CN103045448B - Wine taking process based on gas-phase temperature, pressure and alcohol content variation online measuring - Google Patents
Wine taking process based on gas-phase temperature, pressure and alcohol content variation online measuring Download PDFInfo
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- CN103045448B CN103045448B CN201210569678.2A CN201210569678A CN103045448B CN 103045448 B CN103045448 B CN 103045448B CN 201210569678 A CN201210569678 A CN 201210569678A CN 103045448 B CN103045448 B CN 103045448B
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Abstract
The invention belongs to the field of winemaking techniques, and provides a wine taking process based on gas-phase temperature and pressure variation online measuring, aiming at improving the traditional wine taking method. According to the invention, through the arrangement of alcohol content online measuring detectors on a temperature transmitter located above the outlet of a chamber cover of a grain chamber, a pressure transmitter and a wine outlet pipe, gas-phase temperature, gas-phase pressure and alcohol content can be measured online, relevant real-time data is immediately sent to a DCS (Design Control Specification) control system, the DCS control system compares the real-time gas-phase temperature, gas-phase pressure and alcohol content data with the preset gas-phase temperature, gas-phase pressure and alcohol content data, and when the real-time gas-phase temperature, the gas-phase pressure and the alcohol content data equal to the preset gas-phase temperature, the gas-phase pressure and the alcohol content data respectively, the DCS control system controls an automatic regulating valve of a wine taking part to open or close. The invention breaks the traditional experience of wine taking based on bubbles in the wine, improves the automatic operation degree, reduces human errors, ensures the quality of the wine products, and improves the yield of high-quality wine.
Description
Technical field
The present invention relates to a kind of white wine and pluck wine method, be specifically related to, steaming gas phase temperature in wine process, gaseous pressure and alcoholic strength variation online piecewising algorithms amount quality picking wine technique, belong to brewing technical field.
Background technology
Amount quality picking wine is an important technological operation in White wine brewing process.Amount quality picking wine is exactly after foreshot's extraction, tastes accurately classification while plucking.Different amount quality picking wine processing methodes, has a great impact the quality of white wine, need control stream wine temperature when distillation, leaves out the beginning and the end.
At present, wine brewing operator pluck in wine process spirit brewing, and what generally adopt is to pluck wine experience with the tradition of " observing hops changing conditions, wine body odour, aroma change " to pluck wine.But tradition is plucked wine and is had following shortcoming:
1. see that it is the traditional technology that in white liquor distilling process, operator grasp wine degree height that flower is plucked wine, according to the shape of hops, size, time length, judges the height of wine liquid alcohol molecule content.But there is larger difference in interpersonal micro-judgment.The quality of plucking wine affects the yield of quality liquor largely, and at present, quality liquor yield is only 1.5～2.2%.
2. see that it is the mixing solutions of the alcohol based on various concentration and water that flower is measured, at certain pressure and temperature, the different surfaces tension force forming.The foam that alcohol produces, easily dissipates because tension force is little, and along with the rising of distillation temperature, ethanol concn reduces gradually, and the dissipation speed of the hops that alcohol produces constantly slows down, and the relative density of water is greater than alcohol, and tension force is large, and the dissipation speed of spray is slow.See that flower can be divided into 5 kinds: large blowing, little blowing, Yun Hua, two flowers, oil bloom.But in stream wine process, hops and spray change comparatively fast alternately time, and interpersonal micro-judgment exists larger difference, likely cause excellent section of wine to enter one section or one section of wine and enter the intermixing such as excellent section, affect vinosity.
As application number 201110089637.9, name is called the application for a patent for invention of " method of storing Luzhou-flavor liquor ", and its disclosed wine method of plucking comprises the following steps: a, vinasse loaded steamer is steamed to wine; B, start stream after drinking, stream wine temperature is controlled to 25～35 degrees Celsius, get first paragraph wine, assorted aldehyde taste in wine body etc. taste is extractd totally; After c, one section of wine are won, it is two sections of wine that stream wine to hops turn little Hua, 25～35 degrees Celsius of stream wine temperature; After d, two sections of wine are won, it is three sections of wine that stream wine disappears to hops, 25～35 degrees Celsius of stream wine temperature; E, three sections of wine are got four sections of wine after winning, get while flowing out the alcoholic strength of wine to 0%vol and stop, 25～40 degrees Celsius of stream wine temperature.
