CN103006509A - Emulsion composition and wet tissue applying emulsion composition - Google Patents
Emulsion composition and wet tissue applying emulsion composition Download PDFInfo
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- CN103006509A CN103006509A CN2012105437400A CN201210543740A CN103006509A CN 103006509 A CN103006509 A CN 103006509A CN 2012105437400 A CN2012105437400 A CN 2012105437400A CN 201210543740 A CN201210543740 A CN 201210543740A CN 103006509 A CN103006509 A CN 103006509A
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Abstract
The invention discloses an emulsion composition which comprises a cold sensitizer, a heat sensitizer and water, wherein the mass ratio of the cold sensitizer to the heat sensitizer is 1:0.01-100; the cold sensitizer comprises at least one of piperitol, menthyl lactate, hexa-carbon cyclic amide derivative, non-carbon cyclic amide derivative, mint raw oil, mint oil, mint essence, mint leaf extract, water-soluble menthol and water-soluble mint oil; and the heat sensitizer comprises at least one of vanillyl butyl ether, citronellol n-propyl ether, citronellol isopropyl ether, citronellol isobutyl ether, citronellol n-amino ether, citronellol isoamyl ether, citronellol n-hexyl ether, citronellol methyl ether, citronellol ether, gingerol, shogaol, zingerone, capsaicin and capsaicine. According to the emulsion composition and a wet tissue applying emulsion composition, the preparation process is simple, and the cost is low; a plurality of feeling organs of the skin of a human body can be simulated; and compared with a product which only stimulates a single feeling organ of the human body, the emulsion composition has relatively long refreshing time.
Description
Technical field
The present invention relates to a kind of emulsion compositions and use the wet tissue of this emulsion compositions.
Background technology
Modern society's rhythm of life is accelerated, dog-eat-dog causes people to live and operating pressure increases, the spirit emotion often is in high-pressure and state excitedly, easily occur tired, sleepy, the problems such as distractibility, impact study, work efficiency, even threat to life safety, cross for a long time or when opening night shift bus such as driver's driving time, tired, doze can occur unavoidably, easily cause vehicle accident, jeopardize individual and autre vie safety.To this, people usually adopt at skin surface wiping material or the volatile material different from skin temperature and change skin surface temperature, thus the fatigue and the sleepy sense that occur when stimulating cerebral nervous system, inspire enthusiasm to improve or eliminating work and study.
Traditional mode normally adopts cold/warm water to wash one's face, thereby inspires enthusiasm to produce thermal stimulation at skin, but the out of doors comparatively inconvenience of this mode.A lot of portable external preparation such as aerosol or smear series products, these products mainly comprise following two kinds: (1) with the composite plant liquid extract of many compositions as main refreshment composition; (2) with the pennyroyal composition as main refreshment composition.The complicated process of preparation of (1) series products, cost is high, and normal with the extractant of ethanol as product, because ethanol content is higher, also can stimulates eyes and user is done not feel like oneself.(2) series products mainly is to allow the people produce refrigerant sensation by cold sensation organ or the olfactory sensation that stimulates human body, thereby plays the effect of refreshment, but the time that the common cool feeling of this series products continues is shorter, and the effect of refreshment is unsatisfactory.
Summary of the invention
In view of this, be necessary to provide a kind of emulsion compositions, its preparation technology is simple, and is with low cost, and do not contain ethanol, easy to use, and the refreshment effect is lasting.
In addition, also be necessary to provide a kind of wet tissue that contains the above-mentioned emulsion compositions.
