CN103141567A - Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof - Google Patents

Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof Download PDF

Info

Publication number
CN103141567A
CN103141567A CN2013101009051A CN201310100905A CN103141567A CN 103141567 A CN103141567 A CN 103141567A CN 2013101009051 A CN2013101009051 A CN 2013101009051A CN 201310100905 A CN201310100905 A CN 201310100905A CN 103141567 A CN103141567 A CN 103141567A
Authority
CN
China
Prior art keywords
preparation
antistaling agent
chinese herbal
starch
herbal medicine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101009051A
Other languages
Chinese (zh)
Inventor
王金玉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN2013101009051A priority Critical patent/CN103141567A/en
Publication of CN103141567A publication Critical patent/CN103141567A/en
Pending legal-status Critical Current

Links

Landscapes

  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a Litchi chinensis preservative based on Chinese medicinal herbs and a preparation method thereof. The preservative comprises the following materials in percentage by weight: 8-12% of galangal, 2-8% of radix stemonae, 5-10% of encalyptus robusta, 3-8% of Saxifraga stolonifera, 5-10% of honeysuckle, 8-12% of berberine, 2-5% of Astragalus mongholicus, 2-8% of garlic, 3-10% of konjaku flour, 1-5% of agar, 1-5% of lecithin, 10-15% of starch and 50-80% of water. The preparation method comprises the following steps of: preparation of a Chinese medicinal herb extraction liquid, preparation of gelatinized starch, preparation of preservative and the like. The materials used by the invention are natural Chinese medicinal herbs, so that the preservative is remarkable in preservative effect, long in preservative time, free from chemical residue and environmental-friendly, and is simple in preparation process, low in production cost, and has wide market prospect.