And for example application number 201210066632.9, name is called the application for a patent for invention of " method that continuous soft type white wine is plucked wine ", and its disclosed wine method of plucking comprises the following steps: a, by vinasse loaded steamer complete fermentation, steams wine, be laid on fat mouth to take wine cloth, and form groove shape; B, start stream and win after drinking one section of wine, aldehyde taste, the assorted taste of chaff in wine are won totally; C, one section of wine are won two sections of wine after winning, pluck disconnected when hops transit spray; D, start to win three sections of wine from transit spray, when disconnected flower, pluck disconnected; After e, three sections of wine are won, winning to alcoholic strength is to stop plucking wine at 1 o'clock, is four sections of wine.Meanwhile, the steam pressure value disclosing while steaming wine is 0.02～0.03MPa.
For another example application number CN200910083662.9, name is called the application for a patent for invention of " manufacturing process of dried orange peel beauty wine ", and the wine degree of plucking when it discloses distillation is 60,48,42 degree.
Although above patent has the stream wine temperature to plucking wine or plucks wine degree and control plucking in wine process, traditional see flower is plucked wine and seen flower is measured and pluck wine but still adopt, thereby still exist personal errors to affect yield and the vinosity of wine.
Applicant finds under study for action, and because the material of different aromas composition in distillation there are differences on boiling point, thereby under identical distillation temperature, in the alcohol vapour that day part obtains, the content of each material must exist certain otherness.Be in particular in: the main component at distillation initial stage aggregation is ester, aldehyde and potato spirit; Along with the prolongation of distillation time, their content also declines thereupon.Methyl alcohol is low at first liquor and rear liquor part, and stage casing wine part is high.From high to low, ethyl acetate is more imbued with foreshot's part for ethyl acetate, ethyl hexanoate, ethyl butyrate.It is in 50% later wine tail that ethyl lactate is present in ethanol content in a large number.Ethyl palmitate, ethyl oleate and three kinds of compositions of ethyl linoleate are mainly enriched in foreshot's part, along with the carrying out of distillation, are saddle-shaped fluctuating.Isopropylcarbinol, n-propyl alcohol, propyl carbinol, sec-butyl alcohol are comparatively steadily and the trend of slow decreasing in still-process.Acetaldehyde and acetal progressively decline along with distillation process, more concentrate in front-end volatiles, and the acetaldehyde of total quantity of distillate 80% and 90% acetal are present in finished wine.That is to say have obvious variation and flex point at different duration of distillation alcohol vapour gas phase temperatures and each cut section alcoholic strength.Carry out amount quality picking wine and still belong to pioneering and use it for brewed spirit industry, carry out segmentation amount quality picking wine at the alcoholic strength of wine body when controlling gas phase temperature, the gaseous pressure of alcohol vapour before cooling and go out wine of corresponding time period, science, reasonable more, quality liquor yield obviously improves simultaneously.
Summary of the invention
The present invention is directed to tradition and pluck the above-mentioned shortcoming that wine method exists, provide a kind of gas phase temperature, gaseous pressure and alcoholic strength to change online piecewising algorithms amount quality picking wine technique.This technique is according to the different period various flavour ingredient boiling-point difference opposite sex of distillation, the alcoholic strength that steams wine gas phase temperature, gaseous pressure and each cut section all has the principle of considerable change and flex point, Real-Time Monitoring steams gas phase temperature, gaseous pressure and the alcohol vapour different fractions section of wine in the variation of cooling rear ethanol content, carry out amount quality picking wine, break traditional experience of seeing that flower is plucked wine, improved automated operation degree, reduced personal errors, guarantee wine product quality, promoted the yield of quality liquor.