A kind of emulsion compositions, it contains cool feeling agent, heat sensitizer and water, and the two mass ratio of wherein cool feeling agent, heat sensitizer is 1:0.01-100; This cool feeling agent comprises at least a in menthol, menthol ester, hydrogenation of six carbocyclic amide derivatives, non-carbocyclic ring amide derivatives, raw peppermint oil, Oleum menthae, Herba Menthae quintessence oil, mentha leave extracting solution, water solublity Herba Menthae brain, the water solublity Herba Menthae oil; This heat sensitizer comprises the cephrol butyl ether, the cephrol n-propyl ether, the cephrol isopropyl ether, the cephrol isobutyl ether, the positive amino ethers of cephrol, the cephrol isoamyl ether, cephrol n-hexyl ether, the cephrol methyl ether, the cephrol ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, capsaicin (N-(4-hydroxyl-3-methoxybenzy)-8-methyl pelargonamide, (6E)-N-(4-hydroxyl-3-methoxybenzy)-8-methyl-6-nonenamide), at least a in the capsaicin analog.
A kind of wet tissue that contains the above-mentioned emulsion compositions, it comprises base material and is absorbed in emulsion compositions in the base material, wherein the mass ratio of emulsion compositions and base material is 1-5:1; Described base material is the material with suction, water holding capacity.
Emulsion compositions of the present invention and use the wet tissue of this emulsion compositions, processing technology is simple, with low cost, and esy to use, safe and reliable.Usually the generation of heat sensitizer hotness is guided by cool feeling, therefore when using this emulsion compositions, the existence of heat sensitizer can and prolong the lasting time of cool feeling in product and contact skin initial stage strengthen that emulsion compositions produces refrigerant or sensation and intensity that ice is refreshing.Approach to disappear or during complete obiteration in cool feeling, the cool feeling before the warmth sensation that the heat sensitizer in the emulsion compositions provides will be taken over, thus further stimulate human body to prolong the effect of the refreshment that mixed liquor produces.In addition, this emulsion compositions, has been avoided with ethanol as skin irritation problem that solvent was produced as solvent with water.
The specific embodiment
Emulsion compositions of the present invention contains cool feeling agent, heat sensitizer and an amount of water, the two mass ratio of wherein cool feeling agent, heat sensitizer is 1:0.01-100, wherein the quality percentage composition of cool feeling agent in emulsion compositions is 0.05%-15%, and the quality percentage composition of heat sensitizer in emulsion compositions is 0.001%-5%.
Thereby can be directly after this cool feeling agent and the contact skin and the effect of human body skin cold sensation receptor teleneuron produce physiological action and produce the refreshing sensation of refrigerant/ice.Thereby produce physiological reaction with human thermal sensation's organ teleneuron after this heat sensitizer and the contact skin and produce warm sensation.
Go back alternative in this emulsion compositions and be added with fragrant atmosphere composition, wherein cool feeling agent, heat sensitizer and fragrant atmosphere composition three's mass ratio is 1:0.01-100:0.01-50, and the quality percentage composition of fragrant atmosphere composition in emulsion compositions is 0.001%-5%.This perfume (or spice) atmosphere composition be have with Herba Menthae, Citrua paradiai, green tea, coffee, Fructus Citri Limoniae, Fructus Cucumidis sativi, lavandula angustifolia in essence, spice, quintessence oil or the extracting solution of at least a similar or same characteristic features abnormal smells from the patient.This perfume (or spice) atmosphere composition can stimulate the olfactory sensation of human body make the people produce refrigerant, ice is refreshing or salubrious pleasant sensation, and then feels spirit and QI cleaning.
Usually the generation of heat sensitizer hotness is guided by cool feeling, therefore when using this emulsion compositions, the existence of heat sensitizer can and prolong the lasting time of cool feeling in product and contact skin initial stage strengthen that emulsion compositions produces refrigerant or sensation and intensity that ice is refreshing.When cool feeling approaches disappearance or complete obiteration, cool feeling before the warmth sensation that heat sensitizer in the emulsion compositions provides will be taken over, thereby (heat sensitizer is with after human body skin contacts further to stimulate human body to prolong the effect of the refreshment that mixed liquor produces, what human body was at first experienced is the stimulation of similar cool feeling, then just can experience hotness, so this emulsion compositions at first allow the human feeling to be cool feeling, then be only hotness).The existence of fragrant atmosphere composition can be in emulsion compositions be strengthened the refreshment effect in cool feeling agent and the heat sensitizer performance function.Ternaryly exist simultaneously, can stimulate in use a plurality of sensory receptor officials of human body skin, avoid stimulating separately that same human body skin sensory organ is caused feels fatigue or benumb the effect of refreshing oneself of raising product.In addition, this emulsion compositions, has been avoided with ethanol as skin irritation problem that solvent was produced as solvent with water.
