CN103045447B - Vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality - Google Patents
Vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality Download PDFInfo
- Publication number
- CN103045447B CN103045447B CN201210569608.7A CN201210569608A CN103045447B CN 103045447 B CN103045447 B CN 103045447B CN 201210569608 A CN201210569608 A CN 201210569608A CN 103045447 B CN103045447 B CN 103045447B
- Authority
- CN
- China
- Prior art keywords
- wine
- alcoholic strength
- pressure
- section
- vol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
The invention belongs to the technical field of brewing and provides a vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality, and aims at improving a traditional liquor taking method. Through a temperature transmitter above the outlet of a distinguisher lid of a grain distinguisher and an on-line alcoholic strength detector on a liquor discharge pipeline, the vapor phase temperature and the alcoholic strength of distilled liquor are monitored on line, the vapor phase temperature data and the monitored alcoholic strength data are real-timely transmitted to a DCS (Distributed Control System), and the DCS compares the real-time vapor phase pressure data and the alcoholic strength data with the preset pressure data and alcoholic strength data, and controls an automatic regulating valve at the liquor receiving part to be opened or closed automatically when the vapor phase pressure and the alcoholic strength data is equal to the preset pressure and alcoholic strength data respectively so as to achieve liquor taking according to the quality. The invention breaks the bonds of traditional experience of taking liquor according to liquor bubbles, the degree of automatic operation is improved, human errors are reduced, the liquor quality is guaranteed and the yield of high-quality liquor is improved.
Description
Technical field
The present invention relates to a kind of white wine and pluck wine method, be specifically related to, steaming gaseous pressure and alcoholic strength variation online piecewising algorithms amount quality picking wine technique in wine process, belong to brewing technical field.
Background technology
Amount quality picking wine is an important technological operation in White wine brewing process.Amount quality picking wine is exactly after foreshot's extraction, tastes accurately classification while plucking.Different amount quality picking wine processing methodes, has a great impact the quality of white wine, need control stream wine temperature when distillation, leaves out the beginning and the end.
At present, wine brewing operator pluck in wine process spirit brewing, and what generally adopt is to pluck wine experience with the tradition of " observing hops changing conditions, wine body odour, aroma change " to pluck wine.But tradition is plucked wine and is had following shortcoming:
1. see that it is the traditional technology that in white liquor distilling process, operator grasp wine degree height that flower is plucked wine, according to the shape of hops, size, time length, judges the height of wine liquid alcohol molecule content.But there is larger difference in interpersonal micro-judgment.The quality of plucking wine affects the yield of quality liquor largely, and at present, quality liquor yield is only 1.5～2.2%.
2. see that it is the mixing solutions of the alcohol based on various concentration and water that flower is measured, at certain pressure and temperature, the different surfaces tension force forming.The foam that alcohol produces, easily dissipates because tension force is little, and along with the rising of distillation temperature, ethanol concn reduces gradually, and the dissipation speed of the hops that alcohol produces constantly slows down, and the relative density of water is greater than alcohol, and tension force is large, and the dissipation speed of spray is slow.See that flower can be divided into 5 kinds: large blowing, little blowing, cloud flower, two flowers, oil bloom.But in stream wine process, hops and spray change comparatively fast alternately time, and interpersonal micro-judgment exists larger difference, likely cause excellent section of wine to enter one section or one section of wine and enter the intermixing such as excellent section, affect vinosity.
As application number 201210066632.9, name is called the application for a patent for invention of " method that continuous soft type white wine is plucked wine ", and its disclosed wine method of plucking comprises the following steps: a, by vinasse loaded steamer complete fermentation, steams wine, be laid on fat mouth to take wine cloth, and form groove shape; B, start stream and win after drinking one section of wine, aldehyde taste, the assorted taste of chaff in wine are won totally; C, one section of wine are won two sections of wine after winning, pluck disconnected when hops transit spray; D, start to win three sections of wine from transit spray, when disconnected flower, pluck disconnected; After e, three sections of wine are won, winning to alcoholic strength is to stop plucking wine at 1 o'clock, is four sections of wine.Meanwhile, the steam pressure value disclosing while steaming wine is 0.02～0.03MPa.
