CN103070786B - Softening-free perming agent for hot perming and use method thereof - Google Patents
Softening-free perming agent for hot perming and use method thereof Download PDFInfo
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- CN103070786B CN103070786B CN201310020702.1A CN201310020702A CN103070786B CN 103070786 B CN103070786 B CN 103070786B CN 201310020702 A CN201310020702 A CN 201310020702A CN 103070786 B CN103070786 B CN 103070786B
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Abstract
The invention provides a softening-free perming agent for hot perming and a use method thereof. The perming agent is composed of an agent A and an agent B, wherein the agent A is prepared by the following raw materials in part by weight: 51.9-87.39 parts of water, 1-8 parts of moisturizing agent, 0.5-5 parts of emulsifying agent, 4-10 parts of thickening agent, 1-5 parts of lubricating agent, 2-7 parts of hair conditioner, 3-8 parts of reducing agent, 1-4 parts of PH regulating agent, 0.01-0.1 part of preservative and 0.1-l part of odorant; and the agent B is prepared by the following raw materials in part by weight: 59.99-95.88 parts of water, 4-15 parts of oxidant, 0.1-20 parts of hair conditioner, 0.01-5 parts of essence and 0.01-0.1 part of preservative. The use method comprises the following steps: coating the agent A after hairs are washed, heating, cooling for 4-6 minutes, directly coating the agent B, remaining for 5 minutes and washing to finish perming. The softening-free perming agent for hot perming and the use method thereof have the advantages that the perming time is shortened, and the use method is simple.
Description
Technical field
The invention belongs to boiling hot dyeing technique field, relate in particular to a kind of agent for permanent hair waving and the using method thereof of exempting from softening burn.
Background technology
Agent for permanent hair waving is that the people at various age is for temporarily increasing curling and wave.Known agent for permanent hair waving comprises two steps, namely utilizes cystine (disulphide) key of the effect reproducibility division hair of reducing agent, subsequently with oxidant neutralization or sizing, thus replys cystine (disulphide) key.
The process of general burn is loaded down with trivial details, and the time is long, need through following process: 1, have one's hair wash; 2, softening: this process judges according to different hair quality, is generally 15 minutes, and the hair quality do not scalded completely is 7-8 minute; 3, stop heating, the difference of hair quality, the time of heating and stop is also different.Resistance hair quality is 20-25 minute, and healthy hair quality is 15-20 minute, and general damaged hair is 10-15 minute, and extremely damaged hair is 3-10 minute; 4, test is softening, elongates hair 2-3 doubly, sees resilience ripple; 5, wash by water; 6, upper volume; 7, heat; 8, cooling and shaping, cool 15 minutes, cotton pad of dismantling, upper sizing water, discharges first pass fast, and infiltration, goes up one time again after 5 minutes, discharge in order to avoid waste at twice; 9, thick stick, bath is torn open.Hair-waving flow process of the prior art is loaded down with trivial details, length consuming time.
Summary of the invention
Object of the present invention is intended to the shortcoming overcoming the existence of above-mentioned prior art, provides a kind of agent for permanent hair waving and the using method thereof of exempting from softening burn, and this agent for permanent hair waving makes hair-waving time shorten, using method simple.