Description

A kind of antistaling agent for litchi based on Chinese herbal medicine and preparation method thereof
Technical field
The present invention relates to a kind of fruit antistaling agent, particularly relate to a kind of antistaling agent for litchi based on Chinese herbal medicine and preparation method thereof.
Background technology
Lichee originates in China, is the good fruit in the Chinese south of the Five Ridges, and its color is all beautiful, has won fame both at home and abroad, and has the title of " fruit king ", is distributed in Guangdong, Guangxi, Fujian, Sichuan, Taiwan and Yunnan.After but lichee is adopted very easily brown stain rot, among the people have: " its food lichee one day and look becomes, two days and fragrant the change, three days and flavor becomes, four, multicolored fragrance goes " saying.Because lichee contained humidity, sugar are higher, the physiological property such as pericarp is rich in tannin, and polyphenol oxidase and peroxidase activity are very strong is midsummer when adding maturation, and moisture evaporation, germ easily grow, so very easily brown stain is corrupt, freshness date is extremely short.The perishable characteristics of lichee have had a strong impact on finding a good sale in of this fruit and shelf life.China is the maximum country of plantation lichee at present, and according to statistics, the annual loss that causes because rotting of lichee accounts for more than 20% of total output, causes huge economic loss.As seen the preservation technique of lichee seems particularly important.
The antistaling agent that is used at present lichee mainly contains chemical preservative and bio-preservative, chemical preservative comprises antiseptic drug commonly used such as benomyl, TBZ, sterilization prestige, and the organic acids such as sulphuring or citric acid are processed, the method is fresh-keeping and bactericidal effect is better, but have chemical residual, safety coefficient is not high, and people's health is threatened.The material source of bio-preservative comprises natural animal-plant extract or its compound in nature, and especially the biological film-coating method was constantly developed in recent years.The method be with natural macromolecular materials such as polysaccharide, protein and greases as smearing material, and be coated in fruit surface with the state of the aqueous solution or emulsion, form film after it is dry.This layer film can prevent that moisture evaporation, the physiological biochemical reaction of regulating plant and delayed fruit are old and feeble and corrupt, has again the effects such as the bacterium of preventing infringement.The advantages such as that the natural biological coating antistaling agent has is natural, environmental protection, good refreshing effect, that is that all right is ripe due to its technology, and the material requested cost is higher, is unfavorable for promoting.
Summary of the invention
For above-mentioned deficiency, technical problem to be solved by this invention is to provide a kind of environmental protection of adopting the Chinese herbal medicine material to make, without chemical agent, and production cost is low, good refreshing effect, antistaling agent for litchi that fresh keeping time is long and preparation method thereof.
For addressing the above problem, the present invention is achieved through the following technical solutions:
A kind of antistaling agent for litchi based on Chinese herbal medicine is comprised of the material of following percentage by weight:
Galingal 8~12%, the tuber of stemona 2~8%, eucalyptus robusta 5~10%, kiss-me 3~8%, honeysuckle 5~10%, berberine 8~12%, the Radix Astragali 2~5%, garlic 2~8%, konjaku flour 3~10%, agar 1~5%, lecithin 1~5%, starch 10~15%, water 50~80%.
In such scheme, preferably, described starch is one or both in cornstarch, starch from sweet potato.
The preparation method of above-mentioned a kind of antistaling agent for litchi based on Chinese herbal medicine comprises the following steps:
(1) preparation of extracts of Chinese herbal medicine: first water is mixed by 4:1 with ethanol, with this as extract; Again above-mentioned galingal, the tuber of stemona, eucalyptus robusta, kiss-me, honeysuckle, berberine, the Radix Astragali, 8 kinds of Chinese herbal medicines of garlic are added in the container of heat resisting and pressure resisting, and add the ethanol extract for preparing, its amount to be 5~10 times of Chinese herbal medicine weight; Then extract 10~30min at 20~100MPa and 200~350 ℃ of temperature, then step-down is cooled to normal temperature and pressure, isolates the medium-height grass the effective elements of the medicine, discard the dregs of a decoction, namely get the primary raw material of described antistaling agent;
(2) gelatinized starch preparation: cornstarch or starch from sweet potato are carried out gelatinization with Pasting machine at the temperature of 98~180 ℃, crushed after being dried namely gets gelatinized starch, in order to the crosslinked strengthening agent of antistaling agent;
(3) antistaling agent preparation: gelatinized starch, extracts of Chinese herbal medicine, konjaku flour, lecithin, agar are added in another container, and uniform stirring, mixing 15~30min namely get described antistaling agent finished product.
The fresh-keeping mechanism of the present invention is:
Galingal: belong to zingiberaceous plant.Warm in nature, bitter is hot.The function promoting the circulation of qi, invigorate blood circulation, pain relieving.
The tuber of stemona: also claim Radix stemonae japonicae, perennial herb.The underground spindle shape meat piece root that clusters.On traditional Chinese medicine with piece root people medicine.Slightly warm in nature, bitter but sweet flavor.The cough-relieving of function temperature lung, desinsection.One of this agent primary raw material is as pesticide.
Eucalyptus robusta: the little suffering of property, mildly bitter flavor, flat.Cure mainly dispelling wind analgesic, inhibiting bacteria and diminishing inflammation, anticorrosion antipruritic.One of this agent primary raw material is as bactericide.