This cool feeling agent comprises at least a in menthol, menthol ester, hydrogenation of six carbocyclic amide derivatives, non-carbocyclic ring amide derivatives, raw peppermint oil, Oleum menthae, Herba Menthae quintessence oil, mentha leave extracting solution, water solublity Herba Menthae brain, the water solublity Herba Menthae wet goods.The freshener eutectic that this cool feeling agent preferably is comprised of menthol ester, hydrogenation of six carbocyclic amide derivatives and non-carbocyclic ring amide derivatives.
This menthol ester comprises at least a in Herba Menthae lactate, menthyl 2-pyrrolidone-5-carboxylic acid ester, succinic acid menthyl ester, 3-hydroxybutyrate menthyl ester, monomethyl succinate, p-menthyl-3-hydroxy acid-1-vinyl glyceride (WS-4), p-menthyl-3-hydroxy acid-1-glyceride (WS-30), 1,3-propanedicarboxylic acid-menthyl ester, 3-citraconic acid-menthyl ester, the 2-citraconic acid ester group menthyl monomenthyl glutarate.
This hydrogenation of six carbocyclic amide derivatives comprises terpane formyl ethamine; N-(4-methoxyphenyl)-to menthyl-3-carboxylic acid amides (WS-12); the N-tert-butyl group-to menthyl-3-carboxylic acid amides (WS-14); N-(glycine ethyl ester base)-2-isopropyl-5-methyl-cyclohexyl alkane amide (WS-5); N-(2-(2-pyridine radicals) ethyl)-2-isopropyl-5-methyl-cyclohexyl alkane amide; N-(4-acetylphenyl)-to amide of mint; N-(4-hydroxymethyl phenyl)-to amide of mint and N-(3-hydroxy-4-methoxyphenyl)-to amide of mint; at least a in N-((5-methyl-2-(1-Methylethyl) cyclohexyl) carbonyl) alanine ethyl ester.
This non-carbocyclic ring amide derivatives comprises methyl diisopropyl propionic acid amide., N, N-diethyl 2,2-dimethyl propylene amide, N, at least a in N-diethyl 2-ethyl butyramide, the heptane-2-carboxylic acid amides.
This heat sensitizer comprises at least a in cephrol butyl ether, cephrol n-propyl ether, cephrol isopropyl ether, cephrol isobutyl ether, the positive amino ethers of cephrol, cephrol isoamyl ether, cephrol n-hexyl ether, cephrol methyl ether, cephrol ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, capsaicin (N-(4-hydroxyl-3-methoxybenzy)-8-methyl pelargonamide and/or (6E)-N-(4-hydroxyl-3-methoxybenzy)-8-methyl-6-nonenamide), the capsaicin analog, preferably cephrol butyl ether.
Further, in order to make being present in the wet tissue that emulsion compositions can be stable, can add the emulsifying solubilizing agent emulsion compositions is dispersed in the wet tissue uniformly.This emulsifying solubilizing agent is hydrophilic single emulsifying solubilizing agent or the compound emulsifying solubilizing agent of hydrophilic hydrophobic balance value (Hydrophile-Lipophile Balance Number, HLB) greater than 10.The emulsifying solubilizing agent specifically comprises tween 20, Tween-60, tween 80, tween 20, tween 80, Tween-60, alkyl polyglucoside and derivant thereof, the PEG-20 sucrose stearate, the PEG-5 glyceryl stearate, Cremophor RH40, the PEG-60 castor oil hydrogenated, ceteareth-6, ceteareth-25, stearyl alcohol polyethers-2, stearyl alcohol polyethers-21, laureth-4, laureth-23, single or the compound emulsifying solubilizing agent that the PEG-40 tristerin forms.