And for example application number CN200910083662.9, name is called the application for a patent for invention of " manufacturing process of dried orange peel beauty wine ", and the wine degree of plucking when it discloses distillation is 60,48,42 degree.
Although above patent has the vapor pressure when steaming wine and plucks wine degree and control plucking in wine process, but still be to adopt and traditional see flower is plucked wine and seen flower is measured and pluck wine in distillation liquid phase, thereby still exist personal errors to affect yield and the vinosity of wine.
Applicant finds under study for action, and because the material of different aromas composition in distillation there are differences on boiling point, thereby under identical distillation temperature, in the alcohol vapour that day part obtains, the content of each material must exist certain otherness.Be in particular in: the main component at distillation initial stage aggregation is ester, aldehyde and potato spirit; Along with the prolongation of distillation time, their content also declines thereupon.Methyl alcohol is low at first liquor and rear liquor part, and stage casing wine part is high.From high to low, ethyl acetate is more imbued with foreshot's part for ethyl acetate, ethyl hexanoate, ethyl butyrate.It is in 50% later wine tail that ethyl lactate is present in ethanol content in a large number.Ethyl palmitate, ethyl oleate and three kinds of compositions of ethyl linoleate are mainly enriched in foreshot's part, along with the carrying out of distillation, are saddle-shaped fluctuating.Isopropylcarbinol, n-propyl alcohol, propyl carbinol, sec-butyl alcohol are comparatively steadily and the trend of slow decreasing in still-process.Acetaldehyde and acetal progressively decline along with distillation process, more concentrate in front-end volatiles, and the acetaldehyde of total quantity of distillate 80% and 90% acetal are present in finished wine.That is to say have obvious variation and flex point at different duration of distillation alcohol vapour gaseous pressures and each cut section alcoholic strength.Carry out amount quality picking wine and still belong to pioneering and use it for brewed spirit industry, carry out segmentation amount quality picking wine at the alcoholic strength of wine body when controlling the gaseous pressure of alcohol vapour before cooling and go out wine of corresponding time period, science, reasonable more, quality liquor yield obviously improves.
Summary of the invention
The present invention is directed to tradition and pluck the above-mentioned shortcoming that wine method exists, provide a kind of gaseous pressure and alcoholic strength to change online piecewising algorithms amount quality picking wine technique.This technique is according to the different period various flavour ingredient boiling-point difference opposite sex of distillation, the alcoholic strength that steams fume phase pressure and each cut section all has the principle of considerable change and flex point, the gaseous pressure of Real-Time Monitoring steaming wine and alcohol vapour different fractions section are in the variation of cooling rear ethanol content, carry out amount quality picking wine, break traditional experience of seeing that flower is plucked wine, improved automated operation degree, reduced personal errors, guarantee wine product quality, promoted the yield of quality liquor.
The object of the invention is that technical scheme by being implemented as follows realizes.
Gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the pressure unit of discriminating lid outlet top by grain, and the alcoholic strength on-line detector arranging on wine output pipe, on-line monitoring steams gaseous pressure and the alcoholic strength of wine, by gaseous pressure data and the alcoholic strength data that monitor, be sent in real time DCS Controlling System, DCS Controlling System is by the judgement of comparing of real-time gaseous pressure data and alcoholic strength data and default pressure data and alcoholic strength data, work as gaseous pressure, when alcoholic strength data equate with default pressure and alcoholic strength data respectively, the control of DCS Controlling System connects the automatic regulating valve at wine place and automatically opens or close, carry out amount quality picking wine.
The quantity of described automatic regulating valve is identical with the segments of plucking wine.
The described wine of plucking divides nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, and the pressure that steams the first cut section of wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Described pressure unit is arranged on apart from grain discriminates 30～80cm place, lid outlet top.
