CN103726317B - A kind of preparation method of raw silk - Google Patents
A kind of preparation method of raw silk Download PDFInfo
- Publication number
- CN103726317B CN103726317B CN201310746119.9A CN201310746119A CN103726317B CN 103726317 B CN103726317 B CN 103726317B CN 201310746119 A CN201310746119 A CN 201310746119A CN 103726317 B CN103726317 B CN 103726317B
- Authority
- CN
- China
- Prior art keywords
- raw silk
- solution
- parts
- rereeling
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Peptides Or Proteins (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of preparation method of health care raw silk, it adopts following steps: A) get wild marjoram, sweetgum, cloves, eucalyptus robusta and water by mass fraction, heat-insulation soaking under the condition of 90 ~ 100 DEG C, filter and obtain filtrate; B) get shitosan by mass fraction, alanine, mass percentage concentration be the disecoctylmaleate sodium sulfonate of 10%, add steps A successively) in the solution of gained, stir while adding evenly for subsequent use; C) according to 1 part, raw silk, the ratio that solution is 10 parts, puts into step B by raw silk) solution that obtains takes out after soaking; D) according to 1 part, raw silk, the ratio that solution is 10 parts, above-mentioned raw silk being put into mass percentage concentration is take out after the ethylene glycol diglycidyl base diethyl ether solution immersion of 0.01 ~ 2%, after sending into the rereeling of rereeling workshop, obtains health care raw silk.The beneficial effect of the invention is: 1) preparation method is simple; 2) Raw Silk Surface has the diaphragm of cross-linked structure; 3) fiber has certain health-care effect.
Description
Technical field
The present invention relates to a kind of preparation method of raw silk material, particularly a kind of preparation method of health care raw silk, belongs to raw silk material field.
Background technology
Functional fibre and function textile represent material, chemical industry, and the fibrous material of weaving and association area Sci-Tech Level and textile product are one of scientific worker's focus in the fields such as fiber, weaving, dyeing and finishing, clothes, fine chemistry industry.Raw silk is prepared from by natural silk, is subject to the popular welcome of consumer.Development functionality textiles, integrates comfortable, lies fallow, keeps healthy, and this has become the trend of world today's textiles development.Human body can be made to be in a kind of comfortable state all the time, and this has positive meaning to the exploitation of function clothes and fabric.
Summary of the invention
The object of this invention is to provide a kind of preparation method of health care raw silk; the sweetgum of dispelling rheumatism, antibacterial wild marjoram, eucalyptus robusta, shitosan; prepare health care fiber; and form the diaphragm with cross-linked structure by the Raw Silk Surface that acts on of ethylene glycol diglycidyl base ether and shitosan, alanine, obtain health care raw silk.
In order to achieve the above object, the technical solution used in the present invention is: a kind of preparation method of health care raw silk, it is characterized in that adopting following steps:
A) get wild marjoram 10 ~ 20 parts by mass fraction, sweetgum 2 ~ 5 parts, cloves 1 ~ 3 part, eucalyptus robusta 1 ~ 3 part and 300 parts, water, under the condition of 90 ~ 100 DEG C, heat-insulation soaking is after 30 ~ 50 minutes, filters and obtains filtrate;
B) shitosan 0.3 ~ 6 part is got by mass fraction, alanine 0.1 ~ 1 part, mass percentage concentration is the disecoctylmaleate sodium sulfonate solution 0.01 ~ 0.5 part of 10%, joins steps A successively) filtrate in, stir while adding evenly for subsequent use;
C) according to 1 part, raw silk, the ratio that solution is 10 ~ 20 parts, puts into step B by raw silk) solution that obtains soaks after 10 ~ 60 minutes and takes out;
D) according to 1 part, raw silk, the ratio that solution is 10 ~ 20 parts, above-mentioned raw silk is put into ethylene glycol diglycidyl base diethyl ether solution immersion taking-up after 10 ~ 20 minutes that mass percentage concentration is 0.01 ~ 2%, send into rereeling workshop and after rereeling, obtain health care raw silk under 45 ~ 50 DEG C of conditions.
The present invention compared with the conventional method, has following outstanding advantage: 1) preparation method is simple; 2) Raw Silk Surface generates the diaphragm having cross-linked structure; 3) fiber has certain health-care effect.
Detailed description of the invention
Be described further the present invention below in conjunction with specific embodiment: the preparation method of health care raw silk of the present invention, it adopts following steps:
A) get wild marjoram 10 ~ 20 parts by mass fraction, sweetgum 2 ~ 5 parts, cloves 1 ~ 3 part, eucalyptus robusta 1 ~ 3 part and 300 parts, water, under the condition of 90 ~ 100 DEG C, heat-insulation soaking is after 30 ~ 50 minutes, filters and obtains filtrate;
B) shitosan 0.3 ~ 6 part is got by mass fraction, alanine 0.1 ~ 1 part, mass percentage concentration is the disecoctylmaleate sodium sulfonate solution (penetrant t) 0.01 ~ 0.5 part of 10%, joins steps A successively) filtrate in, stir while adding evenly for subsequent use;
C) according to 1 part, raw silk, the ratio that solution is 10 ~ 20 parts, puts into step B by raw silk) solution that obtains soaks after 10 ~ 60 minutes and takes out;
D) according to 1 part, raw silk, the ratio that solution is 10 ~ 20 parts, above-mentioned raw silk is put into ethylene glycol diglycidyl base diethyl ether solution immersion taking-up after 10 ~ 20 minutes that mass percentage concentration is 0.01 ~ 2%, send into rereeling workshop and after rereeling, obtain health care raw silk under 45 ~ 50 DEG C of conditions.