Further, in order to improve the skin protection performance of this emulsion compositions, also can add skin protectant in the emulsion compositions.This skin protectant comprises alcohols skin protectant, natural plants skin protectant, skin moistening oils and fats.The alcohols skin protectant comprises 1,3 butylene glycol, glycerol, propylene glycol, pentanediol etc.; The natural plants skin protectant comprises hyaluronate sodium, Aloe, collagen protein, oat beta-glucan, hydrolyzed wheat protein, Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, Semen pruni armeniacae oil, olive oil, Jojoba wet goods.The skin moistening oils and fats comprises isopropyl myristate, polydimethylsiloxane, Polyethylene Glycol-7 glyceryl cocoate, Polyethylene Glycol-6 caprylic/capric glyceride type, dicaprylyl carbonate, caprylic/capric triglyceride, isopropyl palmitate, octyl palmitate, Vitamin E acetate etc.
Further, in order to improve the antiinflammatory antiallergic performance of emulsion compositions, can in emulsion compositions, add natural antiinflammatory anti-allergic agent, improve the to external world irritation of environment of skin.This antiinflammatory anti-allergic agent comprises Flos Matricariae chamomillae extracting solution, bisabolol, Flos Lonicerae extractive solution, tea tree ethereal oil, Flos Inulae extracting solution, Radix Glycyrrhizae and derivant thereof, Rhizoma Zingiberis Recens extracting solution, Herba Portulacae extract etc.
Further, for the acid-base value that the makes emulsion compositions acid-base balance value near skin, also an amount of pH adjusting agent can be added in emulsion compositions, such as citric acid, sodium citrate, triethanolamine etc.
Further, in order to improve the storage time of emulsion compositions, can in emulsion compositions, add an amount of antiseptic.
Further, also can in emulsion compositions, add film former, thickening agent, other surfactant etc. to satisfy the actual demand of emulsion compositions.
Wet tissue of the present invention comprises base material and is absorbed in emulsion compositions in the base material, and wherein the mass ratio of emulsion compositions and base material is 1-5:1.Described base material is the material with suction, water holding capacity, concrete non-woven fabrics, cotton, gauze, towel, wet-strength paper etc.
Emulsion compositions of the present invention and use the wet tissue of this emulsion compositions, processing technology is simple, with low cost, and can stimulate a plurality of sensory organ of human body skin, with only to stimulate the single sensory product of human body to compare the refreshment time longer.In addition since with water as solvent, compare skin irritation with ethanol as the refreshment product of solvent and reduce, and esy to use, safe and reliable.
Come the present invention is specifically described below by embodiment.
Embodiment 1
Emulsion compositions preparation: (1) adds about 70% water in the allotment bucket, and the tween 20 of cephrol butyl ether and 0.5% is added in the keg, after mixing, adds an amount of water and continues to add after the stirring and emulsifying (emulsion should be creamy white) in the allotment barrel; (2) tween 20 with freshener eutectic and 2.0% adds in the keg, after mixing, adds an amount of water and continues to add in the allotment bucket after the stirring and emulsifying (emulsion should be creamy white); (3) Aloe, Flos Matricariae chamomillae extracting solution, glycerol, cucumber extract, antiseptic are added in the allotment bucket, stir, add at last pH adjusting agent and get final product about with the pH regulator to 6.0 of mixed emulsion.
The prescription of emulsion compositions is specifically joined shown in the table one.
Wet tissue is made: be that 3:1 adds on the base material (addition manner is immersion) with emulsion compositions according to the mass ratio of emulsion compositions and base material, cut into needed size again and can make required wet tissue.