The object of the invention is that technical scheme by being implemented as follows realizes.
Gas phase temperature, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the temperature transmitter of discriminating lid outlet top by grain, pressure unit and the alcoholic strength on-line detector arranging on wine output pipe, on-line monitoring steams the gas phase temperature of wine, gaseous pressure and alcoholic strength, by gas phase temperature data, gaseous pressure data and the alcoholic strength data that monitor, be sent in real time DCS Controlling System, DCS Controlling System is by real-time gas phase temperature data, gaseous pressure data and alcoholic strength data, with default temperature data, the judgement of comparing of pressure data and alcoholic strength data, work as gas phase temperature, gaseous pressure, alcoholic strength data respectively with default temperature, when pressure and alcoholic strength data equate, the control of DCS Controlling System connects the automatic regulating valve at wine place and automatically opens or close, carry out amount quality picking wine.
The quantity of described automatic regulating valve is identical with the segments of plucking wine.
The described wine of plucking divides nine sections to carry out according to steaming wine gas phase temperature, gaseous pressure and wine body alcoholic strength, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa, and the alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Described temperature transmitter is arranged on apart from grain discriminates 30～80cm place, lid outlet top.
Described pressure unit is arranged on apart from grain discriminates 30～80cm place, lid outlet top.
When described steaming wine, required vapor pressure is: 0.02～0.03Mpa.
When described steaming wine, preferred vapor pressure is 0.025 Mpa.
Described stream wine temperature while plucking wine is 20～30 DEG C.
It is described that preferably to flow wine temperature while plucking wine be 22 DEG C.
Described alcoholic strength on-line detector is white wine alcohol on-line detector.
Described alcoholic strength on-line detector is made up of metal probe, the detection signal treatment system of acid-alkali-corrosive-resisting, in described detection signal treatment system, is provided with an alcohol content tester, and this detection signal treatment system is connected with the input terminus of DCS Controlling System.
The principle of work of described alcoholic strength on-line detector is: the alcoholic strength of the wine body that metal probe is detected, form with electrical signal is fed back and is given DCS Controlling System in time, on DCS control interface, demonstrate alcoholic strength changing conditions, and show the height variation tendency of alcoholic strength with curve form.
The technique effect that the present invention is useful is:
1, the present invention changes according to different period hops, it steams wine gas phase temperature, gaseous pressure and wine body alcoholic strength the principle of considerable change and flex point, respectively by temperature transmitter, pressure unit and alcoholic strength on-line detector, the alcoholic strength data of wine body by gas phase temperature, gaseous pressure and while going out wine, be sent in real time DCS Controlling System, online alcoholic strength variation tendency of observing alcohol vapour gas phase temperature, gaseous pressure and wine body while steaming wine, and pluck wine technique in conjunction with tradition and carry out the multistage scientific and rational amount quality picking wine of multistage.Thereby break traditional experience of seeing that flower is plucked wine, improved automatic operation degree, reduced personal errors, evaded to greatest extent last cut section wine enter next section or a rear cut section wine enter the intermixings such as leading portion, effectively remove impurity, greatly improved the quality of wine.
2, the alcoholic strength that the present invention steams wine gas phase temperature, gaseous pressure and wine body by on-line monitoring changes; control and pluck wine by automation control system (DCS); the alcoholic strength of corresponding gas phase temperature, gaseous pressure and wine body is easily controlled; wine modernization, mass-producing are plucked in formation; not only fully retain main fragrance ingredient such as ester class, alcohols etc. contained in vinasse; assorted taste and objectionable impurities have also thoroughly been removed simultaneously; guarantee wine product quality; promoted quality liquor " yield ", quality liquor yield improves more than 6.2%.
3, when the present invention plucks wine according to the alcoholic strength of alcohol vapour gas phase temperature, gaseous pressure and wine body, also the alcoholic strength to each section of wine and contained beneficiating ingredient have had compared with specification and have divided accurately, can form unified index system, not only be beneficial to the management of wine industry industry, but also can stop to pretend to be quality liquor to lead the generation of consumer behaviour into a trap with feints.