In order to realize the object of foregoing invention, the invention provides a kind of agent for permanent hair waving of exempting from softening burn, described agent for permanent hair waving by with the use of agent A mediating recipe B form; Wherein,
Described dose of A is prepared by the step of following order:
1) 51.9 ~ 87.39 weight parts waters, 1 ~ 8 weight portion wetting agent, 0.5 ~ 5 parts by weight Emulsifier are added in aqueous phase dissolved pot, be heated to 80-85 DEG C; 4 ~ 10 parts by weight of thickening agent, 1 ~ 5 weight portion lubricant are added in oil phase dissolving pan and is heated to 80-85 DEG C;
2) inhale material in a small amount of aqueous phase dissolved pot in emulsifying pot, then the material inhaling a small amount of oil phase dissolving pan is to homogenizing 5-10 minute in emulsifying pot, is sucked in emulsifying pot by the clout in aqueous phase dissolved pot simultaneously; Stir 20 minutes under 200-300 rev/min in a vacuum, add 2 ~ 7 weight portion conditioner for hair when being cooled to feed temperature≤40 DEG C in emulsifying pot and fully stir, rotating speed 200 revs/min;
3) in emulsifying pot, add water in advance dissolving 3 ~ 8 weight portion mass concentrations is 30-80% reductant solution, stir 2 minutes under the rotating speed of 200 revs/min, add 1 ~ 4 weight portion pH adjusting agent again, finally add 0.01 ~ 0.1 weight portion antiseptic, 0.1 ~ 1 weight portion essence fully stirs evenly, then room temperature is chilled to, detect the pH=8-8.1 of solution in emulsifying pot, TGA content when being 6.8%-11% and qualified, take the dish out of the pot, obtain of the present invention dose of A;
Described dose of B is prepared by the step of following order:
First, 59.99-95.88 weight parts water, 4-15 weight portion oxidant are added in reaction pot, is stirred to oxidant with 150 revs/min of rotating speeds and fully dissolves;
Secondly, in described reaction pot, the 0.1-20 weight portion nonyl phenol polyethers-15 and 0.01-5 weight portion essence that mix in clean, dry anhydrous container is in advance added, by the mixed liquor mix homogeneously in reaction pot to as clear as crystal;
Finally, add 0.01-0.1 weight portion antiseptic in reaction pot, discharging when being uniformly mixed pH=4.0-7.0, the oxygenate content > 7 of rear detection mixed liquor with 150 revs/min of rotating speeds, obtains of the present invention dose of B.
Further, wetting agent in described dose of A is glycerol, emulsifying agent is octadecyl trimethyl ammonium chloride, thickening agent is octadecanol, and lubricant is isopropyl palmitate, and conditioner for hair is silicone oil, reducing agent is Mercaptamine, PH regulator is monoethanolamine, and antiseptic is Kazon, and essence is odorant; Oxidant in described dose of B is sodium bromate.
Further, described agent for permanent hair waving A and agent for permanent hair waving B be with the use of, using method is as follows: directly above after hair washing roll up varnish A, heating; Then cool 4-6 minute, without the need to bath, be directly coated with agent for permanent hair waving B, stop 5 minutes afterflush and namely complete hair-waving.Heat time heating time after coating agent A is: resisting hair quality heat time heating time is 14 minutes, and healthy hair quality heat time heating time is 11 minutes, and general damaged hair heat time heating time is 8-10 minute, and extremely damaged hair heat time heating time is 4-5 minute.Described agent B smears at twice, each stop 5 minutes.
The present invention compared with prior art, possesses following outstanding substantive distinguishing features and significant progress:
1) the present invention is without the need to softening, bath, and the rear directly upper volume varnish A of hair washing, heating, then cools 4-6 minute, and without the need to washing by water, direct varnish B, stops 5 minutes afterflush and namely complete hair-waving, and hair-waving program is simple, has greatly saved the hair-waving time.
2) agent B of the present invention be oxidant or claim nertralizer, its effect is that cysteine residues is recombined, and new position forms disulfide bond, like this with regard to make curling after hair style be fixed up, this process is called type-approval process.Can smear at twice when varnish B, each stop 5 minutes, to guarantee abundant absorption and the infiltration of agent B.
The present invention can be well understood to further by specific embodiments of the invention given below.But they are not limitation of the invention.
