentage by weight 95% ethanol, ratio is tiger's whiskers meal 20g: 95% ethanol 300mL, soaked overnight; The setting program of pressure fluid abstraction instrument is pressurization 3min, normal pressure 3min, circulates 240 times, carries out continuous circulation extraction, remove filter bag and interior tiger's whiskers powder thereof after extraction, retain extract; Absolute ethyl alcohol is added in extract, volume ratio is extract: absolute ethyl alcohol=1: 1, be placed in after 4 DEG C of environment precipitate a night and filter, get supernatant after filtration to continue to employ, to be relative density by supernatant reduced pressure concentration be 1.268 medicinal extract, allocate with honey, oil, wine, tiger's whiskers extract: honey: oil: the mass ratio of wine is 85 parts: 5 parts: 5 parts: 5 parts, mix, be called tiger's whiskers composite C; Dilute 10 times with cold boiling water and become tiger's whiskers composite dilution C, be sprayed onto in pipe tobacco by the ratio uniform of pipe tobacco gross weight 1.5%, in placing container airtight 9 days, namely obtain the Shisha paste containing extractive from natural plant Tacca chantrieri Andre of the present invention.
For inquiring into the flavouring effect of above-mentioned natural plants tiger's whiskers Shisha paste, the applicant compared for tiger's whiskers Shisha paste and the shredded tobacco for water pipes sensory evaluation effect of not adding tiger's whiskers composite Shisha paste, and result is as shown in table 1,2,3,4;
Table 1, the Shisha paste sensory evaluating smoking containing extractive from natural plant Tacca chantrieri Andre made with tiger's whiskers composite A
Note: in this table, data are is reference with the light water prepared opium paste of equal pipe tobacco, following form with.
Table 2, the Shisha paste sensory evaluating smoking containing extractive from natural plant Tacca chantrieri Andre made with tiger's whiskers composite B
Table 3, the Shisha paste sensory evaluating smoking containing extractive from natural plant Tacca chantrieri Andre made with tiger's whiskers composite C
Table 4. Shisha paste sensory evaluation of the present invention effect Comprehensive Correlation
As seen from the above table, natural plants tiger's whiskers Shisha paste can enrich cigarette perfume (or spice), make flue gas fine and smooth, smooth and easy, increase flue gas sweet sense (with wine allotment can increase aroma), reduce throat's excitement.
The extractive from natural plant Tacca chantrieri Andre that the applicant also prepares the inventive method has carried out the efficacy assessments of cough-relieving apophlegmatic, as shown in table 5:
Adopt ammonia induced cough in mice and cavy citric acid to draw to cough legal system to make cough model and evaluate antitussive effect; Phlegm-dispelling functions is evaluated with mouse PSP method.
Ammonia induced cough in mice: the male mice getting body weight 18 ~ 22g, be divided into control group, H ~ 11 group, H ~ 12 group, H ~ 13 group, H ~ 14 group and H ~ 15 groups totally 6 groups at random, often organize 15, press 0.2ml/10g gavage every day to tiger's whiskers extract, for three days on end, control group gives the physiological saline of Isodose, gives mouse stomach physiological saline 3 days continuously.Last to 1h after tiger's whiskers extract or physiological saline, mouse is placed in wide-mouth bottle, spray into concentrated ammonia liquor, the time is put in immediate record, observe and record cough latent period and cough number of times in 2 minutes, in 12min, in 22min, whether reducing to evaluate antitussive effect with number of times of coughing compared with blank; And survey mouse tracheae section phenols contents and OD value (the absorption OD value of detected material) with ultraviolet specrophotometer, judge that there is phlegm-dispelling functions with the rising of OD value.
The Antitussive and Expectorant Effect of table 5 tiger's whiskers extract
* P < 0.05, * * P < 0.01 compares with control group
As seen from the above table, tiger's whiskers extract has antibechic and phlegm-dispelling functions simultaneously.
Claims (8)
1. containing a Shisha paste for extractive from natural plant Tacca chantrieri Andre, it is characterized in that: described Shisha paste is mixed by pipe tobacco and tiger's whiskers composite dilution, in the pipe tobacco of 100 parts of weight, evenly spray adds the tiger's whiskers composite dilution of 0.5 ~ 1.5 part of weight; The tiger's whiskers composite A of described tiger's whiskers composite is allocated by tiger's whiskers extract and honey to form, the tiger's whiskers composite B of described tiger's whiskers composite allocate by tiger's whiskers extract and honey and oil to form, and the tiger's whiskers composite C of described tiger's whiskers composite to be allocated with oily and wine by tiger's whiskers extract and honey to form; Described tiger's whiskers composite dilution tiger's whiskers composite A or tiger's whiskers composite B or tiger's whiskers composite C is diluted with water the mixed liquor of 2 ~ 10 times.