4, the present invention arranges multiple automatic regulating valves going out wine place, automatically opens or closes out wine valve, carries out segmentation and connects wine.Be convenient to the finished wine of different vinosity strictly to divide, reach the object that improves quality liquor yield.
5, the present invention adopts automatic control gas phase temperature, gaseous pressure and cut alcoholic strength amount quality picking wine, be conducive to carry out accurate segmentation to plucking wine, the present invention divides nine sections to pluck wine, and two sections of wine and three sections of wine are excellent section of wine, be convenient to the finished wine of different vinosity strictly to divide, be more conducive to improve the quality of wine.
6, the present invention is by the strict temperature of controlling water of condensation in condenser, and 20～30 DEG C of best wine temperature when stream wine temperature is controlled at out to wine have been avoided because excess Temperature makes in finished wine because of the ethanol molecule ethanol concn reduction causing of volatilize; And because temperature is too low and need to increase the problems such as aging time of finished wine.
7, when wine is steamed in control of the present invention, required vapor pressure is 0.02～0.03Mpa, and the best is 0.025Mpa, reaches the object of slow fire stream wine by strict control vapor pressure, avoids the volatilization of wine too fast, causes flavour substances to run off, thereby has ensured the quality of wine.
8, the present invention adopts specific temperature, pressure and alcoholic strength control amount quality picking wine device, by automatic regulating valve and pressure unit are set on main steam header road, vapor pressure signal is sent into DCS control device simultaneously, automatically control vapor pressure, reach the required vapor pressure processing requirement of each distillation sequence.
9, the present invention adopts specific temperature, pressure and alcoholic strength control amount quality picking wine device, by automatic regulating valve being set on water of condensation transport pipe, set temperature transmitter on wine output pipe, stream wine temperature signal is entered to DCS control device simultaneously, automatically control water of condensation operational throughput, the strict temperature of controlling water of condensation in condenser, required temperature process requirement while reaching wine.
Brief description of the drawings
Fig. 1 is that gas phase temperature of the present invention, gaseous pressure and wine body alcoholic strength change online amount quality picking wine process flow sheet
Fig. 2 is that gas phase temperature of the present invention, gaseous pressure and wine body alcoholic strength change online nine sections of amount quality picking wine process flow sheets
Fig. 3 is the different duration of distillation alcohol vapour of the present invention gas phase temperature, gaseous pressure and wine body alcoholic strength change curve
Fig. 4 is that the present invention steams wine gas phase temperature, gaseous pressure, wine body alcoholic strength and wine body flavour substances temporal evolution chart
Fig. 5 is the present invention while plucking wine by nine sections, alcoholic strength, flavour substances content chart in liquor body
Fig. 6 is the structural representation of temperature of the present invention, pressure and alcoholic strength control amount quality picking wine device
Mark in figure: 1, grain is discriminated, 2, discriminate lid, 3, condenser, 4, steam-pipe, 5, wine output pipe, 6, temperature transmitter, 7, DCS Controlling System, 8, automatic regulating valve, 9, pressure unit, 10, automatic regulating valve, 11, temperature transmitter, 12, automatic regulating valve, 13, plate-type heat exchanger, 14, outlet, 15, Zhen Jing, 16, pressure unit, 17, alcoholic strength on-line detector.
Embodiment
Embodiment 1
Below in conjunction with embodiment, essentiality content of the present invention is described in further detail.
Embodiment 1
Gas phase temperature, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the temperature transmitter of discriminating lid outlet top by grain, pressure unit and the alcoholic strength on-line detector arranging on wine output pipe, on-line monitoring steams the gas phase temperature of wine, gaseous pressure and alcoholic strength, by gas phase temperature data, gaseous pressure data and the alcoholic strength data that monitor, be sent in real time DCS Controlling System, DCS Controlling System is by real-time gas phase temperature data, gaseous pressure data and alcoholic strength data, with default temperature data, the judgement of comparing of pressure data and alcoholic strength data, work as gas phase temperature, gaseous pressure, alcoholic strength data respectively with default temperature, when pressure and alcoholic strength data equate, the control of DCS Controlling System connects the automatic regulating valve at wine place and automatically opens or close, carry out amount quality picking wine.