Kiss-me: be commonly called as the spun gold lotus leaf.Saxifragaceae.Perennial herb.Leaf is grown thickly along ground, the meat succulence, the kidney shape is heart-shaped, below aubergine.Summer-flowering, floral white, panicle.On traditional Chinese medicine with herb people medicine.Cold in nature, the hot little hardship of distinguishing the flavor of.Function is clearing heat and detoxicating.
Honeysuckle: lightly seasoned, little hardship, have clearing heat and detoxicating, dispelling wind and heat from the body, cool blood stops clever, falls blood and falls fire, the effect of anti-inflammatory profit diaphragm.
Berberine: also claim jamaicin.From a kind of antibiotic property alkaloid that Chinese Drug Rhizomes of Coptis, golden cypress (cork tree) etc. propose, its hydrochloride is yellow powder, and bitter is slightly soluble in water.Shigella dysenteriae, tubercle bacillus, staphylococcus etc. there is inhibitory action.Be used as anticorrisive agent in this agent.
The Radix Astragali: distinguish the flavor of sweet, temperature is returned lung channel, the spleen channel, has antibacterial action more widely.
Konjaku flour: have another name called the snake hexagonal.Belong to the polysaccharide of carbohydrate, contain a large amount of many contractings grape sweet mellow wine.Pale yellow powder.Nontoxic, fishy smell is arranged.Hygroscopicity is strong.Soluble in water.Chemical stability is good, acidproof, antioxidant and reducing agent.Meeting the alkali retrogradation freezes.Have good film-forming property, transparency advantages of higher.Be used as film forming agent in this agent, select pharmaceutical grade.
The invention has the beneficial effects as follows: the material that the present invention uses is comprised of natural medicinal herb components, and fresh-keeping effect is remarkable, fresh keeping time is long, and without chemical residual, environmental protection, and production cost is low, has wide market prospects.
The specific embodiment
Below by specific embodiment, the present invention is further explained explanation, but does not limit the present invention.
A kind of antistaling agent for litchi based on Chinese herbal medicine is comprised of the material of following percentage by weight: galingal 8%, the tuber of stemona 3%, eucalyptus robusta 5%, kiss-me 4%, honeysuckle 5%, berberine 8%, the Radix Astragali 2%, garlic 3%, konjaku flour 5%, agar 3%, lecithin 4%, starch 10%, water 50%.
In the present embodiment, described starch is cornstarch.
The preparation method of described a kind of antistaling agent for litchi based on Chinese herbal medicine comprises the following steps:
(1) preparation of extracts of Chinese herbal medicine: first water is mixed by 4:1 with ethanol, with this as extract; Again above-mentioned galingal, the tuber of stemona, eucalyptus robusta, kiss-me, honeysuckle, berberine, the Radix Astragali, 8 kinds of Chinese herbal medicines of garlic are added in the container of heat resisting and pressure resisting, and add the ethanol extract for preparing, its amount to be 5~10 times of Chinese herbal medicine weight; Then extract 10~30min at 20~100MPa and 200~350 ℃ of temperature, then step-down is cooled to normal temperature and pressure, isolates the medium-height grass the effective elements of the medicine, discard the dregs of a decoction, namely get the primary raw material of described antistaling agent;
(2) gelatinized starch preparation: cornstarch or starch from sweet potato are carried out gelatinization with Pasting machine at the temperature of 98~180 ℃, crushed after being dried namely gets gelatinized starch, in order to the crosslinked strengthening agent of antistaling agent;
(3) antistaling agent preparation: gelatinized starch, extracts of Chinese herbal medicine, konjaku flour, lecithin, agar are added in another container, and uniform stirring, mixing 15~30min namely get described antistaling agent finished product.
The antistaling agent for litchi that according to said method makes is pasty state.During use, will fresh-keeping lichee be immersed in described antistaling agent after 1~3min, take out, be placed on the shady and cool dry place that ventilates and dry and get final product.Can preserve at the temperature of 10~15 ℃ 32~45 days through the lichee that the method is fresh-keeping.
Embodiment 2:
A kind of antistaling agent for litchi based on Chinese herbal medicine is comprised of the material of following percentage by weight: galingal 12%, the tuber of stemona 8%, eucalyptus robusta 10%, kiss-me 8%, honeysuckle 8%, berberine 10%, the Radix Astragali 5%, garlic 8%, konjaku flour 10%, agar 5%, lecithin 5%, starch 15%, water 80%.
In the present embodiment, described starch is starch from sweet potato.
The preparation method of described a kind of antistaling agent for litchi based on Chinese herbal medicine is identical with embodiment 1.
The antistaling agent for litchi that makes by the method for embodiment 1 is pasty state.During use, will fresh-keeping lichee be immersed in described antistaling agent after 1~3min, take out, be placed on the shady and cool dry place that ventilates and dry and get final product.Can preserve at the temperature of 10~15 ℃ 40~55 days through the lichee that the method is fresh-keeping.
Embodiment 3:
A kind of antistaling agent for litchi based on Chinese herbal medicine is comprised of the material of following percentage by weight: galingal 10%, the tuber of stemona 5%, eucalyptus robusta 6%, kiss-me 5%, honeysuckle 5%, berberine 8%, the Radix Astragali 3%, garlic 7%, konjaku flour 8%, agar 5%, lecithin 5%, starch 12%, water 70%.
In the present embodiment, described starch is cornstarch and starch from sweet potato.
The preparation method of described a kind of antistaling agent for litchi based on Chinese herbal medicine is identical with embodiment 1.
The antistaling agent for litchi that makes by the method for embodiment 1 is pasty state.During use, will fresh-keeping lichee be immersed in described antistaling agent after 1~3min, take out, be placed on the shady and cool dry place that ventilates and dry and get final product.Can preserve at the temperature of 10~15 ℃ 35~50 days through the lichee that the method is fresh-keeping.

