CN103070788B - Sustained-release sweet osmanthus perfume - Google Patents
Sustained-release sweet osmanthus perfume Download PDFInfo
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- CN103070788B CN103070788B CN201210552081.7A CN201210552081A CN103070788B CN 103070788 B CN103070788 B CN 103070788B CN 201210552081 A CN201210552081 A CN 201210552081A CN 103070788 B CN103070788 B CN 103070788B
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Abstract
The invention discloses a sustained-release sweet osmanthus perfume. The sustained-release sweet osmanthus perfume comprises: by volume, 0.25 to 12.5% of sweet osmanthus essential oil, 0.05 to 10% of one or more fixatives, 73.625 to 94.715% of anhydrous ethanol and the balance deionized water. Preferably, the one or more fixatives are selected from vanillin, Peru balsam and orris oil. The sustained-release sweet osmanthus perfume has greatly prolonged fragrance retention time, an obvious sweet osmanthus fragrance and no toxic and side effect and greatly reduces a use amount of natural sweet osmanthus essential oil. The sustained-release sweet osmanthus perfume solves the sweet osmanthus perfume development problem that the existing sweet osmanthus perfume has short fragrance retention time and consumes a large amount of natural sweet osmanthus essential oil, can be popularized and used, and has obvious economic and social benefits.
Description
Technical field
The present invention relates to a kind of sweet osmanthus perfume, especially a kind of spacetabs type sweet osmanthus perfume.
Background technology
Flos Osmanthi Fragrantis (Osmanthus Fragrans Lour.) is the distinctive fragrant flower of China, is one of China's tradition ten large famous flowers, has very high viewing and admiring and edibility.But the domestic application to osmanthus spice material is confined to Flos Osmanthi Fragrantis dry flower and osmanthus concrete at present, and most products directly adds Flos Osmanthi Fragrantis dry flower, some enterprise is directly exported by osmanthus concrete, reduces the value of the domestic utilization of Flos Osmanthi Fragrantis; Perfume in the market, mostly containing various chemosynthesis composition, can cause perfume user generation discomfort in various degree.Sweet osmanthus perfume of the present invention, adopt pure natural to extract osmanthus essential oil, fragrant odour is pleasant, soft, the sweet and joyful sense of the natural Flos Osmanthi Fragrantis of tool, can reach to purify air, people is in a cheerful frame of mind, regulates the effects such as emotion, can eliminate the feeling of fatigue of people.
Main aroma-producing substance due to osmanthus essential oil is alpha, beta-lonone, dihydro-β-ionone and linalool oxide etc., it is impermanent that such material generally has fragrance remaining time, easily adapted to by human body nose olfactory receptor cell, thus cause reducing its fragrance sensitivity, thus determine osmanthus flower fragrant perfume lasting lasting not.
Have a lot for the method delaying the volatilizing perfume time at present, be mostly multiple quintessence oil to share, after the fragrant spice fragrance of head is evaporated completely, adopt other spice fragrance as middle perfume (or spice) and bottom note, be CN102406575A as hair waits all one's life at publication number, the perfume volume constituents adopted during name is called " a kind of sweet osmanthus perfume " is: basic quintessence oil, osmanthus essential oil, Flos Osmanthi Fragrantis hydrosol, quintessence oil emulsifying agent, 95% ethanol.The deficiency of this invention is: add other derived essential oils in perfume, and Flos Osmanthi Fragrantis fragrance is not given prominence to, and does not add slow releasing agent, and Flos Osmanthi Fragrantis fragrance fragrance remaining time is shorter; Patent documentation CN1757311A discloses one " a kind of method of special flavour improvement enzyme comprehensive utilization Flos Osmanthi Fragrantis ", and the method adopts special flavour improvement enzyme to increase Flos Osmanthi Fragrantis fragrance, and this invention substantially increases the production cost of sweet osmanthus perfume, is unfavorable for that commercial production is applied; Current essence release method adopts beta-schardinger dextrin-, porous-starch etc. to be wall material in addition, carries out micro encapsulation, wrapped up by quintessence oil essence, reaches effect of slow release.The large quantity research in early stage of the present inventor finds, essence microcapsule adds the complexity that perfume is produced, and essential oil waste is serious, increases commercial production difficulty simultaneously, is difficult to realize commercial production application; Osmanthus essential oil is carried out nano-capsulation, to increase stability, extend and protect the fragrant phase, but this technology is still immature, the great many of experiments in early stage of the present inventor finds, osmanthus essential oil nano-capsulation is comparatively difficult, and production difficulty is comparatively large, not easily Industry Promotion; Adding fixastive composition in perfume is another important channel extending the volatilizing perfume time, and fixastive mostly is high boiling substance, can reduce essence evaporation rate in quintessence oil, extends perfume fragrance remaining time.But the selection of fixastive is comparatively complicated, must reaches simultaneously make fixastive neither affect original perfume fragrance, effect of flavor component can be stablized again.