When described steaming wine, required vapor pressure is: 0.02～0.03Mpa.
When described steaming wine, preferred vapor pressure is 0.025 Mpa.
Described stream wine temperature while plucking wine is 20～30 ℃.
It is described that preferably to flow wine temperature while plucking wine be 22 ℃.
Described alcoholic strength on-line detector is white wine alcohol on-line detector.
Described alcoholic strength on-line detector is made up of metal probe, the detection signal treatment system of acid-alkali-corrosive-resisting, in described detection signal treatment system, is provided with an alcohol content tester, and this detection signal treatment system is connected with the input terminus of DCS Controlling System.
The principle of work of described alcoholic strength on-line detector is: the alcoholic strength of the wine body that metal probe is detected, form with electrical signal is fed back and is given DCS Controlling System in time, on DCS control interface, demonstrate alcoholic strength changing conditions, and show the height variation tendency of alcoholic strength with curve form.
The technique effect that the present invention is useful is:
1, the present invention changes according to different period hops, its steaming fume phase pressure and wine body alcoholic strength have the principle of considerable change and flex point, respectively by pressure unit and alcoholic strength on-line detector, the alcoholic strength data of wine body by gaseous pressure and while going out wine, be sent in real time DCS Controlling System, the alcoholic strength variation tendency of alcohol vapour gaseous pressure and wine body when wine is steamed in online observation, and pluck wine technique in conjunction with tradition and carry out the multistage scientific and rational amount quality picking wine of multistage.Thereby break traditional experience of seeing that flower is plucked wine, improved automatic operation degree, reduced personal errors, evaded to greatest extent last cut section wine enter next section or a rear cut section wine enter the intermixings such as leading portion, effectively remove impurity, greatly improved the quality of wine.
2, the alcoholic strength that the present invention steams fume phase pressure and wine body by on-line monitoring changes; control and pluck wine by automation control system (DCS); the alcoholic strength of corresponding gaseous pressure and wine body is easily controlled; wine modernization, mass-producing are plucked in formation; not only fully retain main fragrance ingredient such as ester class, alcohols etc. contained in vinasse, also thoroughly removed assorted taste and toxic substance simultaneously, guaranteed wine product quality; promoted quality liquor " yield ", quality liquor yield improves more than 6.2%.
3, when the present invention plucks wine according to the alcoholic strength of alcohol vapour gaseous pressure and wine body, also the alcoholic strength to each section of wine and contained beneficiating ingredient have had compared with standard and have divided accurately, can form unified index system, not only be beneficial to the management of wine industry industry, but also can stop to pretend to be quality liquor to lead the generation of consumer behaviour into a trap with feints.
4, the present invention arranges multiple automatic regulating valves going out wine place, automatically opens or closes out wine valve, carries out segmentation and connects wine.Be convenient to the finished wine of different vinosity strictly to divide, reach the object that improves quality liquor yield.
5, the present invention adopts automatic control gaseous pressure and cut alcoholic strength amount quality picking wine, be conducive to carry out accurate segmentation to plucking wine, the present invention divides nine sections to pluck wine, and two sections of wine and three sections of wine are excellent section of wine, be convenient to the finished wine of different vinosity strictly to divide, be more conducive to improve the quality of wine.
6, the present invention is by the strict temperature of controlling water of condensation in condenser, and 20 ~ 30 ℃ of best wine temperature when stream wine temperature is controlled at out to wine have been avoided because excess Temperature makes in finished wine because of the ethanol molecule ethanol concn reduction causing of volatilize; And because temperature is too low and need to increase the problems such as aging time of finished wine.
7, when wine is steamed in control of the present invention, required vapor pressure is 0.02 ~ 0.03Mpa, and the best is 0.025 Mpa, reaches the object of slow fire stream wine by strict control vapor pressure, avoids the volatilization of wine too fast, causes flavour substances to run off, thereby has guaranteed the quality of wine.