Detailed description of the invention
Embodiment 1
Agent A in a kind of agent for permanent hair waving of exempting from softening burn provided by the invention is prepared by the step of following order:
1) 51.9Kg water, 1Kg glycerol, 0.5Kg octadecyl trimethyl ammonium chloride are added in aqueous phase dissolved pot, be heated to 80-85 DEG C; 4Kg octadecanol, 1Kg isopropyl palmitate are added in oil phase dissolving pan and is heated to 80-85 DEG C;
2) inhale material in a small amount of aqueous phase dissolved pot in emulsifying pot, then the material inhaling a small amount of oil phase dissolving pan is to homogenizing 5-10 minute in emulsifying pot, is sucked in emulsifying pot by the clout in aqueous phase dissolved pot simultaneously; Stir 20 minutes under 200-300 rev/min in a vacuum, add 2Kg silicone oil when being cooled to feed temperature≤40 DEG C in emulsifying pot and fully stir, rotating speed 200 revs/min;
3) in emulsifying pot, adding water in advance, to dissolve the mass concentration that 3Kg Mercaptamine powder is mixed be 30-80% cysteamine hydrochloride solution, stir 2 minutes under the rotating speed of 200 revs/min, add 1Kg monoethanolamine again, finally add 0.01Kg Kazon, 0.1Kg essence fully stirs evenly, then room temperature is chilled to, detect the pH=8-8.1 of solution in emulsifying pot, TGA content when being 6.8%-11% and qualified, take the dish out of the pot, obtain of the present invention dose of A;
Agent B in a kind of agent for permanent hair waving of exempting from softening burn provided by the invention is prepared by the step of following order:
First, 59.99Kg water, 4Kg sodium bromate are added in reaction pot, be stirred to sodium bromate with 150 revs/min of rotating speeds and fully dissolve;
Secondly, in described reaction pot, the 0.1Kg nonyl phenol polyethers-15 and 0.01Kg weight portion essence that mix in clean, dry anhydrous container is in advance added, by the mixed liquor mix homogeneously in reaction pot to as clear as crystal;
Finally, in reaction pot, add 0.01Kg antiseptic, with 150 revs/min of rotating speeds be uniformly mixed the pH=4.0-7.0 of rear detection mixed liquor, sodium bromate content >=7% and mixed liquor Clear & Transparent time be qualified, discharging, obtain of the present invention dose of B.
Embodiment 2
Agent A in a kind of agent for permanent hair waving of exempting from softening burn provided by the invention is prepared by the step of following order:
69.645Kg water, 4.5Kg parts by weight of glycerin, 2.75Kg octadecyl trimethyl ammonium chloride are added in aqueous phase dissolved pot, is heated to 80-85 DEG C; 7Kg octadecanol, 3Kg isopropyl palmitate are added in oil phase dissolving pan and is heated to 80-85 DEG C;
2) inhale material in a small amount of aqueous phase dissolved pot in emulsifying pot, then the material inhaling a small amount of oil phase dissolving pan is to homogenizing 5-10 minute in emulsifying pot, is sucked in emulsifying pot by the clout in aqueous phase dissolved pot simultaneously; Stir 20 minutes under 200-300 rev/min in a vacuum, add 4.5Kg silicone oil when being cooled to feed temperature≤40 DEG C in emulsifying pot and fully stir, rotating speed 200 revs/min;
3) in emulsifying pot, adding water in advance, to dissolve the mass concentration that 5.5Kg Mercaptamine powder is mixed be 30-80% cysteamine hydrochloride solution, stir 2 minutes under the rotating speed of 200 revs/min, add 2.5Kg monoethanolamine again, finally add 0.055Kg Kazon, 0.55Kg essence fully stirs evenly, then room temperature is chilled to, detect the pH=8-8.1 of solution in emulsifying pot, TGA content when being 6.8%-11% and qualified, take the dish out of the pot, obtain of the present invention dose of A;
Agent B in a kind of agent for permanent hair waving of exempting from softening burn provided by the invention is prepared by the step of following order:
First, 77.935Kg water, 9.5Kg sodium bromate are added in reaction pot, be stirred to sodium bromate with 150 revs/min of rotating speeds and fully dissolve;
Secondly, in described reaction pot, the 10.05Kg nonyl phenol polyethers-15 and 2.505Kg essence that mix in clean, dry anhydrous container is in advance added, by the mixed liquor mix homogeneously in reaction pot to as clear as crystal;
Finally, in reaction pot, add 0.055Kg antiseptic, with 150 revs/min of rotating speeds be uniformly mixed the pH=4.0-7.0 of rear detection mixed liquor, sodium bromate content >=7% and mixed liquor Clear & Transparent time be qualified, discharging, obtain of the present invention dose of B.