Table one
Embodiment 2
Emulsion compositions preparation: (1) adds about 70% water in the allotment bucket, and the tween 20 of cephrol butyl ether and 1.5% is added in the keg, after mixing, adds an amount of water and continues to add after the stirring and emulsifying (emulsion should be creamy white) in the allotment barrel; (2) Citrua paradiai essence and Cremophor RH40 are added in the keg, after mixing, add an amount of water and continue to add in the allotment bucket after the stirring and emulsifying (emulsion should be creamy white); (3) tween 20 with tea tree ethereal oil and 0.5% adds in the keg, after mixing, adds an amount of water and continues to add in the allotment bucket after the stirring and emulsifying; (4) successively 1,3 butylene glycol, water solublity Herba Menthae oil, mentha leave extracting solution, Flos Lonicerae extractive solution, antiseptic are added in the allotment bucket, stir, add at last pH adjusting agent and get final product about with the pH regulator to 6.0 of mixed emulsion.
The prescription of emulsion compositions is specifically joined shown in the table two.
Wet tissue is made: be that 3.5:1 adds (addition manner is for spraying) on the base material to emulsion compositions according to the mass ratio of emulsion combination and base material, cut into needed size again and can make required wet tissue.
Table two
Through verification experimental verification: use the wet tissue wiping skin of embodiment 1-2 can produce the lasting effect of refreshing oneself.
In addition, those skilled in the art also can make various modifications, interpolation and the replacement on other form and the details in claim of the present invention scope of disclosure and spirit.Certainly, these all should be included within the present invention's scope required for protection according to the variations such as various modifications, interpolation and replacement that spirit of the present invention is made.
Claims (13)
1. emulsion compositions, it is characterized in that: this emulsion compositions contains cool feeling agent, heat sensitizer and water, and the two mass ratio of wherein cool feeling agent, heat sensitizer is 1:0.01-100; This cool feeling agent comprises at least a in menthol, menthol ester, hydrogenation of six carbocyclic amide derivatives, non-carbocyclic ring amide derivatives, raw peppermint oil, Oleum menthae, Herba Menthae quintessence oil, mentha leave extracting solution, water solublity Herba Menthae brain, the water solublity Herba Menthae oil; This heat sensitizer comprises the cephrol butyl ether, the cephrol n-propyl ether, the cephrol isopropyl ether, the cephrol isobutyl ether, the positive amino ethers of cephrol, the cephrol isoamyl ether, cephrol n-hexyl ether, the cephrol methyl ether, the cephrol ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, capsaicin (N-(4-hydroxyl-3-methoxybenzy)-8-methyl pelargonamide, (6E)-N-(4-hydroxyl-3-methoxybenzy)-8-methyl-6-nonenamide), at least a in the capsaicin analog.
2. emulsion compositions as claimed in claim 1, it is characterized in that: the quality percentage composition of this cool feeling agent in emulsion compositions is 0.05%-15%, the quality percentage composition of heat sensitizer in emulsion compositions is 0.001%-5%.
3. emulsion compositions as claimed in claim 1, it is characterized in that: also containing in this emulsion compositions has fragrant atmosphere composition, wherein cool feeling agent, heat sensitizer and fragrant atmosphere composition three's mass ratio is 1:0.01-100:0.01-50, this perfume (or spice) atmosphere composition be have with Herba Menthae, Citrua paradiai, green tea, coffee, Fructus Citri Limoniae, Fructus Cucumidis sativi, lavandula angustifolia in essence, spice, quintessence oil or the extracting solution of at least a similar or same characteristic features abnormal smells from the patient.
4. emulsion compositions as claimed in claim 3, it is characterized in that: the quality percentage composition of this perfume (or spice) atmosphere composition in emulsion compositions is 0.001%-5%.
5. emulsion compositions as claimed in claim 1 is characterized in that: the freshener eutectic that this cool feeling agent is comprised of menthol ester, hydrogenation of six carbocyclic amide derivatives and non-carbocyclic ring amide derivatives.