Plucking wine divides three sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with three, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The second cut section temperature be 75.1～89.1 DEG C, pressure is 10.35～24.4KPa, the alcoholic strength of second segment wine is 74.1～82.0%VOL; The 3rd cut section temperature be 82～100 DEG C, pressure is 24.5～100KPa, the alcoholic strength of the 3rd section of wine is 81.9～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 60cm place, lid outlet top.Both guaranteed that the probe of temperature transmitter can accurately respond to the changing conditions of gas phase temperature, make again simultaneously operator lifting discriminate cover process in easy handling, and avoid temperature transmitter to suffer damage.
Pressure unit is arranged on apart from grain discriminates 30cm place, lid outlet top.Both guaranteed that the probe of pressure unit can accurately respond to the changing conditions of gaseous pressure, make again simultaneously operator lifting discriminate cover process in easy handling, and avoid pressure unit to suffer damage.
While steaming wine, required vapor pressure is: 0.02Mpa.
Stream wine temperature while plucking wine is 20 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Described alcoholic strength on-line detector is made up of metal probe, the detection signal treatment system of acid-alkali-corrosive-resisting, in described detection signal treatment system, is provided with an alcohol content tester, and this detection signal treatment system is connected with the input terminus of DCS Controlling System.
Embodiment 2
Basic identical with embodiment 1 processing step, on this basis:
Plucking wine divides four sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with four, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～81.9 DEG C, and pressure is 10.35～24.4KPa, and the alcoholic strength of second segment wine is 74.1～82.0%VOL; The temperature of the 3rd cut section is 82～93.4 DEG C, and pressure is 24.5～39KPa, and the alcoholic strength of the 3rd section of wine is 81.9～69.1%VOL; The temperature of the 4th cut section is 93.5～100 DEG C, and pressure is 39.1～100KPa, and the alcoholic strength of the 4th section of wine is 69.0～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 30cm place, lid outlet top.
Pressure unit is arranged on apart from grain discriminates 80cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.03Mpa.
Stream wine temperature while plucking wine is 30 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 3
Basic identical with embodiment 1 processing step, on this basis:
Plucking wine divides nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 80cm place, lid outlet top.
Pressure unit is arranged on apart from grain discriminates 50cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.025Mpa.
Stream wine temperature while plucking wine is 22 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
In above-mentioned nine sections of liquor bodies, alcoholic strength, flavour substances content situation are shown in Fig. 5.
As seen from Figure 5, the wine body flavor substances content of two, three sections of wine is ideal, is excellent section of wine.
Embodiment 4
Basic identical with embodiment 1 processing step, on this basis:
Plucking wine divides nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 40cm place, lid outlet top.
Pressure unit is arranged on apart from grain discriminates 60cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.023Mpa.
Stream wine temperature while plucking wine is 23 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 5
Basic identical with embodiment 1 processing step, on this basis:
Plucking wine divides nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 50cm place, lid outlet top.
Pressure unit is arranged on apart from grain discriminates 70cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.03Mpa.
Stream wine temperature while plucking wine is 28 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 6
Basic identical with embodiment 1 processing step, on this basis:
Plucking wine divides nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 70cm place, lid outlet top.
Pressure unit is arranged on apart from grain discriminates 40cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.026Mpa.
Stream wine temperature while plucking wine is 25 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 7
Basic identical with embodiment 1 processing step, on this basis:
Plucking wine divides nine sections to carry out according to steaming fume phase pressure and wine body alcoholic strength, the automatic regulating valve that meets wine place is provided with nine, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa; The alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL.
Temperature transmitter is arranged on apart from grain discriminates 60cm place, lid outlet top.
Pressure unit is arranged on apart from grain discriminates 30cm place, lid outlet top.
While steaming wine, required vapor pressure is: 0.024Mpa.