Claims (3)

1. antistaling agent for litchi based on Chinese herbal medicine is characterized in that being comprised of the material of following percentage by weight:
Galingal 8~12%, the tuber of stemona 2~8%, eucalyptus robusta 5~10%, kiss-me 3~8%, honeysuckle 5~10%, berberine 8~12%, the Radix Astragali 2~5%, garlic 2~8%, konjaku flour 3~10%, agar 1~5%, lecithin 1~5%, starch 10~15%, water 50~80%.
2. a kind of antistaling agent for litchi based on Chinese herbal medicine according to claim 1, it is characterized in that: described starch is one or both in cornstarch, starch from sweet potato.
3. the preparation method of according to claim 1~2 described a kind of antistaling agent for litchi based on Chinese herbal medicine is characterized in that comprising the following steps:
(1) preparation of extracts of Chinese herbal medicine: first water is mixed by 4:1 with ethanol, with this as extract; Again above-mentioned galingal, the tuber of stemona, eucalyptus robusta, kiss-me, honeysuckle, berberine, the Radix Astragali, 8 kinds of Chinese herbal medicines of garlic are added in the container of heat resisting and pressure resisting, and add the ethanol extract for preparing, its amount to be 5~10 times of Chinese herbal medicine weight; Then extract 10~30min at 20~100MPa and 200~350 ℃ of temperature, then step-down is cooled to normal temperature and pressure, isolates the medium-height grass the effective elements of the medicine, discard the dregs of a decoction, namely get the primary raw material of described antistaling agent;
(2) gelatinized starch preparation: cornstarch or starch from sweet potato are carried out gelatinization with Pasting machine at the temperature of 98~180 ℃, crushed after being dried namely gets gelatinized starch, in order to the crosslinked strengthening agent of antistaling agent;
(3) antistaling agent preparation: gelatinized starch, extracts of Chinese herbal medicine, konjaku flour, lecithin, agar are added in another container, and uniform stirring, mixing 15~30min namely get described antistaling agent finished product.
CN2013101009051A 2013-03-27 2013-03-27 Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof Pending CN103141567A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013101009051A CN103141567A (en) 2013-03-27 2013-03-27 Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013101009051A CN103141567A (en) 2013-03-27 2013-03-27 Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof

Publications (1)

Publication Number Publication Date
CN103141567A true CN103141567A (en) 2013-06-12

Family

ID=48540128

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2013101009051A Pending CN103141567A (en) 2013-03-27 2013-03-27 Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof

Country Status (1)

Country Link
CN (1) CN103141567A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103907677A (en) * 2014-03-24 2014-07-09 王金玉 Method for keeping carambola fresh
CN104489065A (en) * 2014-12-30 2015-04-08 北海万物盛生物技术开发有限公司 Method for preparing litchi preservative by utilizing natural plants
CN104957243A (en) * 2015-06-11 2015-10-07 邹健 Litchi storage and preservation method
CN108651611A (en) * 2017-03-28 2018-10-16 许昌学院 A kind of special crude antistaling agent of lichee and preparation method thereof

Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86101578A (en) * 1986-03-14 1987-01-24 哈尔滨工业大学 Chinese herbal medicine composite semipermeable membrane antistaling agent and manufacture method
CN1052414A (en) * 1989-12-14 1991-06-26 郭玉生 A kind of egg antistaling agent
CN1108951A (en) * 1994-10-31 1995-09-27 姜宗本 Antiphlogistic and sterilizing disinfectant and its preparation
CN1227717A (en) * 1998-03-03 1999-09-08 孟宪忠 Meat food preserving agent and its preparing process
CN1232621A (en) * 1998-04-22 1999-10-27 黎光海 Longan and litchi fresh-keeping agent and its compounding process
CN1302547A (en) * 1999-12-31 2001-07-11 曾稳清 Antistaling disinfectant and its preparing process and usage
CN1359626A (en) * 2002-01-11 2002-07-24 邹宇超 Process for preparing antistaling agent of fruit and vegetable
CN1389162A (en) * 2001-06-06 2003-01-08 王全根 Pollution-less bioactive food preservative and its prepn.
CN1398541A (en) * 2001-07-25 2003-02-26 赵旭洪 Natural food preservative
CN1488261A (en) * 2002-10-11 2004-04-14 黄海雄 Litchi chinensis and longar antistaling agent and use method
CN1541066A (en) * 2001-06-28 2004-10-27 Compsn. for coating fruis, vegetables and fowl eggs, esp. useful for organic produce
CN101366524A (en) * 2008-09-28 2009-02-18 高思 Fresh fruit processed health preserving pot food
CN101427705A (en) * 2008-12-02 2009-05-13 南京师范大学 Chinese medicinal herb antistaling agent for stem vegetables
CN101810218A (en) * 2010-04-23 2010-08-25 青田稼泷食品有限公司 Red bayberry preservative based on Chinese herbal medicines and preparation method thereof
CN101836673A (en) * 2010-05-20 2010-09-22 中山市先禾生物科技有限公司 Chinese medicinal refreshing fruit wax
CN102907226A (en) * 2012-10-13 2013-02-06 合肥市艳九天农业科技有限公司 Fresh-preservation and nuisance-free cultivation method for greenhouse strawberries

Patent Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86101578A (en) * 1986-03-14 1987-01-24 哈尔滨工业大学 Chinese herbal medicine composite semipermeable membrane antistaling agent and manufacture method
CN1052414A (en) * 1989-12-14 1991-06-26 郭玉生 A kind of egg antistaling agent
CN1108951A (en) * 1994-10-31 1995-09-27 姜宗本 Antiphlogistic and sterilizing disinfectant and its preparation
CN1227717A (en) * 1998-03-03 1999-09-08 孟宪忠 Meat food preserving agent and its preparing process
CN1232621A (en) * 1998-04-22 1999-10-27 黎光海 Longan and litchi fresh-keeping agent and its compounding process
CN1302547A (en) * 1999-12-31 2001-07-11 曾稳清 Antistaling disinfectant and its preparing process and usage
CN1389162A (en) * 2001-06-06 2003-01-08 王全根 Pollution-less bioactive food preservative and its prepn.
CN1541066A (en) * 2001-06-28 2004-10-27 Compsn. for coating fruis, vegetables and fowl eggs, esp. useful for organic produce
CN1398541A (en) * 2001-07-25 2003-02-26 赵旭洪 Natural food preservative
CN1359626A (en) * 2002-01-11 2002-07-24 邹宇超 Process for preparing antistaling agent of fruit and vegetable
CN1488261A (en) * 2002-10-11 2004-04-14 黄海雄 Litchi chinensis and longar antistaling agent and use method
CN101366524A (en) * 2008-09-28 2009-02-18 高思 Fresh fruit processed health preserving pot food
CN101427705A (en) * 2008-12-02 2009-05-13 南京师范大学 Chinese medicinal herb antistaling agent for stem vegetables
CN101810218A (en) * 2010-04-23 2010-08-25 青田稼泷食品有限公司 Red bayberry preservative based on Chinese herbal medicines and preparation method thereof
CN101836673A (en) * 2010-05-20 2010-09-22 中山市先禾生物科技有限公司 Chinese medicinal refreshing fruit wax
CN102907226A (en) * 2012-10-13 2013-02-06 合肥市艳九天农业科技有限公司 Fresh-preservation and nuisance-free cultivation method for greenhouse strawberries