8, the present invention adopts specific pressure and alcoholic strength control amount quality picking wine device, by automatic regulating valve and pressure unit are being set on main steam header road, vapor pressure signal is sent into DCS control device simultaneously, automatically control vapor pressure, reach the required vapor pressure processing requirement of each distillation sequence.
9, the present invention adopts specific pressure and alcoholic strength control amount quality picking wine device, by automatic regulating valve being set on water of condensation transport pipe, set temperature transmitter on wine output pipe, stream wine temperature signal is entered to DCS control device simultaneously, automatically control water of condensation operational throughput, the strict temperature of controlling water of condensation in condenser, required temperature process requirement while reaching wine.
Accompanying drawing explanation
Fig. 1 is that gaseous pressure of the present invention and wine body alcoholic strength change online amount quality picking wine process flow sheet
Fig. 2 is that gaseous pressure of the present invention and wine body alcoholic strength change online nine sections of amount quality picking wine process flow sheets
Fig. 3 is the different duration of distillation alcohol vapour gaseous pressures of the present invention and wine body alcoholic strength change curve
Fig. 4 is that the present invention steams wine gas phase temperature, gaseous pressure, wine body alcoholic strength and wine body flavour substances temporal evolution chart
Fig. 5 is the present invention while plucking wine by nine sections, alcoholic strength, flavour substances content chart in liquor body
Fig. 6 is the structural representation of pressure of the present invention and alcoholic strength control amount quality picking wine device
Mark in figure: 1, grain is discriminated, 2, discriminate lid, 3, condenser, 4, steam-pipe, 5, wine output pipe, 6, pressure unit, 7, DCS Controlling System, 8, automatic regulating valve, 9, pressure unit, 10, automatic regulating valve, 11, temperature transmitter, 12, automatic regulating valve, 13, plate-type heat exchanger, 14, outlet, 15, discriminate neck, 16, alcoholic strength online detection instrument.
Embodiment
Embodiment 1
Below in conjunction with embodiment, essentiality content of the present invention is described in further detail.
Embodiment 1
Gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the pressure unit of discriminating lid outlet top by grain, and the alcoholic strength on-line detector arranging on wine output pipe, on-line monitoring steams gaseous pressure and the alcoholic strength of wine, by gaseous pressure data and the alcoholic strength data that monitor, be sent in real time DCS Controlling System, DCS Controlling System is by the judgement of comparing of real-time gaseous pressure data and alcoholic strength data and default pressure data and alcoholic strength data, work as gaseous pressure, when alcoholic strength data equate with default pressure and alcoholic strength data respectively, the control of DCS Controlling System connects the automatic regulating valve at wine place and automatically opens or close, carry out amount quality picking wine.
Pluck wine and divide three sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with three, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～24.4KPa, and the alcoholic strength of second segment wine is 74.1～82.0%VOL; The pressure of the 3rd cut section is 24.5～100KPa, and the alcoholic strength of the 3rd section of wine is 81.9～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 30cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.02Mpa.
Stream wine temperature while plucking wine is 20 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Described alcoholic strength on-line detector is made up of metal probe, the detection signal treatment system of acid-alkali-corrosive-resisting, in described detection signal treatment system, is provided with an alcohol content tester, and this detection signal treatment system is connected with the input terminus of DCS Controlling System.
Embodiment 2
Basic identical with embodiment 1 processing step, on this basis:
Pluck wine and divide four sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with four, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～24.4KPa, and the alcoholic strength of second segment wine is 74.1～82.0%VOL; The pressure of the 3rd cut section is 24.5～39KPa, and the alcoholic strength of the 3rd section of wine is 81.9～69.1%VOL; The pressure of the 4th cut section is 39.1～100KPa, and the alcoholic strength of the 4th section of wine is 69.0～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 80cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.03Mpa.