Extend the method for protecting the fragrant phase above through comprehensive analysis, and the constituent of osmanthus essential oil is analysed in depth, determine that adding of fixastive is the method the most feasible of sweet osmanthus perfume fixation, and wherein the selection of fixastive is of crucial importance.At present, the fixastive of report is mainly natural animal fixastive, natural plant essential oils and extractum and synthetic fixastive.Natural animal fixastive, due to fancy price, increases perfume cost of manufacture; In vegetalitas quintessence oil fixastive, vetiver oil, patchouli oil and Oleum Santali albi all belong to Radix Aucklandiae class quintessence oil, and the present inventor, through verification experimental verification, adding of these fixastive, cancels each other with osmanthus essential oil fragrance fragrance, can not be used for the fixation of osmanthus essential oil; And the breath of orris oil tool sweet taste, the equal tool cream of Benzoinum balsam, Olibanum balsam, peru balm and Styrax cream is fragrant, sweet osmanthus perfume fragrance can be increased, the present inventor finds through lot of experiments checking, in natural plants fixastive, orris oil and peru balm are to the fixation effect optimum of sweet osmanthus perfume, Styrax cream also has certain fixation effect, but effect is excellent not as above two kinds of fixastive.Vanillin is also a kind of fragrance material be widely used extracted from plant, in a large number for needing to increase in the foods and cosmetics of milk fragrance, the present invention's research also finds, this material also can be used for the perfuming of perfume, and to sweet osmanthus perfume fixation Be very effective.
Summary of the invention
The object of the present invention is to provide a kind of sweet osmanthus perfume of spacetabs type, this perfume fragrance remaining time is long, and simultaneously fragrance is pure, the natural Flos Osmanthi Fragrantis fragrance of tool, and fragrance is sent out thoroughly, quiet and tastefully laid out strong and stay length, and formula is simplified, easy and simple to handle.
The sweet osmanthus perfume of a kind of spacetabs type provided by the present invention, be made up of osmanthus essential oil, fixastive, dehydrated alcohol and deionized water, wherein, the volume fraction of each component is: osmanthus essential oil: 0.25-12.5%, fixastive: 0.05-10%, dehydrated alcohol: 73.625-94.715%, deionized water: surplus.
As the improvement of technique scheme, described fixastive is any one of vanillin, peru balm and orris oil or appoints several mixture.
Sweet osmanthus perfume provided by the invention, with natural aromatic plant quintessence oil for raw material, one or more the natural fixastive screening acquisition are in a large number joined sweet osmanthus perfume, obtain a kind of spacetabs type sweet osmanthus perfume, the present invention substantially prolongs sweet osmanthus perfume fragrance remaining time, and fragrance remaining time can reach 24-60 hour, the sweet osmanthus perfume fragrance remaining time of producing on the market comparatively at present extends 5-12 doubly, and Flos Osmanthi Fragrantis fragrance is given prominence to, without any side effects, natural osmanthus essential oil consumption greatly reduces simultaneously.And raw material sources are wide, formula is simplified, and production technology is simple, and product delicate fragrance is simple and elegant.Solve an application difficult problem for the sweet osmanthus perfumes such as short, the natural osmanthus essential oil consumption of sweet osmanthus perfume fragrance remaining time is large exploitation, applying of this invention, economic benefit and social benefit remarkable.
Detailed description of the invention
Below the specific embodiment of the present invention is described further.It should be noted that at this, the explanation for these embodiments understands the present invention for helping, but does not form limitation of the invention.In addition, if below in described each embodiment of the present invention involved technical characteristic do not form conflict each other and just can mutually combine.
The quality requirements of the osmanthus essential oil used in following example is: the brown color working fluid of clarification, has the fragrance of natural Flos Osmanthi Fragrantis; Relative density (25/25 DEG C) 0.900-0.986, refraction index (20 DEG C) 1.440-1.496, ester value >=25, heavy metal (in Pb)≤40mg/kg, arsenic content (As)≤3mg/kg.
In the peru balm of fixastive used in the present invention preferred natural plants extractum quintessence oil apoplexy due to endogenous wind and orris oil and natural plants monomer extract vanillin any one or appoint several mixture, but also can be natural plants extractum quintessence oil and the monomer extract of other kinds, as coumarin.
A sweet osmanthus perfume for spacetabs type, modulation 1000ml sweet osmanthus perfume, the volume component of this perfume is:
Embodiment 1:
Osmanthus essential oil 65ml, orris oil 0.5ml, cosmetics-stage dehydrated alcohol 887.78ml, deionized water 46.72ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, orris oil in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 49 hours.