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
陈三斌: "《180种实用化工产品配方与制造》", 30 December 2002, 金盾出版社 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103907677A (en) * 2014-03-24 2014-07-09 王金玉 Method for keeping carambola fresh
CN103907677B (en) * 2014-03-24 2016-03-23 王金玉 Method for keeping carambola fresh
CN104489065A (en) * 2014-12-30 2015-04-08 北海万物盛生物技术开发有限公司 Method for preparing litchi preservative by utilizing natural plants
CN104957243A (en) * 2015-06-11 2015-10-07 邹健 Litchi storage and preservation method
CN108651611A (en) * 2017-03-28 2018-10-16 许昌学院 A kind of special crude antistaling agent of lichee and preparation method thereof

Similar Documents

Publication Publication Date Title
CN101810218B (en) Red bayberry preservative based on Chinese herbal medicines and preparation method thereof
CN101427705B (en) Chinese medicinal herb antistaling agent for stem vegetables
CN103622111B (en) The preparation method of gold shaddock Oryza glutinosa vinegar drink and the golden shaddock Oryza glutinosa vinegar drink obtained by the method
CN102028002B (en) Preservative composition containing Chinese medicinal herbs and application thereof
Runjala et al. Cashew apple (Anacardium occidentale L.) therap eutic benefits, processing and product development: An over view
CN102960792A (en) Jujube-ginger compound beverage and preparation method thereof
CN103636771B (en) Preparation method and application of dried fruit and preserved fruit fresh-keeping film coating agent
CN103005110B (en) Combined lemon and flower dry tea
CN103238666B (en) Preparation method of washing-free red dates with enhanced flavor and nutrition
KR20200004942A (en) Composition for Liver Protection Containing Hub Extract and Beverage Thereof
CN105166899A (en) Fragrance flavored fruit and vegetable enzyme powder preparation method
CN103141567A (en) Litchi chinensis preservative based on Chinese medicinal herbs and preparation method thereof
Abdelrahman et al. Tamarindus indica: phytochemical constituents, bioactive compounds and traditional and medicinal uses
CN105331484A (en) Rice wine distiller's yeast and preparation method thereof
KR20130032625A (en) Complex composition comprising fermented tea
CN107823026A (en) A kind of fermentation and its is preparing the application of skin whitening, moisturizing skin care item at compound
CN101972025A (en) Bamboo vinegar health care beverage and preparation method thereof
KR101993441B1 (en) manufacturing method of fermentation rice containing flavonoid
CN106281842A (en) The preparation method of Isatis indigotica Fort (Indigofera tinctoria L, Baphicanthus cusia (nees) Brem. Polygonum tinctorium Ait) fruit wine
CN108402205A (en) A kind of Green tea processing technology reducing Determination of Theophylline Concentration
KR102487459B1 (en) Manufacturing method of health food having antioxidant activity containing fermented polygonum multiflorum complex extracts and the health food having antioxidant activity thereby
CN107927151A (en) A kind of natural long-acting fruit and vegetable fresh-keeping agent and preparation method thereof
KR20090024033A (en) Health assistant food and thereof manufacturing method
CN102907490A (en) All natural green strawberry preservative and preparation method thereof
CN111317043A (en) Kiwi flower tea and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20130612