Embodiment 3
Agent A in a kind of agent for permanent hair waving of exempting from softening burn provided by the invention is prepared by the step of following order:
1) 87.39Kg water, 8Kg glycerol, 5Kg octadecyl trimethyl ammonium chloride are added in aqueous phase dissolved pot, be heated to 80-85 DEG C; 10Kg octadecanol, 5Kg isopropyl palmitate are added in oil phase dissolving pan and is heated to 80-85 DEG C;
2) inhale material in a small amount of aqueous phase dissolved pot in emulsifying pot, then the material inhaling a small amount of oil phase dissolving pan is to homogenizing 5-10 minute in emulsifying pot, is sucked in emulsifying pot by the clout in aqueous phase dissolved pot simultaneously; Stir 20 minutes under 200-300 rev/min in a vacuum, add 7Kg silicone oil when being cooled to feed temperature≤40 DEG C in emulsifying pot and fully stir, rotating speed 200 revs/min;
3) in emulsifying pot, adding water in advance, to dissolve the mass concentration that 8Kg Mercaptamine powder is mixed be 30-80% cysteamine hydrochloride solution, stir 2 minutes under the rotating speed of 200 revs/min, add 4Kg monoethanolamine again, finally add 0.1Kg Kazon, 1Kg essence fully stirs evenly, then room temperature is chilled to, detect the pH=8-8.1 of solution in emulsifying pot, TGA content when being 6.8%-11% and qualified, take the dish out of the pot, obtain of the present invention dose of A;
Agent B in a kind of agent for permanent hair waving of exempting from softening burn provided by the invention is prepared by the step of following order:
First, 95.88Kg water, 15Kg sodium bromate are added in reaction pot, be stirred to sodium bromate with 150 revs/min of rotating speeds and fully dissolve;
Secondly, in described reaction pot, the 20Kg nonyl phenol polyethers-15 and 5Kg essence that mix in clean, dry anhydrous container is in advance added, by the mixed liquor mix homogeneously in reaction pot to as clear as crystal;
Finally, in reaction pot, add 0.1Kg antiseptic, with 150 revs/min of rotating speeds be uniformly mixed the pH=4.0-7.0 of rear detection mixed liquor, sodium bromate content >=7% and mixed liquor Clear & Transparent time be qualified, discharging, obtain of the present invention dose of B.
The present invention's a kind of using method exempting from the agent for permanent hair waving of softening burn provided by the invention is: agent for permanent hair waving A and agent for permanent hair waving B is must be with the use of, and using method is as follows:
Directly upper volume varnish A, heating after hair washing, heat time heating time is: resisting hair quality heat time heating time is 14 minutes, and healthy hair quality heat time heating time is 11 minutes, and general damaged hair heat time heating time is 8-10 minute, and extreme damaged hair heat time heating time is 4-5 minute;
Then, cooling 4-6 minute, without the need to bath, is directly coated with agent for permanent hair waving B, stops 5 minutes afterflush and namely complete hair-waving.Agent B also can smear at twice, and each stop 5 minutes, to guarantee abundant absorption and the infiltration of agent B.
Claims (4)
1. exempt from an agent for permanent hair waving for softening burn, it is characterized in that: described agent for permanent hair waving by with the use of agent A mediating recipe B form; Wherein,
Described dose of A is prepared by the step of following order:
1) 51.9 ~ 87.39 weight parts waters, 1 ~ 8 weight portion wetting agent, 0.5 ~ 5 parts by weight Emulsifier are added in aqueous phase dissolved pot, be heated to 80-85 DEG C; 4 ~ 10 parts by weight of thickening agent, 1 ~ 5 weight portion lubricant are added in oil phase dissolving pan and is heated to 80-85 DEG C;
2) inhale material in a small amount of aqueous phase dissolved pot in emulsifying pot, then the material inhaling a small amount of oil phase dissolving pan is to homogenizing 5-10 minute in emulsifying pot, is sucked in emulsifying pot by the clout in aqueous phase dissolved pot simultaneously; Stir 20 minutes under 200-300 rev/min in a vacuum, add 2 ~ 7 weight portion conditioner for hair when being cooled to feed temperature≤40 DEG C in emulsifying pot and fully stir, rotating speed 200 revs/min;
3) in emulsifying pot, add water in advance dissolving 3 ~ 8 weight portion mass concentrations is 30-80% reductant solution, stir 2 minutes under the rotating speed of 200 revs/min, add 1 ~ 4 weight portion pH adjusting agent again, finally add 0.01 ~ 0.1 weight portion antiseptic, 0.1 ~ 1 weight portion essence fully stirs evenly, then room temperature is chilled to, detect the pH=8-8.1 of solution in emulsifying pot, TGA content when being 6.8%-11% and qualified, take the dish out of the pot, obtain described agent A;
Described dose of B is prepared by the step of following order:
First, 59.99-95.88 weight parts water, 4-15 weight portion oxidant are added in reaction pot, is stirred to oxidant with 150 revs/min of rotating speeds and fully dissolves;
Secondly, in described reaction pot, the 0.1-20 weight portion nonyl phenol polyethers-15 and 0.01-5 weight portion essence that mix in clean, dry anhydrous container is in advance added, by the mixed liquor mix homogeneously in reaction pot to as clear as crystal;
Finally, add 0.01-0.1 weight portion antiseptic in reaction pot, discharging when being uniformly mixed pH=4.0-7.0, the oxygenate content > 7% of rear detection mixed liquor with 150 revs/min of rotating speeds, obtains described agent B;
Wetting agent in described dose of A is glycerol, and emulsifying agent is octadecyl trimethyl ammonium chloride, and thickening agent is octadecanol, lubricant is isopropyl palmitate, and conditioner for hair is silicone oil, and reducing agent is Mercaptamine, PH regulator is monoethanolamine, and antiseptic is Kazon, and essence is odorant; Oxidant in described dose of B is sodium bromate.