Embodiment 2:
Osmanthus essential oil 125ml, peru balm 1g, cosmetics-stage dehydrated alcohol 830.3ml, deionized water 43.7ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, peru balm in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 55 hours.
Embodiment 3:
Osmanthus essential oil 2.5ml, vanillin 0.5g, cosmetics-stage dehydrated alcohol 947.15ml, deionized water 49.85ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, vanillin in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 24 hours.
Embodiment 4:
Osmanthus essential oil 125ml, vanillin 10g, orris oil 90ml, cosmetics-stage dehydrated alcohol 736.25ml, deionized water 38.75ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, orris oil, vanillin in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 60 hours.
Embodiment 5:
Osmanthus essential oil 25ml, vanillin 5g, peru balm 5g, cosmetics-stage dehydrated alcohol 916.75ml, deionized water 48.25ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, vanillin and peru balm in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 35 hours.
Embodiment 6:
Osmanthus essential oil 34ml, peru balm 5g, orris oil 15ml, cosmetics-stage dehydrated alcohol 898.7ml, deionized water 47.3ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, peru balm and orris oil in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 45 hours.
Embodiment 7:
Osmanthus essential oil 10ml, peru balm 2g, vanillin 15g, orris oil 8ml, cosmetics-stage dehydrated alcohol 916.75ml, deionized water 48.25ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, peru balm in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 35 hours.
Embodiment 8:
Osmanthus essential oil 10ml, coumarin 5g, cosmetics-stage dehydrated alcohol 935.75ml, deionized water 49.25ml
Be dissolved in dehydrated alcohol by osmanthus essential oil, peru balm in above formula, mix homogeneously, then add wherein by deionized water, mixing, load in vial and seal, display 30 days, rear glass scent flask is canned is finished product.Perfume substantiation can reach 20 hours.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the content disclosed in this embodiment.The equivalence completed under not departing from spirit disclosed in this invention so every or amendment, all fall into the scope of protection of the invention.
Claims (1)
1. a sweet osmanthus perfume for spacetabs type, is made up of osmanthus essential oil, fixastive, dehydrated alcohol and deionized water, it is characterized in that:
The composition of described fixastive is selected from following arbitrary situation: vanillin, the mixture of vanillin and peru balm, the mixture of vanillin and orris oil, or the mixture of vanillin and peru balm and orris oil;
Wherein
The volume fraction of osmanthus essential oil is set to 0.25% ~ 12.5%, its quality is set to: the brown color working fluid of clarification, there is the fragrance of natural Flos Osmanthi Fragrantis, relative density under 25 DEG C/25 DEG C measuring conditions is 0.900-0.986, refraction index at 20 DEG C is 1.440-1.496, ester value >=25, are controlled as≤40mg/kg in the content of beary metal of Pb, and arsenic content is controlled as≤3mg/kg;
The volume fraction of dehydrated alcohol is set to 73.625% ~ 94.715%; The volume fraction of fixastive is 0.05-10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210552081.7A CN103070788B (en) | 2012-12-18 | 2012-12-18 | Sustained-release sweet osmanthus perfume |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210552081.7A CN103070788B (en) | 2012-12-18 | 2012-12-18 | Sustained-release sweet osmanthus perfume |
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| Publication Number | Publication Date |
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| CN103070788A CN103070788A (en) | 2013-05-01 |
| CN103070788B true CN103070788B (en) | 2015-01-28 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106070929A (en) * | 2016-06-11 | 2016-11-09 | 浙江大学 | The preparation method of slow release Murrayae Folium Et Cacumen Folium Camelliae sinensis quintessence oil |
| CN106176310A (en) * | 2016-07-29 | 2016-12-07 | 金玛瑙香水（明光）有限公司 | One is refreshed oneself sweet osmanthus perfume ingredients |
| CN107693417A (en) * | 2017-10-13 | 2018-02-16 | 李丹丹 | A kind of osmanthus spice composition, its preparation method and the purposes in care product |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1065856C (en) * | 1996-06-12 | 2001-05-16 | 中国科学院大连化学物理研究所 | Synthesis of vanillin by one-step oxidation |
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2012
- 2012-12-18 CN CN201210552081.7A patent/CN103070788B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1065856C (en) * | 1996-06-12 | 2001-05-16 | 中国科学院大连化学物理研究所 | Synthesis of vanillin by one-step oxidation |
Non-Patent Citations (2)
| Title |
|---|
| 天津轻工业学院食品工业教学研究室.(一)香兰素.《食品添加剂》.中国轻工业出版社,1985,184. * |
| 马世昌.桂花香精.《化学物质辞典》.陕西科学技术出版社,1999,569. * |
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