Stream wine temperature while plucking wine is 23 DEG C.
Alcoholic strength on-line detector is white wine alcohol on-line detector.
Embodiment 8
The main device the present invention relates to is: temperature, pressure and alcoholic strength control amount quality picking wine device
Described temperature, pressure and alcoholic strength control amount quality picking wine device are shown in accompanying drawing 6, comprise grain Zhen 1, discriminate and cover 2, condenser 3, steam-pipe 4 and wine output pipe 5, steam-pipe 4 connects grain and discriminates 1, Zhen covers 2 and is positioned at grain Zhen upper end, discriminate lid top and have an outlet 14, outlet 14 is connected with condenser 3 by pipeline, the vertical portion of the contiguous outlet of pipeline is for discriminating neck 15, condenser 3 connects wine output pipe 5, it is characterized in that: discriminating neck 15 place's set temperature transmitter 6 and pressure units 16, alcoholic strength on-line detector 17 is set on wine output pipe 5, the wine place that connects of wine output pipe arranges automatic regulating valve 8, temperature transmitter 6, pressure unit 16 is all connected DCS Controlling System 7 input terminuss with alcoholic strength on-line detector 17, DCS Controlling System 7 output terminals connect the automatic regulating valve 8 at wine place.
The described wine place that connects is provided with multiplely, and respectively configures an automatic regulating valve.
Automatic regulating valve 10 and pressure unit 9 are set on described steam-pipe 4, and pressure unit 9 connects DCS Controlling System 7 input terminuss, and DCS Controlling System 7 output terminals connect the automatic regulating valve 10 on steam-pipe.
On the water of condensation transport pipe of described condenser 3, automatic regulating valve 12 is set, set temperature transmitter 11 on wine output pipe 5, temperature transmitter 11 connects DCS Controlling System 7 input terminuss, and DCS Controlling System 7 output terminals connect the automatic regulating valve 12 on water of condensation transport pipe.
On the water of condensation transport pipe of described condenser 3, plate-type heat exchanger 13 is set; Described plate-type heat exchanger 13 is 10M
2plate-type heat exchanger.
Claims (9)
1. gas phase temperature, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the temperature transmitter of discriminating lid outlet top by grain, pressure unit and the alcoholic strength on-line detector arranging on wine output pipe, on-line monitoring steams the gas phase temperature of wine, gaseous pressure and alcoholic strength, by gas phase temperature data, gaseous pressure data and the alcoholic strength data that monitor, be sent in real time DCS Controlling System, DCS Controlling System is by real-time gas phase temperature data, gaseous pressure data and alcoholic strength data, with default temperature data, the judgement of comparing of pressure data and alcoholic strength data, work as gas phase temperature, gaseous pressure, alcoholic strength data respectively with default temperature, when pressure and alcoholic strength data equate, the control of DCS Controlling System connects the automatic regulating valve at wine place and automatically opens or close, carry out amount quality picking wine,
The described wine of plucking divides nine sections to carry out according to steaming wine gas phase temperature, gaseous pressure and wine body alcoholic strength, and the temperature of steaming the first cut section of wine is 72～75 DEG C, and pressure is 10.1～10.34KPa, and the alcoholic strength of first paragraph wine is 73.0～74.0%VOL; The temperature of the second cut section is 75.1～80.5 DEG C, and pressure is 10.35～12.9KPa, and the alcoholic strength of second segment wine is 74.1～79.0%VOL; The temperature of the 3rd cut section is 80.6～81.9 DEG C, and pressure is 13～24.4KPa, and the alcoholic strength of the 3rd section of wine is 79.1～82.0 %VOL; The temperature of the 4th cut section is 82～83.5 DEG C, and pressure is 24.5～26KPa, and the alcoholic strength of the 4th section of wine is 81.9～74.0%VOL; The temperature of the 5th cut section is 83.6～91.5 DEG C, and pressure is 26.1～32.5KPa, and the alcoholic strength of the 5th section of wine is 73.9～72.0%VOL; The temperature of the 6th cut section is 91.6～93.4 DEG C, and pressure is 32.6～39KPa, and the alcoholic strength of the 6th section of wine is 71.9～69.1%VOL; The temperature of the 7th cut section is 93.5～96 DEG C, and pressure is 39.1～52KPa, and the alcoholic strength of the 7th section of wine is 69.0～52.0%VOL; The temperature of the 8th cut section is 96.1～99.4 DEG C, and pressure is 52.1～78.5KPa, and the alcoholic strength of the 8th section of wine is 51.9～40.5%VOL; The temperature of the 9th cut section is 99.5～100 DEG C, and pressure is 78.6～100KPa, and the alcoholic strength of the 9th section of wine is 40.4～6.0%VOL;
