CN103103789A - Preparation method for blood-resistant clothing finishing agent - Google Patents
Preparation method for blood-resistant clothing finishing agent Download PDFInfo
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- CN103103789A CN103103789A CN2012105414485A CN201210541448A CN103103789A CN 103103789 A CN103103789 A CN 103103789A CN 2012105414485 A CN2012105414485 A CN 2012105414485A CN 201210541448 A CN201210541448 A CN 201210541448A CN 103103789 A CN103103789 A CN 103103789A
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Abstract
The invention discloses a preparation method for blood-resistant clothing finishing agent. The preparation method comprises the following process steps: (1) getting and mixing 9 weight parts of ammonium polyphosphate, 78 weight parts of fluorocarbon resin, 7 weight parts of zirconium carbide and 6 weight parts of titanium dioxide; adding 100 weight parts of deionized water to the mixed materials to an emulsifying tank for emulsifying; (2)dropping the mixed materials to the reaction kettle after the emulsifying is completed, simultaneously adding 2 weight parts of cycloaliphatic polyisocyanate, 6 weight parts of dodecafluoroheptyl methacrylate and 0.3 weight part of dibutyltin dilaurate, wherein the dropping time is 2.5 hours and the temperature is controlled at 72 DEG C to 75 DEG C in the dropping process; (3) keeping the temperature of 72 DEG C to 75 DEG C for one hour after the dropping is completed, and cooling the mixed materials to 35 DEG C; and (4) filtering the mixed materials by a filter to obtain the nanometer-level finishing agent product. According to the preparation method disclosed by the invention, the finished textile fabric has blood-resistant effect on the basis of keeping the original performances of the textile fabric; moreover, the original air permeability of the textile is not affected.
Description
Technical field
The present invention relates to spin thing finishing agent field, be specifically related to a kind of preparation method of anti-blood stains clothing finishing agent.
Background technology
At medical field, in order to rescue in time, the doctor can change the clothes of oneself and puts on emergency clothing and take the emergency tender noneffectives is carried out simple first aid process before receiving 120 urgent ambulance calls, emergency clothing is that the doctor is when implementing first aid, be through outermost clothes, wrap up patient's wound in first aid process, lift the simple action such as patient.Traditional emergency clothing adopts the materials such as nonwoven fabric, cotton to make more, when first aid, if there are the spots such as blood stains to be infected with on emergency clothing, just is difficult to wipe, and also is not easy to wash.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of anti-blood stains clothing finishing agent, on the basis that has really kept the original performance of fabric panel, make the fabric panel after arrangement have the effect of anti-blood stains, and do not affect the original gas permeability of fabric.
For achieving the above object, the invention provides a kind of preparation method of anti-blood stains clothing finishing agent, comprise following processing step:
1) get APP 9 weight portions, fluorocarbon resin 78 weight portions, zirconium carbide 7 weight portions, titanium dioxide 6 weight portions, mix, then add deionized water 100 weight portions, pour into and carry out emulsification in emulsion tank;
2) emulsification splashes in reactor after complete, drip simultaneously cycloaliphatic polyisocyanate 2 weight portions, dodecafluoroheptyl methacrylate 6 weight portions and dibutyl tin laurate 0.3 weight portion, time for adding is 2.5 hours, and in the dropping process, temperature is controlled at 72 75 ℃;
3) be added dropwise to complete after, 72 75 ℃ the insulation 1 hour, then be cooled to 35 ℃;
4) carry out the nanofiltration device and filter, obtain nano level finishing agent product.
Advantage of the present invention and beneficial effect are: the preparation method that a kind of anti-blood stains clothing finishing agent is provided, on the basis that has really kept the original performance of fabric panel, make the fabric panel after arrangement have the effect of anti-blood stains, and do not affect the original gas permeability of fabric.
The specific embodiment
Below in conjunction with specific embodiment, the invention will be further described.Following examples only are used for technical scheme of the present invention more clearly is described, and can not limit protection scope of the present invention with this.