Stream wine temperature while plucking wine is 30 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 3
Basic identical with embodiment 1 processing step, on this basis:
Pluck wine and divide nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 50cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.025Mpa.
Stream wine temperature while plucking wine is 22 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
In above-mentioned nine sections of liquor bodies, alcoholic strength, flavour substances content situation are shown in Fig. 5.
As seen from Figure 5, the wine body flavor substances content of two, three sections of wine is ideal, is excellent section of wine.
Embodiment 4
Basic identical with embodiment 1 processing step, on this basis:
Pluck wine and divide nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 60cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.023Mpa.
Stream wine temperature while plucking wine is 23 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Basic identical with embodiment 1 processing step, on this basis:
Pluck wine and divide nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 70cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.03Mpa.
Stream wine temperature while plucking wine is 28 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Basic identical with embodiment 1 processing step, on this basis:
Pluck wine and divide nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 40cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.026Mpa.
Stream wine temperature while plucking wine is 25 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 7
Basic identical with embodiment 1 processing step, on this basis:
Pluck wine and divide nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Pressure unit is arranged on apart from grain discriminates 40cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.024Mpa.
Stream wine temperature while plucking wine is 23 ℃.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
The main device the present invention relates to is: pressure and alcoholic strength control amount quality picking wine device
Described pressure and alcoholic strength control amount quality picking wine device are shown in accompanying drawing 6, comprise grain Zhen 1, discriminate and cover 2, condenser 3, steam-pipe 4 and wine output pipe 5, steam-pipe 4 connects grain and discriminates 1, Zhen covers 2 and is positioned at grain Zhen upper end, discriminate lid top and have an outlet 14, outlet 14 is connected with condenser 3 by pipeline, the vertical portion of the contiguous outlet of pipeline is for discriminating neck 15, condenser 3 connects wine output pipe 5, at Zhen, neck 15 places arrange pressure unit 6, alcoholic strength on-line detector 16 is set on wine output pipe 5, the wine place that connects at wine output pipe arranges automatic regulating valve 8, pressure unit 6 is connected DCS Controlling System 7 input terminuss with alcoholic strength on-line detector 16, DCS Controlling System 7 output terminals connect the automatic regulating valve 8 at wine place.
Described alcoholic strength on-line detector (16) is white wine alcohol on-line detector.
The described wine place that connects is provided with multiplely, and respectively configures an automatic regulating valve.
Automatic regulating valve 10 and pressure unit 9 are set on described steam-pipe 4, and pressure unit 9 connects DCS Controlling System 7 input terminuss, and DCS Controlling System 7 output terminals connect the automatic regulating valve 10 on steam-pipe.
On the water of condensation transport pipe of described condenser 3, automatic regulating valve 12 is set, set temperature transmitter 11 on wine output pipe 5, temperature transmitter 11 connects DCS Controlling System 7 input terminuss, and DCS Controlling System 7 output terminals connect the automatic regulating valve 12 on water of condensation transport pipe.
On the water of condensation transport pipe of described condenser 3,10M is set
2plate-type heat exchanger 13.
Claims (1)
1. gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the pressure unit of discriminating lid outlet top by grain, and the alcoholic strength on-line detector arranging on wine output pipe, on-line monitoring steams gaseous pressure and the alcoholic strength of wine, by gaseous pressure data and the alcoholic strength data that monitor, be sent in real time DCS Controlling System, DCS Controlling System is by the judgement of comparing of real-time gaseous pressure data and alcoholic strength data and default pressure data and alcoholic strength data, work as gaseous pressure, when alcoholic strength data equate with default pressure and alcoholic strength data respectively, the control of DCS Controlling System connects the automatic regulating valve at wine place and automatically opens or close, carry out amount quality picking wine,
The described wine of plucking divides nine sections to carry out according to steaming fume phase pressure with wine body alcoholic strength, and the automatic regulating valve that meets wine place is provided with nine, and the pressure of the first cut section of steaming wine is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The pressure of the second cut section is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The pressure of the 3rd cut section is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The pressure of the 4th cut section is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The pressure of the 5th cut section is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The pressure of the 6th cut section is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The pressure of the 7th cut section is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The pressure of the 8th cut section is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The pressure of the 9th cut section is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL;
Vapor pressure when described steaming wine is: 0.02～0.03Mpa;
Described stream wine temperature while plucking wine is 20～30 ℃.
2. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the quantity of described automatic regulating valve is identical with the segments of plucking wine.
3. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described pressure unit is arranged on apart from grain discriminates 30～80cm place, lid outlet top.
4. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: vapor pressure when described steaming wine is 0.025Mpa.
5. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described in stream wine temperature while plucking wine be 22 ℃.
6. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described alcoholic strength on-line detector is white wine alcohol on-line detector.
7. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described alcoholic strength on-line detector is made up of metal probe, the detection signal treatment system of acid-alkali-corrosive-resisting, in described detection signal treatment system, be provided with an alcohol content tester, and this detection signal treatment system is connected with the input terminus of DCS Controlling System.
8. gaseous pressure according to claim 1 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: realize this process using pressure and alcoholic strength control amount quality picking wine device, comprise grain Zhen (1), discriminate lid (2), condenser (3), steam-pipe (4) and wine output pipe (5), steam-pipe (4) connects grain and discriminates (1), discriminate lid (2) and be positioned at grain Zhen upper end, discriminate lid top and have an outlet (14), outlet (14) is connected with condenser (3) by pipeline, the vertical portion of the contiguous outlet of pipeline is for discriminating neck (15), condenser (3) connects wine output pipe (5), it is characterized in that: locate to arrange pressure unit (6) at Zhen neck (15), alcoholic strength online detection instrument (16) is set on wine output pipe (5), the wine place that connects at wine output pipe arranges automatic regulating valve (8), pressure unit (6) is connected DCS Controlling System (7) input terminus with alcoholic strength online detection instrument (16), DCS Controlling System (7) output terminal connects the automatic regulating valve (8) at wine place.
9. gaseous pressure according to claim 8 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the described wine place that connects is provided with multiplely, and respectively configures an automatic regulating valve.
10. gaseous pressure according to claim 8 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: automatic regulating valve (10) and pressure unit (9) are set on described steam-pipe (4), pressure unit (9) connects DCS Controlling System (7) input terminus, and DCS Controlling System (7) output terminal connects the automatic regulating valve (10) on steam-pipe.
11. gaseous pressures according to claim 8 and alcoholic strength change online amount quality picking wine technique, it is characterized in that: on the water of condensation transport pipe of described condenser (3), automatic regulating valve (12) is set, at the upper set temperature transmitter (11) of wine output pipe (5), temperature transmitter (11) connects DCS Controlling System (7) input terminus, and DCS Controlling System (7) output terminal connects the automatic regulating valve (12) on water of condensation transport pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210569608.7A CN103045447B (en) | 2012-12-25 | 2012-12-25 | Vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210569608.7A CN103045447B (en) | 2012-12-25 | 2012-12-25 | Vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103045447A CN103045447A (en) | 2013-04-17 |
| CN103045447B true CN103045447B (en) | 2014-07-02 |
Family
ID=48058312
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210569608.7A Active CN103045447B (en) | 2012-12-25 | 2012-12-25 | Vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103045447B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112180832A (en) * | 2020-11-04 | 2021-01-05 | 尧米(重庆)智能科技有限公司 | Artificial intelligent wine picking device and wine picking method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1322813A (en) * | 2001-02-26 | 2001-11-21 | 康达（成都）电子有限公司 | Dynamic technological-parameter monitoring system for fermentation tank in white spirit distillery |