6. emulsion compositions as claimed in claim 1 is characterized in that: this menthol ester comprises at least a in Herba Menthae lactate, menthyl 2-pyrrolidone-5-carboxylic acid ester, succinic acid menthyl ester, 3-hydroxybutyrate menthyl ester, monomethyl succinate, p-menthyl-3-hydroxy acid-1-vinyl glyceride (WS-4), p-menthyl-3-hydroxy acid-1-glyceride (WS-30), 1,3-propanedicarboxylic acid-menthyl ester, 3-citraconic acid-menthyl ester, the 2-citraconic acid ester group menthyl monomenthyl glutarate; This hydrogenation of six carbocyclic amide derivatives comprises terpane formyl ethamine, N-(4-methoxyphenyl)-to menthyl-3-carboxylic acid amides (WS-12), the N-tert-butyl group-to menthyl-3-carboxylic acid amides (WS-14), N-(glycine ethyl ester base)-2-isopropyl-5-methyl-cyclohexyl alkane amide (WS-5), N-(2-(2-pyridine radicals) ethyl)-2-isopropyl-5-methyl-cyclohexyl alkane amide, N-(4-acetylphenyl)-to amide of mint, N-(4-hydroxymethyl phenyl)-to amide of mint and N-(3-hydroxy-4-methoxyphenyl)-to amide of mint, at least a in N-((5-methyl-2-(1-Methylethyl) cyclohexyl) carbonyl) alanine ethyl ester; This non-carbocyclic ring amide derivatives comprises methyl diisopropyl propionic acid amide., N, N-diethyl 2,2-dimethyl propylene amide, N, at least a in N-diethyl 2-ethyl butyramide, the heptane-2-carboxylic acid amides.
7. emulsion compositions as claimed in claim 1, it is characterized in that: this emulsion compositions also contains the emulsifying solubilizing agent, and this emulsifying solubilizing agent is hydrophilic hydrophobic balance value greater than 10 the single emulsifying solubilizing agent of hydrophilic or compound emulsifying solubilizing agent.
8. emulsion compositions as claimed in claim 7, it is characterized in that: this emulsifying solubilizing agent comprises tween 20, Tween-60, tween 80, tween 20, tween 80, Tween-60, alkyl polyglucoside and derivant thereof, the PEG-20 sucrose stearate, the PEG-5 glyceryl stearate, Cremophor RH40, the PEG-60 castor oil hydrogenated, ceteareth-6, ceteareth-25, stearyl alcohol polyethers-2, stearyl alcohol polyethers-21, laureth-4, laureth-23, single or the compound emulsifying solubilizing agent that the PEG-40 tristerin forms.
9. emulsion compositions as claimed in claim 1 is characterized in that: also optionally be added with at least a in skin protectant, antiinflammatory anti-allergic agent, pH adjusting agent, antiseptic, film former, thickening agent, the surfactant in this emulsion compositions.
10. emulsion compositions as claimed in claim 9, it is characterized in that: this skin protectant comprises alcohols skin protectant, natural plants skin protectant, skin moistening oils and fats, this alcohols skin protectant comprises glycerol, 1,3 butylene glycol, propylene glycol, pentanediol, Polyethylene Glycol; This natural plants skin protectant comprises Aloe, collagen protein, oat beta-glucan, hydrolyzed wheat protein, transparent sodium phytate, Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, Semen pruni armeniacae oil, olive oil; This skin moistening oils and fats comprises caprylic/capric triglyceride, octyl palmitate, polydimethylsiloxane, dicaprylyl carbonate, isopropyl myristate, isopropyl palmitate, white mineral oil, Vitamin E acetate.
11. emulsion compositions as claimed in claim 9 is characterized in that: this antiinflammatory anti-allergic agent comprises Flos Matricariae chamomillae extracting solution, bisabolol, Flos Lonicerae extractive solution, tea tree ethereal oil, Flos Inulae, Radix Glycyrrhizae and derivant thereof, Rhizoma Zingiberis Recens extracting solution, Herba Portulacae extract; This pH adjusting agent comprises citric acid, sodium citrate, triethanolamine.
12. a wet tissue that contains any described emulsion compositions among the claim 1-11, it comprises base material and is absorbed in emulsion compositions in the base material, and wherein the mass ratio of emulsion compositions and base material is 1-5:1; Described base material is the material with suction, water holding capacity.
13. wet tissue as claimed in claim 12 is characterized in that: this base material is non-woven fabrics, cotton, gauze, towel or wet-strength paper.
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