Embodiment 1
A kind of preparation method of anti-blood stains clothing finishing agent comprises following processing step:
1) get APP 9 weight portions, fluorocarbon resin 78 weight portions, zirconium carbide 7 weight portions, titanium dioxide 6 weight portions, mix, then add deionized water 100 weight portions, pour into and carry out emulsification in emulsion tank;
2) emulsification splashes in reactor after complete, drips simultaneously cycloaliphatic polyisocyanate 2 weight portions, dodecafluoroheptyl methacrylate 6 weight portions and dibutyl tin laurate 0.3 weight portion, and time for adding is 2.5 hours, and in the dropping process, temperature is controlled at 74 ℃;
3) be added dropwise to complete after, 74 ℃ the insulation 1 hour, then be cooled to 35 ℃;
4) carry out the nanofiltration device and filter, obtain nano level finishing agent product.
Embodiment 2
A kind of preparation method of anti-blood stains clothing finishing agent comprises following processing step:
1) get APP 9 weight portions, fluorocarbon resin 78 weight portions, zirconium carbide 7 weight portions, titanium dioxide 6 weight portions, mix, then add deionized water 100 weight portions, pour into and carry out emulsification in emulsion tank;
2) emulsification splashes in reactor after complete, drips simultaneously cycloaliphatic polyisocyanate 2 weight portions, dodecafluoroheptyl methacrylate 6 weight portions and dibutyl tin laurate 0.3 weight portion, and time for adding is 2.5 hours, and in the dropping process, temperature is controlled at 72 ℃;
3) be added dropwise to complete after, 72 ℃ the insulation 1 hour, then be cooled to 35 ℃;
4) carry out the nanofiltration device and filter, obtain nano level finishing agent product.
Embodiment 3
A kind of preparation method of anti-blood stains clothing finishing agent comprises following processing step:
1) get APP 9 weight portions, fluorocarbon resin 78 weight portions, zirconium carbide 7 weight portions, titanium dioxide 6 weight portions, mix, then add deionized water 100 weight portions, pour into and carry out emulsification in emulsion tank;
2) emulsification splashes in reactor after complete, drips simultaneously cycloaliphatic polyisocyanate 2 weight portions, dodecafluoroheptyl methacrylate 6 weight portions and dibutyl tin laurate 0.3 weight portion, and time for adding is 2.5 hours, and in the dropping process, temperature is controlled at 75 ℃;
3) be added dropwise to complete after, 75 ℃ the insulation 1 hour, then be cooled to 35 ℃;
4) carry out the nanofiltration device and filter, obtain nano level finishing agent product.
The above is only the preferred embodiment of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (1)
1. the preparation method of an anti-blood stains clothing finishing agent, is characterized in that, comprises following processing step:
1) get APP 9 weight portions, fluorocarbon resin 78 weight portions, zirconium carbide 7 weight portions, titanium dioxide 6 weight portions, mix, then add deionized water 100 weight portions, pour into and carry out emulsification in emulsion tank;
2) emulsification splashes in reactor after complete, drip simultaneously cycloaliphatic polyisocyanate 2 weight portions, dodecafluoroheptyl methacrylate 6 weight portions and dibutyl tin laurate 0.3 weight portion, time for adding is 2.5 hours, and in the dropping process, temperature is controlled at 72 75 ℃;
3) be added dropwise to complete after, 72 75 ℃ the insulation 1 hour, then be cooled to 35 ℃;
4) carry out the nanofiltration device and filter, obtain nano level finishing agent product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105414485A CN103103789A (en) | 2012-12-14 | 2012-12-14 | Preparation method for blood-resistant clothing finishing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105414485A CN103103789A (en) | 2012-12-14 | 2012-12-14 | Preparation method for blood-resistant clothing finishing agent |
Publications (1)
| Publication Number | Publication Date |
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| CN103103789A true CN103103789A (en) | 2013-05-15 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012105414485A Pending CN103103789A (en) | 2012-12-14 | 2012-12-14 | Preparation method for blood-resistant clothing finishing agent |
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| CN (1) | CN103103789A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102493189A (en) * | 2011-11-15 | 2012-06-13 | 王国栋 | Anti-bloodiness clothing finishing agent and emergency clothes |
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2012
- 2012-12-14 CN CN2012105414485A patent/CN103103789A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102493189A (en) * | 2011-11-15 | 2012-06-13 | 王国栋 | Anti-bloodiness clothing finishing agent and emergency clothes |
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Application publication date: 20130515 |