2. a kind of using method exempting from the agent for permanent hair waving of softening burn according to claim 1, is characterized in that: described agent for permanent hair waving A and agent for permanent hair waving B be with the use of, using method is as follows: directly above after hair washing roll up varnish A, heating; Then cool 4-6 minute, without the need to bath, be directly coated with agent for permanent hair waving B, stop 5 minutes afterflush and namely complete hair-waving.
3. the using method exempting from the agent for permanent hair waving of softening burn according to claim 2, it is characterized in that: the heat time heating time after coating agent A is: resisting hair quality heat time heating time is 14 minutes, healthy hair quality heat time heating time is 11 minutes, general damaged hair heat time heating time is 8-10 minute, and extremely damaged hair heat time heating time is 4-5 minute.
4. the using method exempting from the agent for permanent hair waving of softening burn according to claim 2, is characterized in that: described agent B smears at twice, each stop 5 minutes.
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| CN103898749A (en) * | 2014-03-31 | 2014-07-02 | 许昌恒源发制品股份有限公司 | Wig slipping agent as well as preparation method and use method thereof |
| CN107375001A (en) * | 2017-07-24 | 2017-11-24 | 向明 | Odorlessness neutrality high temperature hair-waving decoction and preparation method thereof and application method |
| CN107375115A (en) * | 2017-08-22 | 2017-11-24 | 刘家明 | The boiling hot formula of hydrogen hydro-thermal and technique |
| CN108210402B (en) * | 2018-04-11 | 2021-06-01 | 大连大学 | Environment-friendly permanent wave agent suitable for families and preparation method thereof |
| CN109171156A (en) * | 2018-11-02 | 2019-01-11 | 北京痧之道科技发展有限公司 | A kind of non-softening plastotype method for permanent waving hair |
| EP4082523A4 (en) * | 2019-12-17 | 2023-08-09 | Konkuk University Industrial Cooperation Corp. | Hair perm forming method using electrolyzed water |
| CN113041165A (en) * | 2021-03-31 | 2021-06-29 | 广州威帕化妆品有限公司 | Low-pH-value zero-damage plant permanent wave agent and production method and use method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| DE19504091A1 (en) * | 1995-02-08 | 1996-08-22 | Wella Ag | Agent for permanent waving of hair |
| FR2769499B1 (en) * | 1997-10-10 | 2000-01-14 | Oreal | PROCESS OF PERMANENT DEFORMATION OF KERATINIC MATERIAL WITHOUT INTERMEDIATE RINSING |
| FR2769500B1 (en) * | 1997-10-10 | 2004-07-02 | Oreal | MULTI-COMPONENT REDUCING AGENT COMPRISING AT LEAST ONE POWDERED COMPOSITION CONTAINING REDUCER FOR DISULFIDE HAIR LINKS AND METHOD FOR PERMANENT DEFORMATION OF KERATINIC MATERIALS |
| DE19803803C1 (en) * | 1998-01-31 | 1999-09-09 | Henkel Kgaa | Process for permanent deformation of keratin fibers |
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