Embodiment of the present invention can on the basis of technique scheme; replaced by the difference of concrete numerical value; numerous embodiment can be obtained; therefore; three embodiments of the following stated; be only the example in numerous embodiment, any technology numerical value done in technique scheme is replaced, and all belongs to protection scope of the present invention.
Embodiment 1: the preparation method of health care raw silk of the present invention, it adopts following steps:
A) get wild marjoram 10 parts by mass fraction, sweetgum 2 parts, cloves 1 part, eucalyptus robusta 1 part, 300 parts, water, under the condition of 90 DEG C after heat-insulation soaking 30min, filter, obtain filtrate;
B) shitosan 0.3 part is got by mass fraction, alanine 0.1 part, mass percentage concentration is the disecoctylmaleate sodium sulfonate solution (penetrant t) 0.01 part of 10%, adds steps A successively) solution in, stir while adding evenly, for subsequent use;
C) according to 1 part, raw silk, the ratio that solution is 100 parts, puts into step B by raw silk) solution that obtains soaks 100 minutes, takes out;
D) according to 1 part, raw silk, the ratio that solution is 10 parts, above-mentioned raw silk is put into mass percentage concentration be 0.01 ethylene glycol diglycidyl base diethyl ether solution soak 10 minutes, take out, send into rereeling workshop and after rereeling, obtain health care raw silk under 45 DEG C of conditions.
Embodiment 2: the preparation method of health care raw silk of the present invention, it adopts following steps:
A) get wild marjoram 15 parts by mass fraction, sweetgum 3 parts, cloves 2 parts, eucalyptus robusta 2 parts, 300 parts, water, under the condition of 90 DEG C after heat-insulation soaking 40min, filter, obtain filtrate;
B) shitosan 3 parts is got by mass fraction, alanine 0.5 part, mass percentage concentration is the disecoctylmaleate sodium sulfonate solution (penetrant t) 0.03 part of 10%, adds steps A successively) solution in, stir while adding evenly, for subsequent use;
C) according to 1 part, raw silk, the ratio that solution is 15 parts, puts into step B by raw silk) solution that obtains soaks 30 minutes, takes out;
D) according to 1 part, raw silk, the ratio that solution is 15 parts, above-mentioned raw silk is put into mass percentage concentration be 0.1% ethylene glycol diglycidyl base diethyl ether solution soak 15 minutes, take out, send into rereeling workshop and after rereeling, obtain health care raw silk under 45 DEG C of conditions.
Embodiment 3: the preparation method of health care raw silk of the present invention, it adopts following steps:
A) get wild marjoram 20 parts by mass fraction, sweetgum 5 parts, cloves 3 parts, eucalyptus robusta 3 parts, 300 parts, water, under the condition of 100 DEG C after heat-insulation soaking 50min, filter, obtain filtrate;
B) shitosan 6 parts is got by mass fraction, alanine 1 part, mass percentage concentration is the disecoctylmaleate sodium sulfonate solution (penetrant t) 0.5 part of 10%, adds steps A successively) solution in, stir while adding evenly, for subsequent use;
C) according to 1 part, raw silk, the ratio that solution is 20 parts, puts into step B by raw silk) solution that obtains soaks 60 minutes, takes out;
D) according to 1 part, raw silk, the ratio that solution is 20 parts, above-mentioned raw silk is put into mass percentage concentration be 2% ethylene glycol diglycidyl base diethyl ether solution soak 20 minutes, take out, send into rereeling workshop under 50 DEG C of conditions, after rereeling, obtain health care raw silk.