2. a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre according to claim 1, is characterized in that: tiger's whiskers extract in described tiger's whiskers composite A: the mass ratio of honey is 80 ~ 95 parts: 5 ~ 20 parts.
3. a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre according to claim 1, is characterized in that: tiger's whiskers extract in described tiger's whiskers composite B: honey: the mass ratio of oil is 80 ~ 95 parts: 2.5 ~ 15 parts: 2.5 ~ 5 parts.
4. a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre according to claim 1, is characterized in that: tiger's whiskers extract in described tiger's whiskers composite C: honey: oil: the mass ratio of wine is 80 ~ 90 parts: 4 ~ 10 parts: 3 ~ 5 parts: 3 ~ 5 parts.
5. a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre according to claim 1, is characterized in that: described oil is olive oil or sesame oil; Described wine is white wine or grape wine or Rum.
6., containing a preparation method for the Shisha paste of extractive from natural plant Tacca chantrieri Andre, it is characterized in that described method is carried out according to the following steps successively:
[1] dry tiger's whiskers root is crushed to meal, load in filter opening specification 0.5 μm of filter bag, put into the extraction still of pressure fluid abstraction instrument, add the ethanol of percentage by weight 95%, ratio is tiger's whiskers meal 20g:95% ethanol 300 ~ 400mL, soaked overnight;
[2] setting program of pressure fluid abstraction instrument is pressurization 3min, normal pressure 3min, circulates 240 times, carries out continuous circulation extraction, remove filter bag and interior tiger's whiskers powder thereof after extraction, retain extract;
[3] in extract, add absolute ethyl alcohol, volume ratio is extract: absolute ethyl alcohol=0.5 ~ 1:1, is placed in after 4 DEG C of environment precipitate a night and filters, get supernatant and continue to employ, be called tiger's whiskers extract after filtration;
[4] to be relative density by tiger's whiskers extract reduced pressure concentration be 1.2 ~ 1.3 medicinal extract, be called tiger's whiskers extract;
[5] tiger's whiskers extract is made tiger's whiskers composite
(1) tiger's whiskers extract: the mass percent of honey is 80 ~ 95 parts: 5 ~ 20 parts, mixes, and is called tiger's whiskers composite A;
(2) tiger's whiskers extract: honey: the mass percent of oil is 80 ~ 95 parts: 2.5 ~ 15 parts: 2.5 ~ 5 parts, mix, be called tiger's whiskers composite B;
(3) tiger's whiskers extract: honey: oil: the mass ratio of wine is 80 ~ 90 parts: 4 ~ 10 parts: 3 ~ 5 parts: 3 ~ 5 parts, mixes, is called tiger's whiskers composite C;
[6] tiger's whiskers composite diluent A or tiger's whiskers composite dilution B or tiger's whiskers composite dilution C are made in the cold boiling water dilution 2 ~ 10 times of tiger's whiskers composite A or tiger's whiskers composite B or tiger's whiskers composite C;
[7] tiger's whiskers composite diluent A or tiger's whiskers composite dilution B or tiger's whiskers composite dilution C are sprayed onto in pipe tobacco by the ratio uniform of pipe tobacco gross weight 0.5 ~ 1.5%, in placing container airtight 5 ~ 10 days, namely obtain the Shisha paste containing extractive from natural plant Tacca chantrieri Andre of the present invention.
7. the preparation method of a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre according to claim 6, is characterized in that described oil is olive oil or sesame oil; Described wine is white wine or grape wine or Rum.
8. the preparation method of a kind of Shisha paste containing extractive from natural plant Tacca chantrieri Andre according to claim 6, it is characterized in that: described pipe tobacco adopts the better-than-average level tobacco leaf combination both domestic and external of one to multiple kind, tobacco leaf will be combined and remove leaf stalk and after chopping, then stir-fry the pipe tobacco obtained for 5 ~ 10 minutes through little fire; Described little fire stir-fries and refers to that the temperature that stir-fries is 60 ~ 80 DEG C.
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| CN104473320B (en) * | 2014-11-20 | 2016-08-17 | 深圳梵活生物科技有限公司 | A kind of shredded tobacco for water pipes sarcocarp preparation method on Water pipe |
| CN104786682A (en) * | 2015-03-12 | 2015-07-22 | 云南中烟工业有限责任公司 | Offline embossed cigarette paper making method and offline embossed cigarette paper |
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