Described temperature transmitter is arranged on apart from grain discriminates 30～80cm place, lid outlet top;
Vapor pressure when described steaming wine is: 0.02～0.03MPa;
Described stream wine temperature while plucking wine is 20～30 DEG C;
Realize this process using temperature, pressure and alcoholic strength control amount quality picking wine device, comprise grain Zhen (1), discriminate lid (2), condenser (3), steam-pipe (4) and wine output pipe (5), steam-pipe (4) connects grain and discriminates (1), discriminate lid (2) and be positioned at grain Zhen upper end, discriminate lid top and have an outlet (14), outlet (14) is connected with condenser (3) by pipeline, the vertical portion of the contiguous outlet of pipeline is for discriminating neck (15), condenser (3) connects wine output pipe (5), it is characterized in that: locate set temperature transmitter (6) and pressure unit (16) at Zhen neck (15), alcoholic strength on-line detector (17) is set on wine output pipe (5), the wine place that connects of wine output pipe arranges automatic regulating valve (8), temperature transmitter (6), pressure unit (16) is all connected DCS Controlling System (7) input terminus with alcoholic strength on-line detector (17), DCS Controlling System (7) output terminal connects the automatic regulating valve (8) at wine place.
2. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: the quantity of described automatic regulating valve is identical with the segments of plucking wine.
3. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change amount quality picking wine technique, it is characterized in that: described pressure unit is arranged on apart from grain discriminates 30～80cm place, lid outlet top.
4. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: vapor pressure when described steaming wine is 0.025 MPa.
5. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described in stream wine temperature while plucking wine be 22 DEG C.
6. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described alcoholic strength on-line detector is white wine alcohol on-line detector; Described alcoholic strength on-line detector is made up of metal probe, the detection signal treatment system of acid-alkali-corrosive-resisting, in described detection signal treatment system, is provided with an alcohol content tester, and this detection signal treatment system is connected with the input terminus of DCS Controlling System.
7. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described in pluck wine device the wine place that connects be provided with multiplely, and respectively configure an automatic regulating valve.
8. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described in pluck on the steam-pipe (4) of wine device automatic regulating valve (10) and pressure unit (9) be set, pressure unit (9) connects DCS Controlling System (7) input terminus, and DCS Controlling System (7) output terminal connects the automatic regulating valve (10) on steam-pipe.
9. gas phase temperature according to claim 1, gaseous pressure and alcoholic strength change online amount quality picking wine technique, it is characterized in that: described in pluck on the water of condensation transport pipe of condenser (3) of wine device automatic regulating valve (12) be set, at the upper set temperature transmitter (11) of wine output pipe (5), temperature transmitter (11) connects DCS Controlling System (7) input terminus, and DCS Controlling System (7) output terminal connects the automatic regulating valve (12) on water of condensation transport pipe.
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| CN105861253B (en) * | 2016-06-24 | 2019-04-19 | 江苏今世缘酒业股份有限公司 | Automation classification connects wine technique and device |
| CN111537685A (en) * | 2020-05-19 | 2020-08-14 | 河北工业大学 | Alcohol content online detection wine picking and blending system |
| CN114806794A (en) * | 2022-05-05 | 2022-07-29 | 西安唐泰节能环保科技有限公司 | Automatic control system and method for white spirit distillation |
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