Claims (1)
1. a preparation method for raw silk, is characterized in that adopting following steps:
A) get wild marjoram 10 ~ 20 parts by mass fraction, sweetgum 2 ~ 5 parts, cloves 1 ~ 3 part, eucalyptus robusta 1 ~ 3 part and 300 parts, water, under the condition of 90 ~ 100 DEG C, heat-insulation soaking is after 30 ~ 50 minutes, filters and obtains filtrate;
B) shitosan 0.3 ~ 6 part is got by mass fraction, alanine 0.1 ~ 1 part, mass percentage concentration is the disecoctylmaleate sodium sulfonate solution 0.01 ~ 0.5 part of 10%, joins steps A successively) filtrate in, stir while adding evenly for subsequent use;
C) according to 1 part, raw silk, the ratio that solution is 10 ~ 20 parts, puts into step B by raw silk) solution that obtains soaks after 10 ~ 60 minutes and takes out;
D) according to step C) 1 part, raw silk obtaining, the ratio that solution is 10 ~ 20 parts, above-mentioned raw silk is put into ethylene glycol diglycidyl base diethyl ether solution immersion taking-up after 10 ~ 20 minutes that mass percentage concentration is 0.01 ~ 2%, send into rereeling workshop and after rereeling, obtain raw silk under 45 ~ 50 DEG C of conditions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310746119.9A CN103726317B (en) | 2013-12-28 | 2013-12-28 | A kind of preparation method of raw silk |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310746119.9A CN103726317B (en) | 2013-12-28 | 2013-12-28 | A kind of preparation method of raw silk |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103726317A CN103726317A (en) | 2014-04-16 |
| CN103726317B true CN103726317B (en) | 2015-08-19 |
Family
ID=50450590
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310746119.9A Active CN103726317B (en) | 2013-12-28 | 2013-12-28 | A kind of preparation method of raw silk |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103726317B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108729213A (en) * | 2017-10-27 | 2018-11-02 | 湖州卓宇丝织有限公司 | The functional treatment method of silk goods |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102978911A (en) * | 2012-11-21 | 2013-03-20 | 吴江红蔷薇纺织有限公司 | Mercerizing assistant for fabric and preparation method thereof |
| CN103160944B (en) * | 2013-03-26 | 2015-11-18 | 成进学 | Rich selenium germanium chitosan natural fabric summer grade vest |
-
2013
- 2013-12-28 CN CN201310746119.9A patent/CN103726317B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN103726317A (en) | 2014-04-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103361872B (en) | Production technology of medical stone fiber seamless knitted underwear with health-care function | |
| CN103710965B (en) | A kind of preparation method of natural silk functional textile | |
| CN103898658B (en) | A kind of preparation method of health care fabric | |
| CN104975374A (en) | Preparation process of blended yarn weaved fabric containing tea fiber | |
| CN104153096A (en) | Ultraviolet-proof blended fabric and method for manufacturing same | |
| CN103061161A (en) | Preparation method of nano anion kapok fiber fabric and applications of nano anion kapok fiber fabric in home textile product | |
| CN103726317B (en) | A kind of preparation method of raw silk | |
| CN103526557A (en) | Preparation technology of health care fabric | |
| CN104499064B (en) | Anti-pilling shell fabric spinning method | |
| CN104005227B (en) | The preparation method of milk protein composite fibre, milk protein composite fibre and application | |
| CN103541215A (en) | Production process for antibacterial shell fabric | |
| CN104294473A (en) | Production process of health care type wool elastic knitted fabric | |
| CN107696629A (en) | A kind of ultraviolet-resistant fabric | |
| CN103680656A (en) | Process for manufacturing radiation protection fiber cloth | |
| CN104126883B (en) | A kind of production technology of mulberry silk health care female bra fabric | |
| CN103726306B (en) | A kind of function silk fiber preparation method utilizing husks | |
| CN106498553A (en) | A kind of highly-breathable antiultraviolet modified fibre fabric | |
| CN106592229A (en) | Cashmere fabric anti-pilling finishing liquor containing modified sericin and preparation method of finishing liquor | |
| CN103911854B (en) | A kind of preparation method of health care silk clothes | |
| CN105780529A (en) | Cardamine hirsute cloth dyeing technology | |
| CN105063849A (en) | Extremely-soft baby garment fabric | |
| CN104611865B (en) | A kind of dyeing silk pre-treating technology | |
| CN104532540A (en) | A producing method of a milk fiber fabric | |
| CN110344236A (en) | A kind of tea grounds modified function quilted stockings of antibacterial and deodouring and preparation method thereof | |
| CN110158199B (en) | Preparation method of biomass fiber capable of shielding ultraviolet rays |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent for invention or patent application | ||
| CB02 | Change of applicant information |
Address after: 310021, Zhejiang, Jianggan District province Hangzhou Ding Qiao Metro Plaza business suite 1307 Applicant after: Hangzhou Fanlin Technology Co., Ltd. Address before: Hangzhou City, Zhejiang Province, 310016 Qingchun Road No. 78 Building No. 1809 Amethyst Hotel Applicant before: Hangzhou Fanlin Technology Co., Ltd. |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 310016 HANGZHOU, ZHEJIANG PROVINCE TO: 310021 HANGZHOU, ZHEJIANG PROVINCE |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171115 Address after: 226000 Changjiang West Road, Haian Town, Haian County, Nantong City, Jiangsu Province, No. 288 Patentee after: Jiangsu Huaxin hi tech Innovation Co., Ltd. Address before: 310021, Zhejiang, Jianggan District province Hangzhou Ding Qiao Metro Plaza business suite 1307 Patentee before: Hangzhou Fanlin Technology Co., Ltd. |