| CN2682410Y (en) * | 2004-03-17 | 2005-03-02 | 田鹰 | On-line measuring apparatus for alcohol content and alcohol quantity of spirit |
| CN101153257A (en) * | 2007-09-27 | 2008-04-02 | 广州保捷机电有限公司 | Five-tower two-grade difference pressure distillation equipment for senior edible ethanol and technique thereof |
| CN202175668U (en) * | 2011-07-06 | 2012-03-28 | 刘民 | White wine brewage proportioning water numerical control device |
-
2012
- 2012-12-25 CN CN201210569608.7A patent/CN103045447B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1322813A (en) * | 2001-02-26 | 2001-11-21 | 康达（成都）电子有限公司 | Dynamic technological-parameter monitoring system for fermentation tank in white spirit distillery |
| CN2682410Y (en) * | 2004-03-17 | 2005-03-02 | 田鹰 | On-line measuring apparatus for alcohol content and alcohol quantity of spirit |
| CN101153257A (en) * | 2007-09-27 | 2008-04-02 | 广州保捷机电有限公司 | Five-tower two-grade difference pressure distillation equipment for senior edible ethanol and technique thereof |
| CN202175668U (en) * | 2011-07-06 | 2012-03-28 | 刘民 | White wine brewage proportioning water numerical control device |
Non-Patent Citations (2)
| Title |
|---|
| 固态发酵法白酒连续蒸馏工艺;黄亚东等;《酿酒科技》;20120731(第7期);94-96 * |
| 黄亚东等.固态发酵法白酒连续蒸馏工艺.《酿酒科技》.2012,(第7期),94-96. |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103045447A (en) | 2013-04-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103045446B (en) | Wine taking process based on alcohol content online measuring | |
| CN103045449B (en) | Vapor phase temperature and alcoholic strength variation on-line liquor taking process according to quality | |
| CN103045448B (en) | Wine taking process based on gas-phase temperature, pressure and alcohol content variation online measuring | |
| CN106018651B (en) | Analysis method and the application of wine are plucked in segmentation during white liquor distilling | |
| CN103436361B (en) | The blending of a kind of flavouring essence for tobacco intelligence, imitative fragrant method | |
| CN203096043U (en) | Flavor substance based online device for picking liquor according to quality | |
| CN103045445B (en) | Online quantitative liquor receiving process for flavor substances | |
| CN203174075U (en) | Device for controlling liquor taking process according to quality by temperature and alcoholic strength | |
| CN109266479A (en) | A kind of brewage process of brandy | |
| CN108041189A (en) | Tea perfume collector used in a kind of tea Processing method and this method | |
| CN203096042U (en) | Device for controlling liquor picking according to quality by utilizing temperature, pressure and alcohol content | |
| CN112795428A (en) | Lotus-fragrance-style tobacco essence and preparation method and application thereof | |
| CN103114028B (en) | Gas phase temperature and pressure changing online quality-based liquor making process | |
| CN103351948B (en) | Preparation method of Kaoliang liquor fragrance characteristic fragrance reference solution in liquor evaluation | |
| CN103045447B (en) | Vapor phase pressure and alcoholic strength variation on-line liquor taking process according to quality | |
| CN103725581A (en) | Distillation method for lowering ethyl lactate of white spirit | |
| CN107637858A (en) | A kind of plant for improving water extraction and alcohol precipitation method extraction causes perfumery and extracting method and application | |
| CN203096040U (en) | Device for controlling liquor picking according to quality by utilizing pressure and alcohol content | |
| CN203096044U (en) | Alcohol content based online device for picking liquor according to quality | |
| CN103114027B (en) | Gas-phase temperature change-based on-line quality-measuring liquor receiving process | |
| CN103114026B (en) | Gas-phase pressure change-based on-line quality-measuring liquor receiving process | |
| CN106190713A (en) | A kind of preparation method of Fragrant fruit wine | |
| CN203096041U (en) | Gas phase temperature change based online device for picking liquor according to quality | |
| CN108410637A (en) | Lichee brandy that the smell of fruits is very sweet and preparation method thereof | |
| CN203021543U (en) | Device for liquor taking according to quality through vapor phase temperature and pressure control |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |